CN101983585A - Buccal tablet of jujube alcohol extract and preparation method thereof - Google Patents

Buccal tablet of jujube alcohol extract and preparation method thereof Download PDF

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Publication number
CN101983585A
CN101983585A CN201010523318XA CN201010523318A CN101983585A CN 101983585 A CN101983585 A CN 101983585A CN 201010523318X A CN201010523318X A CN 201010523318XA CN 201010523318 A CN201010523318 A CN 201010523318A CN 101983585 A CN101983585 A CN 101983585A
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China
Prior art keywords
jujube
powder
leaching liquor
jujube powder
date
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Pending
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CN201010523318XA
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Chinese (zh)
Inventor
陈雪峰
蒋水星
张华�
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Shaanxi University of Science and Technology
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Shaanxi University of Science and Technology
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Priority to CN201010523318XA priority Critical patent/CN101983585A/en
Publication of CN101983585A publication Critical patent/CN101983585A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a buccal tablet of a jujube alcohol extract and a preparation method thereof. The preparation method comprises the following steps: cleaning jujubes, coring, drying, recooling, crushing, adding an ethanol solution to leach, and collecting the leaching solution; filtering or centrifuging to remove jujube slag in the leaching solution so as to obtain a concentrated solution; preparing the concentrated solution into jujube powder by a spray drying method or a freezing drying method; uniformly mixing the jujube powder with glucose powder, dextrin, starch, sucrose powder, mannitol, lactose or microcrystalline cellulose, jujube powder perfume, citric acid, malic acid or tartaric acid and edible pigment, granulating with a granulator, and drying to obtain jujube powder granules; and adding magnesium stearate or micropowder silica gel to the dried jujube granules, and tabletting with a tabletting machine. By preparing the jujube alcohol extract into the buccal tablet, the invention maintains the nourishing essence of the jujubes and has the characteristics of good mouthfeel, small volume, light weight, convenient carrying, convenient eating and the like.

Description

A kind of date alcohol extract buccal tablet and preparation method thereof
Technical field
The present invention relates to a kind of buccal tablet of sucking and chewing of being fit to, relate in particular to a kind of date alcohol extract buccal tablet and preparation method thereof.
Background technology
Date is the dry mature fruit of Rhamnaceae plant, is the natural health-care products of a kind of medicine-food two-purpose of extensive approval during people live, and not only has very high nutritive value, and very high medical value is also arranged simultaneously.The traditional Chinese medical science thinks that red date is used as medicine, and nature and flavor are sweet flat, nontoxic, to weakness of the spleen and the stomach, diarrhoea protracted dysentery, palpitation and severe palpitation, the deficiency of blood is sallow and disease such as cough due to deficiency of the lung, is the good medicine of nourishing qi and blood invigorating the spleen simply.The deep processed product of date has much at present, mainly contain products such as dried jujube, jujube paste, candied date, jujube powder, jujube milk and jujube wine, though these products have certain nutrient value, the functional component of date does not obtain enrichment, and be not easy to carry and eat, it is also not too convenient to store.Adopt alcohol extract technology processing date, gained date alcohol extract contains functional components such as flavone compound, rutin, polysaccharide, oleanolic acid and CAMP, concentrate the nutrition elite in the date, had various health care functions such as rehabilitation human body speed is fast, raising immunologic function, antifatigue, enhancing endurance, the U.S. face that nourishes blood, calmness, hypnosis, climacteric nursing.The date alcohol extract is processed into the buccal tablet product, makes it easy to easy for carrying and eatingly, meet easy, quick, the healthy consumption demand of modern.
Summary of the invention
The object of the present invention is to provide a kind ofly can make full use of distinctive nutrition of date and medical value, after the enrichment of date functional component, make a kind of being easy to carry, the date alcohol extract buccal tablet of instant edible.
For achieving the above object, the preparation method that the present invention adopts is:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 10~1: 25 mass ratio, and leaching liquor was collected in lixiviate in 2.5~3.5 hours under 55~65 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 20%~35% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the auxiliary material of 10~35% jujube powder and 62~85%, 1~4% jujube powdered flavor, citric acid, malic acid or tartaric acid and 0.1~1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
Said auxiliary material is the mixture of one or more arbitrary proportions in powdered glucose, dextrin, starch, cane sugar powder, sweet mellow wine, lactose or the microcrystalline cellulose;
6) dolomol or the superfine silica gel powder of adding jujube powder quality 1~2% in the jujube powder of oven dry are sent into the tablet press machine compressing tablet and are shaped.
The present invention makes the form of buccal tablet with the date alcohol extract, the various health care functions of existing date, have again that mouthfeel is good, volume is little, in light weight, be easy to carry, characteristics such as easy to use.Get a slice during use and directly put into containing of mouth or chew absorption, can be widely used in lying fallow, handle official business, travel, go out and family life in nutritional supplementation.
The specific embodiment
Embodiment 1:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 15 mass ratio, and leaching liquor was collected in lixiviate in 2.5 hours under 65 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 20% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 35% jujube powder and 62%, 2% jujube powdered flavor and 1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol of adding jujube powder quality 1% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
Embodiment 2:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 23 mass ratio, and leaching liquor was collected in lixiviate in 3 hours under 60 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 353% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the dextrin of 10% jujube powder and 40%, 45% starch, 1.5% citric acid, 2.5% malic acid and 1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) superfine silica gel powder of adding jujube powder quality 2% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
Embodiment 3:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 10 mass ratio, and leaching liquor was collected in lixiviate in 3.5 hours under 55 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 30% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the cane sugar powder of 20% jujube powder and 30%, 25% sweet mellow wine, 23% lactose, 1.9% tartaric acid and 0.1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol of adding jujube powder quality 1.5% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
Embodiment 4:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 20 mass ratio, and leaching liquor was collected in lixiviate in 3.5 hours under 58 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 28% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 30% jujube powder and 15%, 40% cane sugar powder, 11% microcrystalline cellulose, 3.5% jujube powdered flavor and 0.5% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) superfine silica gel powder of adding jujube powder quality 1.8% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
Embodiment 5:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 25 mass ratio, and leaching liquor was collected in lixiviate in 2.5 hours under 62 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 33% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 25% jujube powder and 72%, 2.2% jujube powdered flavor, citric acid, malic acid or tartaric acid and 0.8% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol or the superfine silica gel powder of adding jujube powder quality 1.3% in the jujube powder of oven dry are sent into the tablet press machine compressing tablet and are shaped.

Claims (7)

1. the preparation method of a date alcohol extract buccal tablet is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 10~1: 25 mass ratio, and leaching liquor was collected in lixiviate in 2.5~3.5 hours under 55~65 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 20%~35% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the auxiliary material of 10~35% jujube powder and 62~85%, 1~4% jujube powdered flavor, citric acid, malic acid or tartaric acid and 0.1~1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
Said auxiliary material is the mixture of one or more arbitrary proportions in powdered glucose, dextrin, starch, cane sugar powder, sweet mellow wine, lactose or the microcrystalline cellulose;
6) dolomol or the superfine silica gel powder of adding jujube powder quality 1~2% in the jujube powder of oven dry are sent into the tablet press machine compressing tablet and are shaped.
2. the preparation method of date alcohol extract buccal tablet according to claim 1 is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 15 mass ratio, and leaching liquor was collected in lixiviate in 2.5 hours under 65 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 20% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 35% jujube powder and 62%, 2% jujube powdered flavor and 1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol of adding jujube powder quality 1% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
3. the preparation method of date alcohol extract buccal tablet according to claim 1 is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 23 mass ratio, and leaching liquor was collected in lixiviate in 3 hours under 60 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 353% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the dextrin of 10% jujube powder and 40%, 45% starch, 1.5% citric acid, 2.5% malic acid and 1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) superfine silica gel powder of adding jujube powder quality 2% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
4. the preparation method of date alcohol extract buccal tablet according to claim 1 is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 10 mass ratio, and leaching liquor was collected in lixiviate in 3.5 hours under 55 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 30% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the cane sugar powder of 20% jujube powder and 30%, 25% sweet mellow wine, 23% lactose, 1.9% tartaric acid and 0.1% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol of adding jujube powder quality 1.5% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
5. the preparation method of date alcohol extract buccal tablet according to claim 1 is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 20 mass ratio, and leaching liquor was collected in lixiviate in 3.5 hours under 58 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 28% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 30% jujube powder and 15%, 40% cane sugar powder, 11% microcrystalline cellulose, 3.5% jujube powdered flavor and 0.5% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) superfine silica gel powder of adding jujube powder quality 1.8% in the jujube powder of oven dry is sent into the tablet press machine compressing tablet and is shaped.
6. the preparation method of date alcohol extract buccal tablet according to claim 1 is characterized in that:
1) at first date is cleaned stoning, cold pulverizing is returned in dry back under 70 ℃ of conditions, crosses 40~60 mesh sieves and collects the jujube meal;
2) being 60% ethanolic solution with jujube meal and volumetric concentration mixes by 1: 25 mass ratio, and leaching liquor was collected in lixiviate in 2.5 hours under 62 ℃ of insulations;
3) leaching liquor is filtered or the centrifugal jujube slag of removing, it is 33% that concentrated leaching liquor makes the solid content in the leaching liquor;
4) concentrate is made the jujube powder with spray drying process or freeze-drying;
5) food coloring of the powdered glucose of 25% jujube powder and 72%, 2.2% jujube powdered flavor, citric acid, malic acid or tartaric acid and 0.8% is mixed with comminutor granulation and oven dry obtain the jujube powder by mass percentage;
6) dolomol or the superfine silica gel powder of adding jujube powder quality 1.3% in the jujube powder of oven dry are sent into the tablet press machine compressing tablet and are shaped.
7. the date alcohol extract buccal tablet that makes according to the described preparation method of claim 1, it is characterized in that: date alcohol extract buccal tablet comprises jujube grain and dolomol or superfine silica gel powder, wherein the quality of dolomol or superfine silica gel powder accounts for 1~2% of jujube powder quality, contains jujube powder, 62~85% powdered glucose, dextrin, starch, cane sugar powder, sweet mellow wine, lactose or microcrystalline cellulose, 1~4% jujube powdered flavor, citric acid, malic acid or tartaric acid and 0.1~1% the food coloring of mass percent 10~35% in the jujube powder.
CN201010523318XA 2010-10-28 2010-10-28 Buccal tablet of jujube alcohol extract and preparation method thereof Pending CN101983585A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103251002A (en) * 2013-05-17 2013-08-21 邹桂怀 Water shield buccal tablet and preparation method thereof
CN106619734A (en) * 2016-12-15 2017-05-10 湖南中健欣元生物科技有限公司 Royal jelly pellet lozenge and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1435206A (en) * 2002-01-30 2003-08-13 贵州仙灵药业股份有限公司 Sedative jujube kernel capsule
CN1562097A (en) * 2004-03-17 2005-01-12 北京乾露春科技有限公司 Fructus choerospondiatis freeze-drying powder injection and its preparing method
CN1653951A (en) * 2005-03-09 2005-08-17 陕西科技大学 Chinese date buccal tablet and its preparing process
CN101475965A (en) * 2008-12-29 2009-07-08 刘明全 Method for preparing ethanol from Chinese date

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1435206A (en) * 2002-01-30 2003-08-13 贵州仙灵药业股份有限公司 Sedative jujube kernel capsule
CN1562097A (en) * 2004-03-17 2005-01-12 北京乾露春科技有限公司 Fructus choerospondiatis freeze-drying powder injection and its preparing method
CN1653951A (en) * 2005-03-09 2005-08-17 陕西科技大学 Chinese date buccal tablet and its preparing process
CN101475965A (en) * 2008-12-29 2009-07-08 刘明全 Method for preparing ethanol from Chinese date

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
《食品研究与开发》 20080229 胡春凤等 红枣皂甙提取工艺及定性分析 第29卷, 第02期 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103251002A (en) * 2013-05-17 2013-08-21 邹桂怀 Water shield buccal tablet and preparation method thereof
CN103251002B (en) * 2013-05-17 2014-06-04 邹桂怀 Water shield buccal tablet and preparation method thereof
CN106619734A (en) * 2016-12-15 2017-05-10 湖南中健欣元生物科技有限公司 Royal jelly pellet lozenge and preparation method thereof
CN106619734B (en) * 2016-12-15 2019-09-03 湖南中健欣元生物科技有限公司 A kind of royal jelly pellet lozenge and preparation method thereof

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Application publication date: 20110309