CN101991113A - Sea cucumber oil soft capsule and preparation method thereof - Google Patents
Sea cucumber oil soft capsule and preparation method thereof Download PDFInfo
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- CN101991113A CN101991113A CN201010564243XA CN201010564243A CN101991113A CN 101991113 A CN101991113 A CN 101991113A CN 201010564243X A CN201010564243X A CN 201010564243XA CN 201010564243 A CN201010564243 A CN 201010564243A CN 101991113 A CN101991113 A CN 101991113A
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Abstract
The invention discloses a sea cucumber oil soft capsule and a preparation method thereof. The sea cucumber oil soft capsule comprises the following compatible formula: a weight ratio of sea cucumber oil to vegetable oil is 1:9-3:7. The preparation method comprises the following steps of: blending, filling and granulating according to the formula. The invention belongs to the field of deep processing of the sea cucumber oil. The prepared sea cucumber oil soft capsule has the characteristics of low cost and rich nutriments, and can be used for health care and beautifying.
Description
Technical field
The present invention relates to a kind of accessory substance sea cucumber oil and vegetable oil of producing in the sea cucumber process of utilizing and allocate the sea cucumber fat capsule that forms, belong to the technical field of marine product deep processing.
Background technology
Sea cucumber is as the profuse marine prods of a kind of nutritive value, and its body and accessory substance deep processing using value thereof are very high.
Sea cucumber oil is meant and utilizes the boil matter, sea cucumber intestine, sea cucumber that produce in sea cucumber and the sea cucumber process to be rich in nutritious oily maters such as DHA, EPA, arachidonic acid, leukotrienes, linoleic acid through the biotechnology preparation.At present, the research application of sea cucumber oil only rests on the research and development stage of sea cucumber oil both at home and abroad, as 200910013942.2 1 kinds of methods of boiling extraction sea cucumber oil the matter of number of patent application from sea cucumber, application number 200910011137.6 sea cucumber oil products and preparation method thereof patent disclosure adopt sea cucumber to boil the method that matter or sea cucumber prepare sea cucumber oil, both are all disclosed all to be how to boil matter or sea cucumber from sea cucumber, sea cucumber intestine, sea cucumber is extracted the method for sea cucumber oil, and, have only the manufacture method of number of patent application 200610134221.3 sea cucumber oil to disclose a kind of sea cucumber boiling water that utilizes at present in sea cucumber oil deep processing field, the sea cucumber internal organ are the research that raw material is made soy sauce.Above-mentioned disclosed patent is the preparation of sea cucumber oil or utilizes the document of its processing soy sauce, and expand sea cucumber oil value field in the deep processing of sea cucumber oil, all do not have relevant research at present both at home and abroad, the potential comprehensive utilization value of sea cucumber oil deep processing also fails fully to tap the latent power out.
Summary of the invention
In order to improve the value of sea cucumber oil deep processing, the invention provides a kind of sea cucumber fat capsule and preparation method thereof, this sea cucumber fat capsule is that the sea cucumber oil that boils matter, sea cucumber intestine, sea cucumber extraction from sea cucumber with applicant invention is raw material, add the sea cucumber fat capsule that vegetable oil system forms, this method comprises allotment, can and granulation.
In order to realize the present invention, its concrete technical scheme is as follows:
A kind of sea cucumber fat capsule and preparation method thereof, its sea cucumber fat capsule by component with following formula compatibility: sea cucumber oil is 1 with the vegetable oil weight ratio: 9-3: 7.
In the above-mentioned prescription, described vegetable oil is any vegetable oil in palm oil, olive oil, the soybean salad oil, and this vegetable oil is the common edible vegetable oil in market;
In the above-mentioned prescription, described sea cucumber oil utilizes the accessory substance that produces in the sea cucumber process for the applicant---and sea cucumber is boiled the sea cucumber oil that matter, sea cucumber intestine, sea cucumber are extracted through biotechnology, this sea cucumber oil main component is to check according to GB/T17376-2008, GB/T17377-2008, DHA content 6.2%.-7.4%, EPA content 23.47%-28.8%, arachidonic acid content 8.5%-11.1%, linolenic acid content 0.76%-1.11%, linoleic acid content 4.2%-6.88%.
A kind of sea cucumber fat capsule and preparation method thereof, its preparation method comprises allotment, can and granulation step according to above-mentioned prescription:
Step 1: allotment
1) preparation content: get sea cucumber oil, under the normal temperature, be 1 by sea cucumber oil with the vegetable oil weight ratio: 9-3: 7 mix, and grind 20-60 minute on colloid mill, make uniform liquid, and splendid attire is standby;
2) preparation capsule shells: get gelatin, glycerine, pure water, chocolate brown food coloring, ratio is a gelatin: glycerine: water: chocolate brown pigment=1.0: 0.2-0.4: 1.0-1.2: 0.005, take by weighing in above ratio, in the addingization glue bucket, be warming up to 60 ℃, stirred 4 hours, be incubated 50 ℃-60 ℃, placed 6-8 hour, the degassing, standby.
Step 2: can
The sizing material bucket of insulation is connected with capsule machine, the content of allotment is put into hopper, according to the content loading amount, select to roll mould, adjusting pelleting parameter is as follows: glue box temperature: 50 ℃-52 ℃, sprinkler body temperature: 40 ℃-42 ℃, adhesive tape thickness: 0.8mm rolls mould rotating speed: 1.8rpm/min, regulates loading amount, the tolerant heavy 0.50g of every intragranular makes soft capsule.
Step 3: granulate
Step 2 is sent in the rotating cage through the soft capsule that the capsule machine pelleting extrudes, blows 14 ℃ of cold wind while rotating, typing is dry, the soft capsule that typing is finished is contained in pallet and is shakeout, under 25 ℃ of environment, continued dry 4 hours, and soft capsule remained on surface liquid was cleaned, bottling with 95% ethanol.
Colloid mill, change glue bucket, capsule machine equipment that this preparation method is related are industry common equipment.
Adopt the sea cucumber fat capsule of the present invention's preparation to have abundant nutritive value, can be used as health care, cosmetics are directly taken, its concrete nutrition component is as follows:
Lead≤0.5mg/kg, inorganic arsenic≤0.5mg/kg, methyl mercury≤0.5mg/kg, total plate count≤30000cfu/g, coliform≤90MPN/100g, mould, saccharomycete 25cfu/g, EPA 〉=0.5g/100g, DHA 〉=1.5g/100g, arachidonic acid 〉=0.2g/100g, acid value≤3.0mg/g, peroxide value≤0.25g/100g.
The main detection method of above-mentioned nutrient content is as follows:
Plumbous: as to press GB5009.12-2010, inorganic arsenic: press GB/T5009.11-2003, methyl mercury: press GB/T5009.17-1996, total plate count: press GB4789.2-2010, coliform: press GB4789.3-2010, mould, saccharomycete: press 4789.15-2010, EPA: press GB/T17376-2008, DHA: press GB/T17376-2008, arachidonic acid: press GB/T17376-2008, acid value: press GB/T5009.37-2003, peroxide value: press GB/T5009.37-2003.
Patent of the present invention belongs to the deep processing of sea cucumber oil, has low cost of manufacture, the characteristics nutritious, that market value is very high.
The specific embodiment
The present invention is described in more detail below in conjunction with embodiment.
Embodiment 1
Step 1: allotment
1) preparation content: sea cucumber oil and the palm oil of getting DHA content 6.2%, EPA content 28.8%, arachidonic acid content 8.5%, linolenic acid content 0.76%, linoleic acid content 4.2% are mixing at normal temperatures in 1: 9 by weight, on colloid mill, ground 20 minutes, make uniform liquid, splendid attire is standby;
2) preparation capsule shells: get gelatin, glycerine, pure water, chocolate brown food coloring, ratio is a gelatin: glycerine: water: chocolate brown pigment=1.0: 0.2-0.4: 1.0-1.2: 0.005, take by weighing in above ratio, in the addingization glue bucket, be warming up to 60 ℃, stirred 4 hours, be incubated 50 ℃, placed 6 hours, the degassing, standby.
Step 2: can
The sizing material bucket of insulation is connected with capsule machine, the content of allotment is put into hopper, according to the content loading amount, select to roll mould, adjusting pelleting parameter is as follows: glue box temperature: 50 ℃, sprinkler body temperature: 40 ℃, adhesive tape thickness: 0.8mm rolls mould rotating speed: 1.8rpm/min, regulates loading amount, the tolerant heavy 0.50g of every intragranular makes soft capsule.
Step 3: granulate
Step 2 is sent in the rotating cage through the soft capsule that the capsule machine pelleting extrudes, blows 14 ℃ of cold wind while rotating, typing is dry, the soft capsule that typing is finished is contained in pallet and is shakeout, under 25 ℃ of environment, continued dry 4 hours, and soft capsule remained on surface liquid was cleaned, bottling with 95% ethanol.
Embodiment 2
Step 1: allotment
1) preparation content: sea cucumber oil and the olive oil of getting DHA content 7.4%, EPA content 23.47%, arachidonic acid content 11.1%, linolenic acid content 1.11%, linoleic acid content 6.88% are mixing at normal temperatures in 3: 7 by weight, on colloid mill, ground 60 minutes, make uniform liquid, splendid attire is standby;
2) preparation capsule shells: get gelatin, glycerine, pure water, chocolate brown food coloring, ratio is a gelatin: glycerine: water: chocolate brown pigment=1.0: 0.2-0.4: 1.0-1.2: 0.005, take by weighing in above ratio, in the addingization glue bucket, be warming up to 60 ℃, stirred 4 hours, be incubated 60 ℃, placed 8 hours, the degassing, standby.
Step 2: can
The sizing material bucket of insulation is connected with capsule machine, the content of allotment is put into hopper, according to the content loading amount, select to roll mould, adjusting pelleting parameter is as follows: glue box temperature: 52 ℃, sprinkler body temperature: 42 ℃, adhesive tape thickness: 0.8mm rolls mould rotating speed: 1.8rpm/min, regulates loading amount, the tolerant heavy 0.50g of every intragranular makes soft capsule.
Step 3: granulate
Step 2 is sent in the rotating cage through the soft capsule that the capsule machine pelleting extrudes, blows 14 ℃ of cold wind while rotating, typing is dry, the soft capsule that typing is finished is contained in pallet and is shakeout, under 25 ℃ of environment, continued dry 4 hours, and soft capsule remained on surface liquid was cleaned, bottling with 95% ethanol.
Embodiment 3
Step 1: allotment
1) preparation content: the sea cucumber oil and the soybean salad oil weight ratio of getting DHA content 6.8%, EPA content 25%, arachidonic acid content 10%, linolenic acid content 1%, linoleic acid content 5.5% are mixing at normal temperatures in 3: 7, on colloid mill, ground 60 minutes, make uniform liquid, splendid attire is standby;
2) preparation capsule shells: get gelatin, glycerine, pure water, chocolate brown food coloring, ratio is a gelatin: glycerine: water: chocolate brown pigment=1.0: 0.2-0.4: 1.0-1.2: 0.005, take by weighing in above ratio, in the addingization glue bucket, be warming up to 60 ℃, stirred 4 hours, be incubated 55 ℃, placed 7 hours, the degassing, standby.
Step 2: can
The sizing material bucket of insulation is connected with capsule machine, the content of allotment is put into hopper, according to the content loading amount, select to roll mould, adjusting pelleting parameter is as follows: glue box temperature: 51 ℃, sprinkler body temperature: 41 ℃, adhesive tape thickness: 0.8mm rolls mould rotating speed: 1.8rpm/min, regulates loading amount, the tolerant heavy 0.50g of every intragranular makes soft capsule.
Step 3: granulate
Step 2 is sent in the rotating cage through the soft capsule that the capsule machine pelleting extrudes, blows 14 ℃ of cold wind while rotating, typing is dry, the soft capsule that typing is finished is contained in pallet and is shakeout, under 25 ℃ of environment, continued dry 4 hours, and soft capsule remained on surface liquid was cleaned, bottling with 95% ethanol.
Adopt the sea cucumber fat capsule of the present invention's preparation to check checking by experiment, have the advantages that to be of high nutritive value, can be widely used in health care, improve looks directly take product, and the market sale price can reach 1.5 yuan/.
Claims (2)
1. sea cucumber oil capsule and preparation method thereof is characterized in that: described sea cucumber oil capsule by component with following formula compatibility: sea cucumber oil is 1 with the vegetable oil weight ratio: 9-3: 7; Described vegetable oil is any vegetable oil in palm oil, olive oil, the soybean salad oil; Described sea cucumber oil is DHA content 6.2%.-7.4%, EPA content 23.47%-28.8%, arachidonic acid content 8.5%-11.1%, linolenic acid content 0.76%-1.11%, linoleic acid content 4.2%-6.88%.
2. sea cucumber oil capsule and preparation method thereof, it is characterized in that: the preparation method comprises allotment, can and granulation step:
Step 1: allotment
1) preparation content: get sea cucumber oil, under the normal temperature, be 1 by sea cucumber oil with the vegetable oil weight ratio: 9-3: 7 mix, and grind 20-60 minute on colloid mill, make uniform liquid, and splendid attire is standby;
2) preparation capsule shells: get gelatin, glycerine, pure water, chocolate brown food coloring, ratio is a gelatin: glycerine: water: chocolate brown pigment=1.0: 0.2-0.4: 1.0-1.2: 0.005, take by weighing in above ratio, in the addingization glue bucket, be warming up to 60 ℃, stirred 4 hours, be incubated 50 ℃-60 ℃, placed 6-8 hour, the degassing, standby;
Step 2: can
The sizing material bucket of insulation is connected with capsule machine, the content of allotment is put into hopper, according to the content loading amount, select to roll mould, adjusting pelleting parameter is as follows: glue box temperature: 50 ℃-52 ℃, sprinkler body temperature: 40 ℃-42 ℃, adhesive tape thickness: 0.8mm rolls mould rotating speed: 1.8rpm/min, regulates loading amount, the tolerant heavy 0.50g of every intragranular makes soft capsule;
Step 3: granulate
Step 2 is sent in the rotating cage through the capsule that the capsule machine pelleting extrudes, blows 14 ℃ of cold wind while rotating, typing is dry, the soft capsule that typing is finished is contained in pallet and is shakeout, continuing with 95% ethanol soft capsule remained on surface liquid to be cleaned bottling between dry 4 hours under 25 ℃ of environment.
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| CN201010564243XA CN101991113B (en) | 2010-11-30 | 2010-11-30 | Sea cucumber oil soft capsule and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102823666A (en) * | 2012-09-18 | 2012-12-19 | 大连海晏堂生物有限公司 | Sea cucumber lipid preparation and preparation method thereof |
| CN103340846A (en) * | 2013-07-02 | 2013-10-09 | 黑龙江八一农垦大学 | Arachidonic acid soft capsule and preparation method |
| CN107699359A (en) * | 2017-11-24 | 2018-02-16 | 黑龙江美丽石岛科技开发有限公司 | A kind of extraction process of sea cucumber intestine egg oil and the method that sea cucumber intestine ovum oil soft capsule is prepared using sea cucumber intestine egg oil |
| CN110236197A (en) * | 2019-05-15 | 2019-09-17 | 池州市月亮湾生物科技有限公司 | Sea cucumber intestine egg oil composition, sea cucumber intestine ovum oil soft capsule and preparation method thereof |
| CN111096457A (en) * | 2019-12-21 | 2020-05-05 | 池州市月亮湾生物科技有限公司 | Sea cucumber oil microcapsule powder and preparation method thereof |
Citations (2)
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| CN101473979A (en) * | 2009-01-17 | 2009-07-08 | 青岛佳日隆海洋食品有限公司 | Method for extracting trepang oil from boiled trepang juice |
| CN101530127A (en) * | 2009-04-10 | 2009-09-16 | 大连海晏堂生物有限公司 | Sea cucumber oil product and method for preparing same |
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2010
- 2010-11-30 CN CN201010564243XA patent/CN101991113B/en not_active Expired - Fee Related
Patent Citations (2)
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| CN101473979A (en) * | 2009-01-17 | 2009-07-08 | 青岛佳日隆海洋食品有限公司 | Method for extracting trepang oil from boiled trepang juice |
| CN101530127A (en) * | 2009-04-10 | 2009-09-16 | 大连海晏堂生物有限公司 | Sea cucumber oil product and method for preparing same |
Non-Patent Citations (1)
| Title |
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| 张强等: "《药剂学》", 31 January 2008 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102823666A (en) * | 2012-09-18 | 2012-12-19 | 大连海晏堂生物有限公司 | Sea cucumber lipid preparation and preparation method thereof |
| CN103340846A (en) * | 2013-07-02 | 2013-10-09 | 黑龙江八一农垦大学 | Arachidonic acid soft capsule and preparation method |
| CN107699359A (en) * | 2017-11-24 | 2018-02-16 | 黑龙江美丽石岛科技开发有限公司 | A kind of extraction process of sea cucumber intestine egg oil and the method that sea cucumber intestine ovum oil soft capsule is prepared using sea cucumber intestine egg oil |
| CN110236197A (en) * | 2019-05-15 | 2019-09-17 | 池州市月亮湾生物科技有限公司 | Sea cucumber intestine egg oil composition, sea cucumber intestine ovum oil soft capsule and preparation method thereof |
| CN111096457A (en) * | 2019-12-21 | 2020-05-05 | 池州市月亮湾生物科技有限公司 | Sea cucumber oil microcapsule powder and preparation method thereof |
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