CN101999493B - Preparation method of plant health-care cool tea - Google Patents
Preparation method of plant health-care cool tea Download PDFInfo
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- CN101999493B CN101999493B CN 201010577936 CN201010577936A CN101999493B CN 101999493 B CN101999493 B CN 101999493B CN 201010577936 CN201010577936 CN 201010577936 CN 201010577936 A CN201010577936 A CN 201010577936A CN 101999493 B CN101999493 B CN 101999493B
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- 241000196324 Embryophyta Species 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 241001122767 Theaceae Species 0.000 title abstract description 17
- 238000000605 extraction Methods 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000011347 resin Substances 0.000 claims abstract description 11
- 229920005989 resin Polymers 0.000 claims abstract description 11
- 239000003480 eluent Substances 0.000 claims abstract description 10
- 238000010992 reflux Methods 0.000 claims abstract description 9
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims abstract description 4
- 230000001954 sterilising effect Effects 0.000 claims abstract description 4
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 3
- 239000000284 extract Substances 0.000 claims description 17
- 244000183685 Citrus aurantium Species 0.000 claims description 8
- 235000007716 Citrus aurantium Nutrition 0.000 claims description 8
- 241000233855 Orchidaceae Species 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 238000011010 flushing procedure Methods 0.000 claims description 6
- 238000013467 fragmentation Methods 0.000 claims description 6
- 238000006062 fragmentation reaction Methods 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 241000205585 Aquilegia canadensis Species 0.000 claims description 4
- 244000025254 Cannabis sativa Species 0.000 claims description 4
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 4
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims description 4
- 240000007171 Imperata cylindrica Species 0.000 claims description 4
- 240000000249 Morus alba Species 0.000 claims description 4
- 235000008708 Morus alba Nutrition 0.000 claims description 4
- 235000006753 Platycodon grandiflorum Nutrition 0.000 claims description 4
- 240000003582 Platycodon grandiflorus Species 0.000 claims description 4
- 244000215777 Plumeria rubra Species 0.000 claims description 4
- 235000013087 Plumeria rubra Nutrition 0.000 claims description 4
- 244000046146 Pueraria lobata Species 0.000 claims description 4
- 235000010575 Pueraria lobata Nutrition 0.000 claims description 4
- 244000185386 Thladiantha grosvenorii Species 0.000 claims description 4
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 claims description 4
- 235000013399 edible fruits Nutrition 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 230000006837 decompression Effects 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims description 3
- 238000011084 recovery Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000000108 ultra-filtration Methods 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 244000269722 Thea sinensis Species 0.000 claims 4
- 235000013616 tea Nutrition 0.000 claims 4
- 235000019224 Camellia sinensis var Qingmao Nutrition 0.000 claims 2
- 235000020339 pu-erh tea Nutrition 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 5
- 238000004440 column chromatography Methods 0.000 abstract description 4
- 230000006378 damage Effects 0.000 abstract description 4
- 235000016709 nutrition Nutrition 0.000 abstract description 4
- 238000005406 washing Methods 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 4
- 239000000470 constituent Substances 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 230000035764 nutrition Effects 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 8
- 235000013361 beverage Nutrition 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- 239000012535 impurity Substances 0.000 description 3
- 238000002372 labelling Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 235000010980 cellulose Nutrition 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 235000019789 appetite Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
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- Non-Alcoholic Beverages (AREA)
- Cosmetics (AREA)
- Alcoholic Beverages (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides a preparation method of plant health-care cool tea, comprising the following steps of: crushing raw materials, then carrying out reflux extraction with a solvent, and then filtering; filtering filter liquor through a micropore, and then carrying out macroporous resin column chromatography; washing with distilled water, and then eluting with an ethanol solvent; filtering the collected eluent by using a filtering membrane; concentrating and drying the filter liquor to obtain extractum; and carrying out blending, acid regulation and sterilization to obtain the plant health-care cool tea. The extractum extracted by the method has high purity and yield; in addition, the plant health-care cool tea prepared from the extractum has the advantages of pure color, translucent crystal, stable property and little damage to nutrition constituents.
Description
Technical field
The present invention relates to the plant beverage field, be specifically related to a kind of preparation method of plant health-care cold tea.
Background technology
The plant beverage of existing market is of a great variety, taste is different, production technology is simple boiling, or simple technology such as water extract-alcohol precipitation, contain impurity such as a large amount of celluloses, electrolyte, pigment in the medicinal extract that extracts, make that the destruction of target component and nutritional labeling is big because high temperature decocts.
Summary of the invention
The invention provides a kind of preparation method of plant health-care cold tea, the medicinal extract purity height that the inventive method is extracted, the yield height, pure, sparkling and crystal-clear bright with the plant health-care cold tea color and luster of this medicinal extract allotment, stable performance, the destruction of nutritional labeling is few.
The present invention adopts following technical scheme for achieving the above object:
The preparation method of plant health-care cold tea is characterized in that: specifically may further comprise the steps:
(1) raw material is carried out fragmentation after the weighing in proportion;
(2) leaching liquor is joined in the raw material after the fragmentation, carry out refluxing extraction, the weight ratio of leaching liquor and raw material is: (5-10): 1, and extraction time is 2-4 hour;
(3) mixture that refluxing extraction is finished carries out filter and remove residue, collects filtered fluid;
(4) filtered fluid with step (3) filters through the millipore filter of 1-5mm, and the filtrate of gained adds the absorption of low pole macropore resin post, uses distilled water flushing low pole macropore resin post 2-3 time again;
(5) with 30-80% ethanolic solution flushing low pole macropore resin post, wash to eluent Fei Linshi reaction colourless till, collect eluent;
(6) the eluent decompression of collecting is concentrated and the recovery solvent, the relative density that is concentrated into concentrate is 1.02-1.12;
(7) with the concentrate ultrafiltration membrance filter;
(8), get medicinal extract shape raw extract with the ultrafiltrate drying;
(9) a certain proportion of distilled water is joined in the medicinal extract, after stirring, after acid adjustment, blending, sterilization, make plant health-care cold tea of the present invention again; Described blending is the aroma ingredients that adds when allocating the smell of cold tea from bitter orange flower and orchid extraction;
The ratio of the weight portion of described each raw material is a honeysuckle: chrysanthemum: frangipanis: celestial grass: balloonflower root: Momordica grosvenori: the root of kudzu vine: cogongrass rhizome: Radix Glycyrrhizae: sealwort: general bait tea: mulberry fruit: bitter orange flower: orchid: water=(2-8): (2-8): (10-20): (5-15): (10-15): (10-20): (10-20): (5-10): (1-4): (5-10): (10-20): (2-10): (1-3): (1-2): (8000-10000).
The preparation method of described plant health-care cold tea is characterized in that: the described leaching liquor of step (2) is the ethanolic solution of 30-70%; The aperture of used milipore filter is 100,000-300,000 molecular weight in the step (8).
Beneficial effect of the present invention:
1, the production technology of traditional plant beverage is simple boiling, or simple technology such as water extract-alcohol precipitation, contains impurity such as a large amount of celluloses, electrolyte, pigment in the medicinal extract of extraction.Big molecule and small molecular weight impurity can be fully removed in the combination of this process using film separation and column chromatography technology, and the purity of target components is increased to more than 80%.
2, this process using low-concentration ethanol solution refluxing extraction technology, by refluxing, composition as much as possible can be dissolved out, flavones a large amount of in the prescription, saponin(e and polyphenol component effectively are dissolved out, make the yield of extraction higher, reach more than 60%.
3, adopted macropore resin column chromatography technology in this extraction process, this The Application of Technology can make nonpolar pigment composition be separated effectively, make the pigment content in the medicinal extract of final separation reduce to minimum, thereby it is pure, sparkling and crystal-clear bright with its color and luster of products such as beverage of this medicinal extract allotment, and be difficult for prolonging in time and change color, increased aesthetic feeling and appetite sense.The shelf-life of product can be longer simultaneously.
4, this invention has taked column chromatography to separate two kinds of separation purifying techniques with film on manufacture craft, and the composition of extraction all separates at low temperatures, to the destruction minimum of target component in the product and nutritional labeling.
The specific embodiment
A kind of preparation method of plant health-care cold tea specifically may further comprise the steps:
(1) choose raw material in following ratio earlier: the ratio of the weight portion of each raw material (gram) is: honeysuckle: chrysanthemum: frangipanis: celestial grass: balloonflower root: Momordica grosvenori: the root of kudzu vine: cogongrass rhizome: Radix Glycyrrhizae: sealwort: general bait tea: mulberry fruit: bitter orange flower: orchid: water=(2-8): (2-8): (10-20): (5-15): (10-15): (10-20): (10-20): (5-10): (1-4): (5-10): (10-20): (2-10): (1-3): (1-2): (8000-10000).Raw material is carried out fragmentation after the weighing in proportion;
(2) 70% ethanolic solution is joined in the raw material (not comprising bitter orange flower and orchid) after the fragmentation, carry out refluxing extraction, the weight ratio of ethanolic solution and raw material is: 6:1, and extraction time is 3 hours;
(3) mixture that refluxing extraction is finished carries out filter and remove residue, collects filtered fluid;
(4) filtered fluid with step (3) filters through the millipore filter of 5mm, and the filtrate of gained adds the absorption of low pole macropore resin post, uses distilled water flushing low pole macropore resin post 3 times again, discards washing lotion;
(5) with 80% ethanolic solution flushing low pole macropore resin post, wash to eluent Fei Linshi reaction colourless till, collect eluent;
(6) the eluent decompression of collecting is concentrated and recovery ethanol, the relative density that is concentrated into concentrate is 1.02-1.12;
(7) with the concentrate ultrafiltration membrance filter;
(8), get medicinal extract shape raw extract with the ultrafiltrate freeze drying; Extract the aroma ingredients in bitter orange flower and the orchid, make aqua aromatica;
(9) a certain proportion of distilled water is joined in the medicinal extract, after stirring, after acid adjustment, blending, sterilization, make plant health-care cold tea of the present invention again; Blending is to add when allocating the smell of cold tea from bitter orange flower and orchid to extract the aqua aromatica that makes.
Claims (2)
1. the preparation method of a plant health-care cold tea is characterized in that: specifically may further comprise the steps:
(1) honeysuckle, chrysanthemum, frangipanis, celestial grass, balloonflower root, Momordica grosvenori, the root of kudzu vine, cogongrass rhizome, Radix Glycyrrhizae, sealwort, Pu'er tea, mulberry fruit in the raw material are carried out fragmentation after the weighing in proportion;
(2) leaching liquor is joined in the raw material after the fragmentation, carry out refluxing extraction, the weight ratio of leaching liquor and raw material is: (5-10): 1, and extraction time is 2-4 hour; Described leaching liquor is 70% ethanolic solution;
(3) mixture that refluxing extraction is finished carries out filter and remove residue, collects filtered fluid;
(4) filtered fluid with step (3) filters through the millipore filter of 1-4 μ m, and the filtrate of gained adds the absorption of low pole macroporous resin column, uses distilled water flushing low pole macroporous resin column 2-3 time again;
(5) with 80% ethanolic solution flushing low pole macroporous resin column, wash to eluent Fei Linshi reaction colourless till, collect eluent;
(6) the eluent decompression of collecting is concentrated and the recovery solvent, the relative density that is concentrated into concentrate is 1.02-1.12;
(7) with the concentrate ultrafiltration membrance filter;
(8), get medicinal extract shape raw extract with the ultrafiltrate drying;
(9) a certain proportion of distilled water is joined in the medicinal extract, after stirring, after acid adjustment, blending, sterilization, make plant health-care cold tea again; Described blending is the aroma ingredients that adds when allocating the smell of cold tea from bitter orange flower and orchid extraction;
The weight part ratio of described each raw material is a honeysuckle: chrysanthemum: frangipanis: celestial grass: balloonflower root: Momordica grosvenori: the root of kudzu vine: cogongrass rhizome: Radix Glycyrrhizae: sealwort: Pu'er tea: mulberry fruit: bitter orange flower: orchid: distilled water=(2-8): (2-8): (10-20): (5-15): (10-15): (10-20): (10-20): (5-10): (1-4): (5-10): (10-20): (2-10): (1-3): (1-2): (8000-10000).
2. the preparation method of plant health-care cold tea according to claim 1, it is characterized in that: the molecular cut off of used milipore filter is 100,000-300,000 in the step (7).
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| Application Number | Priority Date | Filing Date | Title |
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| CN 201010577936 CN101999493B (en) | 2010-12-08 | 2010-12-08 | Preparation method of plant health-care cool tea |
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| CN 201010577936 CN101999493B (en) | 2010-12-08 | 2010-12-08 | Preparation method of plant health-care cool tea |
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| CN101999493A CN101999493A (en) | 2011-04-06 |
| CN101999493B true CN101999493B (en) | 2013-07-31 |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102232454A (en) * | 2011-08-05 | 2011-11-09 | 葛双铭 | Fire-removing tea |
| CN102919422B (en) * | 2012-10-31 | 2014-01-01 | 深圳市深宝技术中心有限公司 | Process for extracting herbal tea concentrate |
| CN105325616A (en) * | 2014-08-12 | 2016-02-17 | 天台山康能保健食品有限公司 | Technology for processing honeysuckle flower herbal tea |
| CN104255996A (en) * | 2014-09-02 | 2015-01-07 | 岳西县皖山绿生态农业开发有限公司 | Coconut milk flavored polygonatum sibiricum substituted tea and preparation method thereof |
| CN104322796A (en) * | 2014-10-09 | 2015-02-04 | 合肥跃杰生态农业科技有限公司 | Health care tea and making method thereof |
| CN104856032A (en) * | 2015-06-01 | 2015-08-26 | 巨鹿县三丰银杞饮品有限公司 | Method for preparing honeysuckle beverage concentrate through recycled solvent |
| CN105168262A (en) * | 2015-10-22 | 2015-12-23 | 河南行知专利服务有限公司 | Preparation method of traditional Chinese medicine decocting-free preparation containing carbohydrate |
| CN106605818B (en) * | 2016-12-13 | 2020-01-17 | 暨南大学 | Instant granule of Shangqingyin and its preparation method |
| CN109662226A (en) * | 2019-01-31 | 2019-04-23 | 广西古岭龙食品有限公司 | The preparation method of plant beverage |
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| CN100560578C (en) * | 2004-06-07 | 2009-11-18 | 辽宁新中现代医药有限公司 | A kind ofly be used to prevent and treat asthenopic plant milk extract and preparation and preparation method |
| CN101669558B (en) * | 2009-09-27 | 2012-05-02 | 安徽板蓝花生物科技有限公司 | Composite plant beverage |
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