CN101967041A - Anti-reflection high-transmittance coated solar super-white embossed glass and manufacturing method thereof - Google Patents
Anti-reflection high-transmittance coated solar super-white embossed glass and manufacturing method thereof Download PDFInfo
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- CN101967041A CN101967041A CN201010201967.8A CN201010201967A CN101967041A CN 101967041 A CN101967041 A CN 101967041A CN 201010201967 A CN201010201967 A CN 201010201967A CN 101967041 A CN101967041 A CN 101967041A
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Abstract
The invention relates to anti-reflection high-transmittance coated solar super-white embossed glass and a manufacturing method thereof. The glass comprises a glass base layer and a coating layer. The manufacturing method comprises the following steps of: selection of raw materials, proportioning, mixing, melting, calendaring, annealing, sheet collection with specified size, deep processing of appearance, coating processing and toughening. The reflected rays of the glass are reduced; and the glass is treated by double-sided coating technology so as to improve the effective sunlight section transmittance of the glass and fulfill the purposes of controlling the crystalline silicon used by a photovoltaic assembly to be relative reduced and improving the power of a solar power generation assembly.
Description
Technical field
Use in the solar photovoltaic battery component involved in the present invention crystal silicon cell and non-crystalline silicon battery lead plate supporting energy ultrawhite figured glass, particularly a kind of antireflective high permeability coating solar energy ultrawhite figured glass and manufacture method thereof.
Background technology
Along with sun power utilizes cause and development of technology, because the crystalline silicon bonding film EVA that photovoltaic module uses, very easily generation is aging under ultraviolet radiation, falls to subtract cohesive force and light permeable rate, shortens its work-ing life.Because crystalline silicon output subtracts, cost an arm and a leg and restricting the development that sun power utilizes market to a great extent again.To subtract the many R﹠D institutions of cost and used non-crystalline silicon to replace crystalline silicon to be used as cell panel in order to fall, only need 1/3 cost input that better economic is promptly arranged as the carrier of photovoltaic cell.Just because of non-crystalline silicon very easily takes place to wear out, therefore the requirements at the higher level of ultraviolet blocking-up solar energy ultra-white configurated glass have been proposed under the influence of ultraviolet light.
In addition, the reflection of light of general energy ultrawhite figured glass by force 10%, the transmitance of effective sunlight is lower, therefore, influenced the power of solar electrical energy generation assembly.
Summary of the invention
The object of the present invention is to provide a kind of antireflective high permeability coating solar energy ultrawhite figured glass and manufacture method thereof, mainly solve existing technical problem in the above-mentioned prior art, thereby the reflection ray that makes glass falls and subtracts, glass is through the double-sided coating technical finesse, glass is improved the effective light section of sun transmitance, the crystalline silicon that reaches the use of control photovoltaic module reduces relatively, and the purpose that the solar electrical energy generation component power is improved.
For achieving the above object, the present invention is achieved in that
A kind of antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that it comprises glass-base and coatings; Wherein,
(1) weight percent of each component of composition glass-base is:
SiO
2 72.5-74.00％；
Al
2O
3 0.50-2.50％；
Fe
2O
3 0.006-0.01％；
CaO 8.00-11.00％；
MgO 0-4.00％；
R
2O 13.5-14.5％；
Sb
2O
3 0.10-0.40％；
CeO
2 0.02-0.4％；
(2) weight percent of each component of composition coatings is:
{ (CH
3)
2CHOH} (Virahol) 68-77%;
(H
2O) (deionized water) 5-7%;
(C
2H
6O
2) (ethylene glycol) 8-10%;
SiO
2(silicon-dioxide) 10-15%.
Described antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that the raw material that forms each component ratio of glass-base comprises:
| Sequence number | Title | Chemical Composition | Performance perameter |
| 1 | Smart quartz sand | SiO 2 | 〉=99.3% undulating quantity ± 0.2% |
| Fe 2O 3 | ≤0.001％ | ||
| 2 | Rhombspar | CaO | ≤30％ |
| Fe 2O 3 | ≤0.10％ | ||
| 3 | Wingdale | CaO | 〉=55.00% undulating quantity ± 0.02% |
| Fe 2O 3 | ≤ 0.01% undulating quantity ± 0.002% | ||
| 4 | Aluminium hydroxide | Al 2O 3 | ≥65.00％ |
| Fe 2O 3 | ≤0.019％ | ||
| 5 | Soda ash | Na 2CO 3 | ≥99.00％ |
| Fe 2O 3 | ≤ 0.004% water-insoluble≤0.04% | ||
| 6 | SODIUMNITRATE | NaNO 3 | ≥99.00％ |
| Fe 2O 3 | ≤0.004％ | ||
| 7 | Cerium | CeO 2 | ≥95.00％ |
Described antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that described coatings is located at the single or double of glass-base.
A kind of method of making aforesaid antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that it comprises the steps:
1. raw material selectes, prepares burden, mixes;
2. fusing;
3. calendering;
4. annealing;
5. scale takes up;
6. profile deep processing;
7. the coating process course of processing;
8. tempering.
The manufacture method of described antireflective high permeability coating solar energy ultrawhite figured glass, it is characterized in that: described step is melting in glass melter under 1600 degree high temperature in 2., adjust temperature control again at the 1200-1250 degree, make the overflow port metal level reach 80-110mm, temperature 1180-1200 degree enters the calendering operation.
The manufacture method of described antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that: described step 1. middle MgO, R
2O, CeO
2, Sb
2O
3By the accurate weighing of electronic scales, vibrations feeding machine feed is emitted in the weigh belt in the formulation material process, enters mixing machine with other load weighted materials of while and mixes, and after fully mixed, delivers into the outer storehouse of head material, cellar for storing things by conveyor.
Described step is to make the glass planar pattern precision in 3.; Control planeness tolerance; Control by the calender system operation realizes.
Described step is glass carries out the transition to normal temperature state procedure system under condition of high temperature situation control in 4., makes glass-board surface smooth; Cold cracking not; Control by the annealing furnace system operation realizes.
Described step is glass is implemented clean cut in the speed operational process is arranged operation in 5., controls by the system operation of the pulse plating membrane process course of processing and realizes.
Described step is that difference is required and the glass of shape is made in 6., controls by the operation of various glass deep-processing machine and realizes.
7. described step further comprises:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 68-77％；
(H
2O) 5-7％；
(C
2H
6O
2) 8-10％；
SiO
2 10-15％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution.
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method dynamically (0.5-0.7Mpa) while is robbed in the pressure spray to be coated with the covering plated film with many under (speed 25-45ml/min) condition, enter according to processing requirement then and carry out constant temperature under the temperature (250-350 degree) of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface at glass.Film hardness 6-7H after filming improves 2-2.5% in 380-1100nm wavelength region transmitance.
8. described step makes all solvent evaporates through the temperature (700-800 degree) that steel process in the annealing furnace sets, effectively SiO
2Be tightly adhered to glass surface through high temperature and have high hardness.Because SiO
2The specific refractory power of plated film and glass is close, interferes to reach the effect that reflection reduces when visible light incident.
6. described step can be omitted.
By technique scheme, the present invention has following technique effect:
1, the present invention is a kind of cerium dioxide CeO that adds in the solar energy ultra-white configurated glass composition of raw materials that the iron content utmost point subtracts
2Thereby, glass is subtracted to reach the purpose of control solar components decay the ultraviolet ray transmittance utmost point, the blocking-up rate reaches more than 36%.
2, compare with existing like product, product of the present invention contains Fe
2O
3More subtract, the sun power transmitance is higher, and the ultraviolet blocking-up of the photoelectric conversion rate of photovoltaic cell higher (seeing Fig. 1 transmittance curve) more heat-flash effect more subtracts.
3. used Sb among the present invention
2O
3As finings, made full use of its clarification mechanism, absorb O in the desuperheat stage of fusing
2, be converted into Sb
2O
3, emit O at the hot stage of fusing
2, the clarifying effect that reaches a high temperature, and the valence state of Fe in glass metal is converted into+3 valencys substantially, further improved the glass whiteness, increased the transmitance of sun power to greatest extent, the content that increases cerium in the prescription improves the blocking ability of base to ultraviolet spectrogram.
Description of drawings
Fig. 1 is the sun power transmittance curve figure of product of the present invention.
Embodiment
Embodiment 1:
A kind of antireflective high permeability coating solar energy ultrawhite figured glass, the weight percent composition of forming each component of glass-base is:
SiO
2 72.50％
Al
2O
3 2.50％
Fe
2O
3 0.01％
CaO 11.00％
R
2O 13.50％
Sb
2O
3 0.39％
CeO
2 0.10％
The forming process of coatings is as follows on the glass-base:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 68％；
(H
2O) 7％；
(C
2H
6O
2) 10％；
SiO
2 15％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution.
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method dynamically (0.5-0.7Mpa) while is robbed in the pressure spray to be coated with the covering plated film with many under (speed 25-45ml/min) condition, enter according to processing requirement then and carry out constant temperature under the temperature (250-350 degree) of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface at glass.Film hardness 6-7H after filming improves 2-2.5% in 380-1100nm wavelength region transmitance.
After tested, the present embodiment product reaches 40% to the blocking-up rate of ultraviolet spectrogram, and reflectivity is lower than 5%.
Embodiment 2:
A kind of antireflective high permeability coating solar energy ultrawhite figured glass, the weight percent composition of forming each component of glass-base is:
SiO
2 73.50％
Al
2O
3 0.50％
Fe
2O
3 0.006％
CaO 8.00％
MgO 4.00％
R
2O 13.50％
Sb
2O
3 0.10％
CeO
2 0.394％
The forming process of coatings is as follows on the glass-base:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 77％；
(H
2O) 5％；
(C
2H
6O
2) 8％；
SiO
2 10％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution.
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method dynamically (0.5-0.7Mpa) while is robbed in the pressure spray to be coated with the covering plated film with many under (speed 25-45ml/min) condition, enter according to processing requirement then and carry out constant temperature under the temperature (250-350 degree) of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface at glass.Film hardness 6-7H after filming improves 2-2.5% in 380-1100nm wavelength region transmitance.
After tested, the present embodiment product reaches 43% to the blocking-up rate of ultraviolet spectrogram, and reflectivity is lower than 5%.
Embodiment 3:
A kind of antireflective high permeability coating solar energy ultrawhite figured glass, the weight percent composition of forming each component of glass-base is:
SiO
2 74.00％
Al
2O
3 0.50％
Fe
2O
3 0.006％
CaO 10.194％
R
2O 14.50％
Sb
2O
3 0.40％
CeO
2 0.40％
The forming process of coatings is as follows on the glass-base:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 70％；
(H
2O) 6％；
(C
2H
6O
2) 9％；
SiO
2 15％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution.
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method dynamically (0.5-0.7Mpa) while is robbed in the pressure spray to be coated with the covering plated film with many under (speed 25-45ml/min) condition, enter according to processing requirement then and carry out constant temperature under the temperature (250-350 degree) of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface at glass.Film hardness 6-7H after filming improves 2-2.5% in 380-1100nm wavelength region transmitance.
After tested, the present embodiment product reaches 44% to the blocking-up rate of ultraviolet spectrogram, and reflectivity is lower than 5%.
Embodiment 4:
A kind of antireflective high permeability coating solar energy ultrawhite figured glass, the weight percent composition of forming each component of glass-base is:
SiO
2 72.57％
Al
2O
3 2.50％
Fe
2O
3 0.01％
CaO 11.00％
R
2O 13.50％
Sb
2O
3 0.40％
CeO
2 0.02％
The forming process of coatings is as follows on the glass-base:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 75％；
(H
2O) 5％；
(C
2H
6O
2) 10％；
SiO
2 10％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution.
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method dynamically (0.5-0.7Mpa) while is robbed in the pressure spray to be coated with the covering plated film with many under (speed 25-45ml/min) condition, enter according to processing requirement then and carry out constant temperature under the temperature (250-350 degree) of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface at glass.Film hardness 6-7H after filming improves 2-2.5% in 380-1100nm wavelength region transmitance.
After tested, the present embodiment product reaches 36% to the blocking-up rate of ultraviolet spectrogram, and reflectivity is lower than 5%.
Being preferred embodiment of the present invention only in sum, is not to be used for limiting practical range of the present invention.Be that all equivalences of doing according to the content of the present patent application claim change and modification, all should be technology category of the present invention.
Claims (9)
1. an antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that it comprises glass-base and coatings; Wherein,
(1) weight percent of each component of composition glass-base is:
SiO
2 72.5-74.00％；
Al
2O
3 0.50-2.50％；
Fe
2O
3 0.006-0.01％；
CaO 8.00-11.00％；
MgO 0-4.00％；
R
2O 13.5-14.5％；
Sb
2O
3 0.10-0.40％；
CeO
2 0.02-0.4％；
(2) weight percent of each component of composition coatings is:
{(CH
3)
2CHOH} 68-77％；
(H
2O) 5-7％；
(C
2H
6O
2) 8-10％；
SiO
2 10-15％。
2. antireflective high permeability coating solar energy ultrawhite figured glass according to claim 1 is characterized in that the raw material that forms each component ratio of glass-base comprises:
3. antireflective high permeability coating solar energy ultrawhite figured glass according to claim 1 and 2 is characterized in that described coatings is located at the single or double of glass-base.
4. the method for a manufacturing such as claim 1 or 2 or 3 described antireflective high permeability coating solar energy ultrawhite figured glass is characterized in that it comprises the steps:
1. raw material selectes, prepares burden, mixes;
2. fusing;
3. calendering;
4. annealing;
5. scale takes up;
6. profile deep processing;
7. the coating process course of processing;
8. tempering.
5. the manufacture method of antireflective high permeability coating solar energy ultrawhite figured glass according to claim 4, it is characterized in that: described step is melting in glass melter under 1600 degree high temperature in 2., adjust temperature control again at the 1200-1250 degree, make the overflow port metal level reach 80-110mm, temperature 1180-1200 degree enters the calendering operation.
6. the manufacture method of antireflective high permeability coating solar energy ultrawhite figured glass according to claim 4 is characterized in that: described step 1. middle MgO, R
2O, CeO
2, Sb
2O
3By the accurate weighing of electronic scales, vibrations feeding machine feed is emitted in the weigh belt in the formulation material process, enters mixing machine with other load weighted materials of while and mixes, and after fully mixed, delivers into the outer storehouse of head material, cellar for storing things by conveyor.
7. the manufacture method of antireflective high permeability coating solar energy ultrawhite figured glass according to claim 4, it is characterized in that: 7. described step further comprises:
(1) preparation of plated film nano material;
The weight percent of forming each component of coatings is:
{(CH
3)
2CHOH} 68-77％；
(H
2O) 5-7％；
(C
2H
6O
2) 8-10％；
SiO
2 10-15％
Use SiO
2As precursor, needing to obtain the porous nanometer material SiO of existence through the temperature-time control reduction reaction cooling for reflux speed of pure reduction process
2After obtaining colloid,, be configured to a kind of nano material of proportion 0.82g/ml, viscosity 2.6cps, particle diameter 30-40nm again with the alcohol dilution;
(2) coating operation;
The original sheet glass of deep processing will be finished, adopt spraying method under glass dynamic speed 25-45ml/min condition, the 0.5-0.7Mpa while is robbed in the pressure spray to be coated with the covering plated film, enter according to processing requirement then and carry out constant temperature under the temperature 250-350 degree of setting and the time 2.8-2.6min condition and bake and bank up with earth from the trend glass surface with many.
8. the manufacture method of antireflective high permeability coating solar energy ultrawhite figured glass according to claim 7 is characterized in that: 8. described step makes all solvent evaporates through the temperature 700-800 degree degree that steel process in the annealing furnace sets.
9. the manufacture method of antireflective high permeability coating solar energy ultrawhite figured glass according to claim 4, it is characterized in that: 6. described step can be omitted.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010201967.8A CN101967041B (en) | 2009-06-08 | 2010-06-02 | Anti-reflection high-transmittance coated solar super-white embossed glass and manufacturing method thereof |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNPCT/CN2009/000632 | 2009-06-08 | ||
| PCT/CN2009/000632 WO2010142056A2 (en) | 2009-06-08 | 2009-06-08 | Low reflectivity high transmissivity solar energy ultra-white configurated glass with coating and method for manufacturing the same |
| CN201010201967.8A CN101967041B (en) | 2009-06-08 | 2010-06-02 | Anti-reflection high-transmittance coated solar super-white embossed glass and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101967041A true CN101967041A (en) | 2011-02-09 |
| CN101967041B CN101967041B (en) | 2013-02-13 |
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| CN102285765A (en) * | 2011-06-07 | 2011-12-21 | 福莱特光伏玻璃集团股份有限公司 | Online coating system of solar ultrawhite patterned glass |
| CN102531406A (en) * | 2012-01-17 | 2012-07-04 | 信义玻璃工程（东莞）有限公司 | Antireflective coating solution and preparation method thereof, as well as photovoltaic glass and preparation method of photovoltaic glass |
| CN103258887A (en) * | 2013-04-28 | 2013-08-21 | 王博 | Super-white embossed glass |
| CN103508669A (en) * | 2013-05-14 | 2014-01-15 | 河源旗滨硅业有限公司 | Ultraviolet-resistant solar photovoltaic glass and applications thereof |
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Cited By (16)
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|---|---|---|---|---|
| CN102285765A (en) * | 2011-06-07 | 2011-12-21 | 福莱特光伏玻璃集团股份有限公司 | Online coating system of solar ultrawhite patterned glass |
| CN104024172A (en) * | 2011-10-24 | 2014-09-03 | 中央硝子株式会社 | Solar cell cover glass and method for producing same |
| CN102531406A (en) * | 2012-01-17 | 2012-07-04 | 信义玻璃工程（东莞）有限公司 | Antireflective coating solution and preparation method thereof, as well as photovoltaic glass and preparation method of photovoltaic glass |
| CN102531406B (en) * | 2012-01-17 | 2015-03-25 | 信义玻璃工程（东莞）有限公司 | Antireflective coating solution and preparation method thereof, as well as photovoltaic glass and preparation method of photovoltaic glass |
| CN103258887B (en) * | 2013-04-28 | 2016-08-17 | 中航三鑫太阳能光电玻璃有限公司 | A kind of energy ultrawhite figured glass |
| CN103258887A (en) * | 2013-04-28 | 2013-08-21 | 王博 | Super-white embossed glass |
| CN103508669A (en) * | 2013-05-14 | 2014-01-15 | 河源旗滨硅业有限公司 | Ultraviolet-resistant solar photovoltaic glass and applications thereof |
| CN103508669B (en) * | 2013-05-14 | 2015-10-28 | 河源旗滨硅业有限公司 | A kind of uvioresistant ultra-white photovoltaic glass and application thereof |
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Application publication date: 20110209 Assignee: Fulaite PV Glass Group Co., Ltd. Assignor: Shanghai Flat Glass Co., Ltd. Contract record no.: 2014330000298 Denomination of invention: Anti-reflection high-transmittance coated solar super-white embossed glass and manufacturing method thereof Granted publication date: 20130213 License type: Common License Record date: 20140724 |
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Effective date of registration: 20160509 Address after: 314001 No. 1999 Canal Road, Xiuzhou District, Zhejiang, Jiaxing Patentee after: Follett, Mary Parker glass Group Plc Address before: 201802 No. 59 Ting Road, Anting Dazhong Industrial Park, Shanghai, China Patentee before: Shanghai Flat Glass Co., Ltd. |