CN101974376B - Adhesive removing soft capsule by extracting limonene from orange peel and preparation method thereof - Google Patents
Adhesive removing soft capsule by extracting limonene from orange peel and preparation method thereof Download PDFInfo
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- CN101974376B CN101974376B CN 201010525359 CN201010525359A CN101974376B CN 101974376 B CN101974376 B CN 101974376B CN 201010525359 CN201010525359 CN 201010525359 CN 201010525359 A CN201010525359 A CN 201010525359A CN 101974376 B CN101974376 B CN 101974376B
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- soft capsule
- limonene
- glue
- orange peel
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Abstract
The invention relates to a preparation method of an adhesive removing soft capsule by extracting limonene from orange peel. The preparation method is characterized by comprising the following steps: limonene is extracted from orange peel, turpentine oil and the limonene are mixed into adhesive removing liquid which is added into a drug hopper of a soft capsule machine, the injection rate of the adhesive removing liquid is adjusted to be 1g, the soft capsule machine uses a soft capsule rotary die with the 1g volume of a die cavity, the gelatin liquid is pressed into soft capsule peel, the soft capsule machine carries out close fitting of the capsule peel while injecting the adhesive removing liquid, the semi-finished product of the adhesive removing soft capsule by extracting the limonene from the orange peel is pressed by one-time molding, by drying and sizing, the inner part of a drying rotary drum carries out capsule cleansing so as to obtain an adhesive removing soft capsule finished product by extracting the limonene from the orange peel, and each adhesive removing soft capsule by extracting the limonene from the orange peel contains 1g adhesive removing liquid. The invention is extremely convenient to carry, store and use, and can fast remove gum residue, dirty spots and insect spots adhered firmly when being coated on the surfaces of gum residue, dirty spot and insect spots. The invention has the characteristics of fast volatility, no residue after use, no toxic hazard to environments and human bodies and the like.
Description
Technical field
The present invention relates to a kind of orange peel and extract limonene except glue soft capsule and preparation method thereof, belong to daily necessities sanitising agent technical field.
Background technology
In daily life, the glue of chewing gum, non-setting adhesive stain and automobile case are difficult to remove near common washings such as the pitch spot near the lacquer limit wheel and the winged insect soma stains of automotive front.Especially on the smooth finish surface, as the non-setting adhesive stain on glass, ceramic tile, electric appliance casing surface.Stick on crude surface, as the more difficult removal of mouth balosam stain on the road surface, on the clothes, on the hair, or time-consuming tediously long.Common sanitising agent adds washing more difficult flush away usually.In addition, in the soft capsule production process, it is to wash ball with petroleum ether solvent that tradition is washed ball, and sherwood oil is inflammable, explosive, and production environment requires high, and producing has potential safety hazard when using.
Summary of the invention
The objective of the invention is to overcome above-mentioned weak point, thereby provide a kind of orange peel to extract limonene except glue soft capsule and preparation method thereof, should be except the glue soft capsule, it is all very convenient to carry, preserve, use.Puncture or cut off soft capsule and extrude in the soft capsule except glue and be applied to glue stain, spot, worm stain surface uses cloth to wipe with and wipes away, and can remove glue stain, spot, the worm stain of obstinate adhesion fast.
According to technical scheme provided by the invention, a kind of orange peel extracts limonene and comprises following component except the glue soft capsule:
Be that the orange peel of 60% or 95% limonene extracts limonene 80～100 weight parts, turps 5～20 weight parts mix except glue by mass percentage concentration;
Orange peel extracted to make after limonene, turps are mixed except glue be added in the spice bucket of encapsulating machine, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine carries out driving fit except in the glue to rubber in filling, once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process, rolling in drying typing, the drying drum and washing ball is that orange peel extracts limonene except glue soft capsule finished product, and each orange peel extracts limonene and contains 1g except glue except the glue soft capsule.
A kind of orange peel of the present invention extracts limonene except glue preparation of soft capsule method, adopts following preparation process:
1, the preparation of gelatin glue:
35 weight part glycerine, 100 parts of purified water are added reactor, be heated to 70 ℃, add water content≤14% dry gelatin, 100 weight parts and stir, 80～100 rev/mins of rotating speeds continue to be heated to 80～85 ℃, insulated and stirred 2 hours, vacuumizing and defoaming, vacuum tightness-0.06～-0.08MPa, be discharged to insulated tank, leave standstill 3.5 hours, standby;
2, preparation removes glue:
By mass percentage concentration be the orange peel of 60% or 95% limonene extract that limonene 80～100 weight parts, turps 5～20 weight parts mix except glue;
3, preparation soft capsule work in-process:
To be added in the spice bucket of encapsulating machine except glue, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine rubber roll temperature constant temperature is at 18 ℃～20 ℃, encapsulating machine carries out driving fit except in the glue to rubber in filling, and once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process continuously;
4, dryness finalization:
Orange peel is extracted limonene carry out dryness finalization except the whole ball workplace of glue soft capsule work in-process immigration;
The orange peel that is pressed into is extracted limonene pour air stream drying typing in the stainless steel rotating cage dryer drum into except glue soft capsule work in-process, gas flow temperature keeps 20 ℃～22 ℃, air stream drying is 1.8～2.2 hours in drying drum, take out stereotyped orange peel and extract limonene except the glue soft capsule, pave on the stainless steel pallet, between whole ball, placed seasoning again 7.5～8.5 hours;
The whole ball workplace isoperibol that must keep dry keeps 15～20 ℃ of envrionment temperatures, and relative humidity is below 40 ℃.
Envrionment temperature surpasses 25 ℃ the soft capsule adhesion easily takes place.
5, wash ball:
The orange peel of above-mentioned dryness finalization is extracted limonene under envrionment conditions between whole ball, roll in the stainless steel rotating cage dryer drum except the cotton block of glue soft capsule and dry cleansing joins and wash ball and namely get orange peel of the present invention after 30 minutes and extract limonene except the glue soft capsule, include the 1g peel of Citrus reticulata Blanco and extract the limonene adhesive remover.
Washing ball is to remove the solvent of soft capsule outside with cotton wiping in rolling process, and makes it light.
The present invention has the following advantages:
It is all very convenient that orange peel extraction limonene adhesive remover soft capsule of the present invention carries, preserves, uses.Puncture or cut off soft capsule and extrude in the soft capsule orange peel and extract the limonene adhesive remover and be applied to glue stain, spot, worm stain surface, use cloth to wipe with and wipe away, can remove glue stain, spot, the worm stain of obstinate adhesion fast, orange peel extracts limonene and turps has quick volatility, has the characteristics of effect with fresh air concurrently with back noresidue and citrus fragrance.
Orange peel extraction limonene and turps reality are nontoxic, to the toxicological harmless of human body environment.The soft capsule cot is that natural glutin is made, very easily degraded, environmentally safe.
Orange peel extracts limonene is that product is easily buied in market, obtains by supercritical extraction with orange peel, contains limonene 60% or 95% usually, and the two all can use in the present invention.In Guangdong, citrus such as Fujian, Zhejiang, area, the two lakes natural perfume factory that abounds with the district all can buy.The orange peel of import extracts lemon peel extraction limonene and contains limonene more than 95%.
Used turps is tasteless turps, and market is easily purchased.
Embodiment
Embodiment during following the present invention incites somebody to action by reference to the accompanying drawings is further described:
Embodiment one:
A kind of orange peel of the present invention extracts limonene except glue preparation of soft capsule method, adopts following preparation process:
1, the preparation of gelatin glue:
35 weight part glycerine, 100 parts of purified water are added reactor, be heated to 70 ℃, add water content≤14% dry gelatin, 100 weight parts and stir, 90 rev/mins of rotating speeds continue to be heated to 83 ℃, insulated and stirred 2 hours, vacuumizing and defoaming, vacuum tightness-0.07MPa is discharged to insulated tank, leave standstill 3.5 hours, standby;
2, preparation removes glue:
The orange peel that contains mass percentage concentration and be 60% limonene extract that limonene 100 weight parts, turps 5 weight parts are mixed and made into except glue;
3, preparation soft capsule work in-process:
To be added in the spice bucket of encapsulating machine except glue, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine rubber roll temperature constant temperature is at 18 ℃, encapsulating machine carries out driving fit except in the glue to rubber in filling, and once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process continuously;
4, dryness finalization:
Orange peel is extracted limonene carry out dryness finalization except the whole ball workplace of glue soft capsule work in-process immigration.
The orange peel that is pressed into is extracted limonene pour air stream drying typing in the stainless steel rotating cage dryer drum into except glue soft capsule work in-process, gas flow temperature keeps 20 ℃, air stream drying is 1.8 hours in drying drum, take out stereotyped orange peel and extract limonene except the glue soft capsule, pave on the stainless steel pallet, placed seasoning again 7.5 hours in whole ball workplace;
The whole ball workplace isoperibol that must keep dry keeps envrionment temperature 15, and relative humidity is below 40 ℃.
Envrionment temperature surpasses 25 ℃ the soft capsule adhesion easily takes place.
5, wash ball:
The orange peel of above-mentioned dryness finalization is extracted limonene under whole ball workplace envrionment conditions, roll in the stainless steel rotating cage dryer drum except the cotton block of glue soft capsule and dry cleansing joins and wash ball and namely get orange peel of the present invention after 30 minutes and extract limonene except the glue soft capsule, include 1g peel of Citrus reticulata Blanco extraction limonene adhesive remover.
Washing ball is to remove the solvent of soft capsule outside with cotton wiping in rolling process, and makes it light.
Encapsulating machine is the RJWJ-180 type encapsulating machine that friendship medicineization machinery company limited produces in the Wuxi City.
Stainless steel rotating cage drying machine is the RJWJ-ZL stainless steel rotating cage drying machine that friendship medicineization machinery company limited produces in the Wuxi City.
Orange peel of the present invention extracts limonene adhesive remover soft capsule, and it is all very convenient to carry, preserve, use.Cut off soft capsule during use and extrude in the soft capsule orange peel and extract limonene and be applied to glue stain surface, use cloth to wipe with and wipe away, can remove the glue stain of obstinate adhesion fast.
Embodiment two:
A kind of orange peel of the present invention extracts limonene except glue preparation of soft capsule method, adopts following preparation process:
1, the preparation of gelatin glue:
35 weight part glycerine, 100 parts of purified water are added reactor, be heated to 70 ℃, add water content≤14% dry gelatin, 100 weight parts and stir, 85 rev/mins of rotating speeds continue to be heated to 80 ℃, insulated and stirred 2 hours, vacuumizing and defoaming, vacuum tightness-0.08MPa is discharged to insulated tank, leave standstill 3.5 hours, standby;
2, preparation removes glue:
The orange peel that contains mass percentage concentration and be 95% limonene extract that limonene 80 weight parts, turps 20 weight parts mix except glue;
2, preparation soft capsule work in-process:
To be added in the spice bucket of encapsulating machine except glue, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine rubber roll temperature constant temperature is at 20 ℃, encapsulating machine carries out driving fit except in the glue to rubber in filling, and once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process continuously;
3, dryness finalization:
Orange peel is extracted limonene carry out dryness finalization except the whole ball workplace of glue soft capsule work in-process immigration.
The orange peel that is pressed into is extracted limonene pour air stream drying typing in the stainless steel rotating cage dryer drum into except glue soft capsule work in-process, gas flow temperature keeps 22 ℃, air stream drying is 2.2 hours in drying drum, take out stereotyped orange peel and extract limonene except the glue soft capsule, pave on the stainless steel pallet, placed seasoning again 8.5 hours in whole ball workplace;
The whole ball workplace isoperibol that must keep dry keeps 20 ℃ of envrionment temperatures, and relative humidity is below 40 ℃.
Envrionment temperature surpasses 25 ℃ the soft capsule adhesion easily takes place.
Encapsulating machine is the RJWJ-180 type encapsulating machine that friendship medicineization machinery company limited produces in the Wuxi City.
Stainless steel rotating cage drying machine is the RJWJ-ZL stainless steel rotating cage drying machine that friendship medicineization machinery company limited produces in the Wuxi City.
Orange peel of the present invention extracts limonene adhesive remover soft capsule, and it is all very convenient to carry, preserve, use.Cut off soft capsule during use and extrude in the soft capsule orange peel and extract limonene and be applied to glue stain surface, use cloth to wipe with and wipe away, can remove the glue stain of obstinate adhesion fast.
Embodiment three
A kind of orange peel of the present invention extracts limonene except glue preparation of soft capsule method, adopts following preparation process:
1, the preparation of gelatin glue:
35 weight part glycerine, 100 parts of purified water are added reactor, be heated to 70 ℃, add water content≤14% dry gelatin, 100 weight parts and stir, 100 rev/mins of rotating speeds continue to be heated to 85 ℃, insulated and stirred 2 hours, vacuumizing and defoaming, vacuum tightness-0.08MPa is discharged to insulated tank, leave standstill 3.5 hours, standby;
2, preparation removes glue:
The orange peel that contains mass percentage concentration and be 95% limonene extract that limonene 90 weight parts, turps 10 weight parts mix except glue;
2, preparation soft capsule work in-process:
To be added in the spice bucket of encapsulating machine except glue, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine rubber roll temperature constant temperature is at 19 ℃, encapsulating machine carries out driving fit except in the glue to rubber in filling, and once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process continuously;
3, dryness finalization:
Orange peel is extracted limonene carry out dryness finalization except the whole ball workplace of glue soft capsule work in-process immigration.
The orange peel that is pressed into is extracted limonene pour air stream drying typing in the stainless steel rotating cage dryer drum into except glue soft capsule work in-process, gas flow temperature keeps 21 ℃, air stream drying is 2.0 hours in drying drum, take out stereotyped orange peel and extract limonene except the glue soft capsule, pave on the stainless steel pallet, placed seasoning again 8 hours in whole ball workplace;
The whole ball workplace isoperibol that must keep dry keeps 21 ℃ of envrionment temperatures, and relative humidity is below 40 ℃.
Envrionment temperature surpasses 25 ℃ the soft capsule adhesion easily takes place.
Encapsulating machine is the RJWJ-180 type encapsulating machine that friendship medicineization machinery company limited produces in the Wuxi City.
Stainless steel rotating cage drying machine is the RJWJ-ZL stainless steel rotating cage drying machine that friendship medicineization machinery company limited produces in the Wuxi City.
Orange peel of the present invention extracts limonene adhesive remover soft capsule, and it is all very convenient to carry, preserve, use.Cut off soft capsule during use and extrude in the soft capsule orange peel and extract limonene and be applied to glue stain surface, use cloth to wipe with and wipe away, can remove the glue stain of obstinate adhesion fast.
Claims (1)
1. an orange peel extracts limonene except glue preparation of soft capsule method, it is characterized in that: adopt following preparation process:
(1), the preparation of gelatin glue:
35 weight part glycerine, 100 parts of purified water are added reactor, be heated to 70 ℃, add water content≤14% dry gelatin, 100 weight parts and stir, 80～100 rev/mins of mixing speed continue to be heated to 80～85 ℃, insulated and stirred 2 hours, vacuumizing and defoaming, vacuum tightness-0.06～-0.08MPa, be discharged to insulated tank, leave standstill 3.5 hours, standby;
(2), preparation removes glue:
Be that the orange peel of 60% or 95% limonene extracts limonene 80～100 weight parts, turps 5～20 weight parts are mixed into except glue by mass percentage concentration;
(3), preparation soft capsule work in-process:
To be added in the spice bucket of encapsulating machine except glue, the injection rate of regulating except glue is 1g, encapsulating machine uses the soft capsule revolving die of film chamber 1g capacity, the gelatin glue is pressed into the soft capsule skin, encapsulating machine rubber roll temperature constant temperature is at 18 ℃～20 ℃, encapsulating machine carries out driving fit except in the glue to rubber in filling, and once shaped is pressed into orange peel and extracts limonene except glue soft capsule work in-process continuously;
(4), dryness finalization:
Orange peel is extracted limonene carry out dryness finalization except the whole ball workplace of glue soft capsule work in-process immigration;
The orange peel that is pressed into is extracted limonene pour air stream drying typing in the stainless steel rotating cage dryer drum into except glue soft capsule work in-process, gas flow temperature keeps 20 ℃～22 ℃, air stream drying is 1.8～2.2 hours in drying drum, take out stereotyped orange peel and extract limonene except the glue soft capsule, pave on the stainless steel pallet, placed seasoning again 7.5～8.5 hours in whole ball workplace;
(5), wash ball:
The orange peel extraction limonene of above-mentioned dryness finalization is joined in the stainless steel rotating cage dryer drum except glue soft capsule and dry cotton block, and rolling is washed ball and is namely got orange peel extraction limonene after 30 minutes except the glue soft capsule under whole ball workplace envrionment conditions; Described orange peel extracts limonene and extracts the limonene adhesive remover except the glue soft capsule includes the 1g peel of Citrus reticulata Blanco;
The described whole ball workplace isoperibol that keeps dry, 15～20 ℃ of envrionment temperatures, relative humidity is below 40 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010525359 CN101974376B (en) | 2010-10-31 | 2010-10-31 | Adhesive removing soft capsule by extracting limonene from orange peel and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010525359 CN101974376B (en) | 2010-10-31 | 2010-10-31 | Adhesive removing soft capsule by extracting limonene from orange peel and preparation method thereof |
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| Publication Number | Publication Date |
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| CN101974376A CN101974376A (en) | 2011-02-16 |
| CN101974376B true CN101974376B (en) | 2013-07-03 |
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| CN106954858A (en) * | 2017-03-31 | 2017-07-18 | 广州市健鸣春生物科技有限公司 | A kind of preparation method with beautifying face and moistering lotion anti-aging, the natural VE formula added with rose oil, capsule and capsule |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1789398A (en) * | 2005-12-13 | 2006-06-21 | 张刚 | Natural plant type detergent |
| CN100395300C (en) * | 2005-12-13 | 2008-06-18 | 天津鎏虹科技发展有限公司 | Natural plant type oil paint and its preparation method |
| JP4589068B2 (en) * | 2004-09-28 | 2010-12-01 | アース製薬株式会社 | Insecticide dissolution promoter and heat transpiration insecticide |
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| JPH07292390A (en) * | 1994-04-28 | 1995-11-07 | Raku:Kk | Cleaning agent composition |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4589068B2 (en) * | 2004-09-28 | 2010-12-01 | アース製薬株式会社 | Insecticide dissolution promoter and heat transpiration insecticide |
| CN1789398A (en) * | 2005-12-13 | 2006-06-21 | 张刚 | Natural plant type detergent |
| CN100395300C (en) * | 2005-12-13 | 2008-06-18 | 天津鎏虹科技发展有限公司 | Natural plant type oil paint and its preparation method |
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