CN101945579A - 特特拉姆酸衍生物用于树干、分枝、花序或蓓蕾处理之后防治动物有害物的用途 - Google Patents
特特拉姆酸衍生物用于树干、分枝、花序或蓓蕾处理之后防治动物有害物的用途 Download PDFInfo
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Classifications
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
- A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pretreatment Of Seeds And Plants (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
本发明涉及式(I)或(II)的特特拉姆酸衍生物用于树干处理(喷雾、涂抹、注射、涂布)，分枝、茎、芽和幼枝处理(涂抹、喷雾、涂布)和通过注射对花序或蓓蕾处理之后防治动物有害物的用途。
Description
本发明涉及特特拉姆酸(tetramic acid)衍生物用于树干处理(stem treatment)(喷雾、涂抹、注射、涂布)，分枝、茎、芽和幼枝处理(涂抹、喷雾、涂布)和通过注射进行花序处理和蓓蕾处理之后防治动物有害物(animal pest)的用途。
具有杀虫和/或杀螨活性的特特拉姆酸衍生物(WO 98/05638)及其顺式异构体(WO 04/007448)是已知的。
特特拉姆酸衍生物用于在浇注、滴流或土壤注射之后抵抗蛛螨和昆虫(WO 07/126691)及在叶面施用之后抵抗线虫(美国申请号61/008507)的用途，以及在浇灌施用之后防治植物病害(EP申请号07150293)的用途，也是已知的。
其他用途在WO 2007/131681中有描述。
令人惊讶的是，现已发现式(I)或(II)的化合物
还很适于在树干处理(例如通过涂抹、喷雾、涂布、注射)之后，茎、分枝、幼枝和芽处理(例如通过涂抹、喷雾、涂布)之后，和注射到花蕾及花序中(在本领域中称为蓓蕾注射)之后，防治昆虫和蛛螨。
相应地，本发明涉及特特拉姆酸衍生物用于在开放或封闭系统(例如温室或在薄片覆盖物下)中在一年生作物(例如观赏植物)和在多年生作物(例如热带水果、柑橘类、松柏类、梨果、核果、啤酒花)中在树干施用、分枝施用、茎施用、幼枝施用和芽施用以及花序和花蕾处理之后防治昆虫和蛛螨的用途。
对仅以宽泛术语描述的待保护作物在下文进行区分并以更详细的方式进行说明。
例如，在多年生作物中的用途应理解为意指柑橘类，例如橙、葡萄柚、橘、柠檬、莱檬、酸橙(Seville orange)、金橘、小蜜柑；
以及梨果，例如苹果、梨和榅桲，和核果，例如桃、蜜桃、樱桃、李子、凯秋李子(quetsch)、杏；
以及葡萄藤、啤酒花、橄榄、茶树，及热带作物，例如芒果、番木瓜、无花果、菠萝、海枣、香蕉、榴莲、柿子(kaki fruit)、椰子、可可、咖啡、鳄梨、荔枝、百香果(maracuja)、番石榴、油椰；
以及扁桃和坚果，例如榛子、核桃、阿月浑子、槚如树坚果、巴西坚果、美洲山核桃、灰核桃、栗子、山核桃坚果、澳洲坚果、花生，
此外，还有浆果，例如茶藨子(currant)、醋栗(gooseberry)、悬钩子、黑莓、蓝莓、草莓、酸果蔓、猕猴桃、美洲酸果蔓。
就用途而言，观赏植物的含义应理解为一年生及多年生植物，例如切花，如玫瑰、康乃馨、非洲菊、百合、雏菊(margarite)、菊花、郁金香、水仙花、银莲花、罂粟、孤挺花、大丽花、杜鹃花、木槿，
以及例如庭院植物(border plant)、盆栽植物和多年生植物例如玫瑰、万寿菊、堇菜、天竺葵、倒挂金钟、木槿、菊花、凤仙花、仙客来、非洲堇、向日葵、秋海棠，
以及例如灌木和松柏类，例如无花果(ficus)、杜鹃花、冷杉、云杉、松树、紫杉、日本金松、夹竹桃。
蓟马科(Thripidae)中优选的有：作物例如浆果、观赏植物、马铃薯、热带作物、葡萄藤、坚果、柑橘类、茶树中的花蓟马属(Frankliniella spp.)、蓟马属(Thrips spp.)、网蓟马属(Heliothrips spp.)、褐带蓟马属(Hercinothrips spp.)、巢蓟马属(Caliothrips spp.)、硬蓟马属(Scirthothrips spp.)。
粉蚧科(Pseudococcidae)中优选的有：作物例如柑橘类、核果类和梨果类、茶树、葡萄藤、观赏植物和热带作物中的Pericerga、粉蚧属(Pseudococcus spp.)、臀纹粉蚧属(Planococcus spp.)、灰粉蚧属(Dysmicoccus spp.)。
蚧科(Coccidae)中优选的有：多年生作物例如柑橘类、梨果、核果、橄榄、葡萄藤、咖啡、茶树、热带作物、观赏植物中的蜡蚧属(Ceroplastes spp.)、履棉蚧属(Drosicha spp.)、棉蚧属(Pulvinaria spp.)、Protopulminaria spp.、黑盔蚧属(Saissetia spp.)、软蚧属(Coccus spp.)。
盾蚧科(Diaspididae)中优选的有：作物例如柑橘类、梨果、核果、扁桃、坚果、橄榄、茶树、观赏植物、葡萄藤、热带作物中的笠圆盾蚧属(Quadraspidiotus spp.)、肾圆盾蚧属(Aonidiella spp.)、蛎盾蚧属(Lepidosaphes spp.)、圆盾蚧属(Aspidiotus spp.)、片盾蚧属(Parlatoria spp.)、白盾蚧属(Pseudaulacaspis spp.)、尖盾蚧属(Unaspis spp.)、并盾蚧属(Pinnaspis spp.)、刺圆盾蚧属(Selenaspidus spp.)。
所有植物及植物部位均可依据本发明处理。在本发明的上下文中，植物的含义应理解为所有植物及植物种群，例如需要的及不需要的野生植物或作物植物(包括天然存在的作物植物)。作物植物可为可通过常规育种和优选法或通过生物技术和重组方法或通过前述方法的结合而获得的植物，包括转基因植物并包括可受植物育种者权益(Plant Breeders’Right)保护或不受其保护的植物变种。植物部位的含义应理解为植物所有的地上及地下部位及植物器官，例如芽、叶、花和根，可提及的实例有叶、针叶、茎、树干、花、子实体、果实和种子，以及根、块茎和根茎。植物部位还包括采收物，及无性与有性繁殖物，例如插枝、块茎、根茎、压枝和种子。
依据本发明用活性物质对植物及植物部位的处理，使用常规处理方法直接进行或者通过作用于其环境、生境或贮存空间而进行，所述常规处理方法例如浸渍、喷雾、蒸发、雾化、撒播、涂抹、注射，并且，对于繁殖物，尤其是对于种子，还可涂以一层或多层包衣。
如上所提及，所有植物及其部位均可依据本发明处理。在一个优选的实施方案中，处理野外中存在的或者通过常规生物育种法(例如杂交或原生质体融合)而获得的植物品种及植物变种，及这些品种和变种的部位。在另一个优选的实施方案中，处理通过重组方法——如果合适与常规方法结合——而获得的转基因植物和植物变种(基因修饰生物)及它们的部位。术语“部位”、“植物的部位”或“植物部位”描述如上。
尤其优选依据本发明处理的植物为各自市售或正在使用的植物变种的植株。植物变种的含义理解为通过常规育种、诱变或重组DNA技术而培育的具有新特征的植物。它们可为变种、生物型或基因型的形式。
依据植物品种或植物变种、其种植地点和生长条件(土壤、气候、生长期、营养)，本发明的处理也可产生超加和(“协同”)效应。超过实际预期效果的效果有，例如降低可依据本发明使用的物质和组合物的施用率和/或加宽其活性谱和/或提高其活性、改善植物生长状况、提高高温或低温耐受性、提高对干旱或对水或土壤含盐量的耐受性、提高开花品质、使采收更便利、加速成熟、提高产率、提高作物产品的品质和/或提高其营养价值、改善作物产品的可贮性和/或其加工性能。
待依据本发明处理的优选的转基因植物或植物变种(通过遗传工程获得的植物或植物变种)包括通过重组修饰接受了遗传物质的所有植物，所述遗传物质赋予所述植物特别有利的有价值特征。所述特征的实例有改善植物生长、提高高温或低温耐受性、提高对干旱或对水或土壤含盐量的耐受性、提高开花品质、使采收更便利、加速成熟、提高产率、提高作物产品的品质和/或提高其营养价值、改善作物产品的可贮性和/或其加工性能。特别强调的所述特征的其他实例有改善植物对动物和微生物有害物的抵抗力，例如对昆虫、螨虫、植物致病真菌、细菌和/或病毒的抵抗力，以及提高植物对特定除草活性化合物的耐受性。特别强调的转基因植物的实例有重要的作物植物，例如谷物(小麦、稻)、玉米、大豆、马铃薯、棉花、烟草、油菜及果实植物(果实为苹果、梨、柑橘类水果及葡萄)，特别强调的是玉米、大豆、马铃薯、棉花、烟草和油菜。特别强调的特征为由在植物体内形成的毒素，特别是由苏云金芽孢杆菌(Bacillus thuringiensis)的遗传物质(例如基因Cry ⅠA(a)、Cry ⅠA(b)、Cry ⅠA(c)、CryⅡA、CryⅢA、CryⅢB2、Cry9c、Cry2Ab、Cry3Bb和Cry ⅠF及其结合)在植物体内产生的毒素，提高植物对昆虫、蛛形纲动物、线虫和蛞蝓以及蜗牛的抵抗力(以下简称为“Bt植物”)。还特别强调的特征为通过系统获得性抗性(SAR)、系统素、植物抗毒素、引发物(elicitor)和抗性基因以及相应的表达蛋白质和毒素来提高植物对真菌、细菌和病毒的抵抗力。此外尤其强调的特征为提高植物对特定除草活性化合物的耐受性，例如对咪唑啉酮类、磺酰脲类、草甘膦(glyphosate)或草丁膦(phosphinothricin)的耐受性(例如“PAT”基因)。赋予所述所需特征的特定基因也可在转基因植物体内相互结合而存在。可提及的“Bt植物”的实例有市售的商品名称为YIELD GARD
(例如玉米、棉花、大豆)、KnockOut
(例如玉米)、StarLink
(例如玉米)、Bollgard
(棉花)、Nucotn
(棉花)和NewLeaf
(马铃薯)的玉米变种、棉花变种、大豆变种和马铃薯变种。可提及的除草剂耐受性植物的实例有市售的商品名称为Roundup Ready
(具有草甘膦耐受性，例如玉米、棉花、大豆)、Liberty Link
(具有草丁膦耐受性，例如油菜)、IMI(具有咪唑啉酮耐受性)和STS
(具有磺酰脲耐受性，例如玉米)的玉米变种、棉花变种和大豆变种。还可提及的具有除草剂抗性的植物(以常规的除草剂耐受性方式育种)有名称为Clearfield
(例如玉米)的市售变种。当然，所述内容也适用于将在未来进行开发或上市的植物变种，所述植物变种具有所述基因特征或未来待开发的特征。
式(I)和(II)的活性化合物可转化为常规制剂，例如溶液剂、乳剂、可湿性粉剂、悬浮剂、粉剂、粉末剂、膏剂、可溶性粉剂、颗粒剂、悬乳浓缩剂、经活性化合物浸渍的天然及合成材料，及聚合材料中的超细微胶囊剂。
这些制剂以已知方式制备，例如通过将活性化合物与填充剂混合，即，与液体溶剂和/或固体载体混合，任选地使用表面活性剂，即乳化剂和/或分散剂和/或发泡剂。
在用水作填充剂的情况下，还可使用例如有机溶剂作为助溶剂。适宜的液体溶剂主要有：芳族化合物，例如二甲苯、甲苯或烷基萘；氯代芳族化合物和氯代脂族烃，例如氯苯、氯乙烯或二氯甲烷；脂族烃，例如环己烷或石蜡，如矿物油馏分、矿物油和植物油；醇，例如丁醇或乙二醇，及其醚和酯；酮，例如丙酮、甲基乙基酮、甲基异丁基酮或环己酮；强极性溶剂，例如二甲基甲酰胺和二甲亚砜；以及水。
适宜的固体载体有：
例如铵盐，和粉碎的天然矿物如高岭土、粘土、滑石、白垩、石英、凹凸棒石、蒙脱石或硅藻土，及粉碎的合成矿物如细分散的二氧化硅、氧化铝和硅酸盐；适宜的颗粒剂固体载体有：例如粉碎并分级的天然岩石，例如方解石、大理石、浮石、海泡石和白云石；及合成的无机及有机粉颗粒；及有机物颗粒，例如锯屑、椰壳、玉米穗轴和烟草茎；适宜的乳化剂和/或发泡剂有：例如非离子及阴离子乳化剂，例如聚氧乙烯脂肪酸酯、聚氧乙烯脂肪醇醚，如烷基芳基聚乙二醇醚，烷基磺酸盐、烷基硫酸盐、芳基磺酸盐，以及蛋白质水解产物；适宜的分散剂有：例如木素亚硫酸盐废液及甲基纤维素。
制剂中可使用粘合剂，例如羧甲基纤维素，以及粉末、颗粒或胶乳形式的天然及合成聚合物，例如阿拉伯树胶、聚乙烯醇和聚乙酸乙烯酯，及天然磷脂，例如脑磷脂和卵磷脂，及合成磷脂。其他添加剂可为矿物油和植物油。
可以使用着色剂，例如无机颜料，如氧化铁、二氧化钛及普鲁士蓝，以及有机染料，例如茜素染料、偶氮染料及金属酞菁染料，以及微量营养物，例如铁盐、锰盐、硼盐、铜盐、钴盐、钼盐及锌盐。
制剂通常含有0.1-95重量％、优选0.5-90％的活性化合物，并另外优选含有填充剂和/或表面活性剂。
由市售制剂制备的使用形式的活性化合物含量可在较宽范围内变化。使用形式的活性化合物浓度可在0.0000001至最高95重量％活性化合物的范围内，优选0.0001-1重量％。
以适合于使用形式的常规方式施用。
用途实施例
蓟马科
极尤其优选的是在以下作物中进行花序和蓓蕾处理之后对以下蓟马科物种进行防治：
粉蚧科
极尤其优选的是在以下作物中进行树干处理之后对以下粉蚧科物种进行防治：
蚧科
极尤其优选的是在以下作物中——优选进行树干施用之后——对以下蚧科物种进行防治：
盾蚧科
极尤其优选的是在以下作物中——优选进行树干施用之后——对以下盾蚧科物种进行防治：
实施例1
对香蕉树栽培种“Cavendish”进行三个重复处理以抵抗黄胸蓟马(Thrips hawaiiensis)。此处，对活性物质实例(II)(100OD)与市售标准品吡虫啉(imidacloprid)(100SL)相比较在指定的施用率下进行试验。所述施用通过将各80ml注射溶液注射到花蕾中而进行。在每种情况下，对三朵花蕾进行处理。在处理之后第3天和第91天通过评估对花序和花束上种群受到的破坏而进行评价。
实施例2
对由亲本植物和吸根(sucker)构成的香蕉树(生长阶段BBCH 1130)栽培种“Cavendish”在叶面处理之后通过假茎施用进行三个重复处理以抵抗椰圆盾蚧(Aspidiotus destructor)和抵抗菠萝灰粉蚧(Dysmicoccus brevipes)。为此，各施用100ml喷雾溶液，分别向叶上喷雾50ml和向树干上喷雾50ml。在对树干施用之前，首先剥去最外面的树干层，这是惯例。此处，将活性物质(II)(SC 240)在桶混物中与0.025％的Hoestick(XL 500)一起进行试验，并与市售标准品甲基毒死蜱(chlorpyrifos-methyl)(500EC)和液体石蜡(Banole oil)(EC 600)进行比较。
在处理之后第3、7、14和22天通过评估树干上所述菠萝粉蚧受到的破坏而进行评价。
| Banole oil | 30 | 87.9 | 91.7 | 89.0 | 96.5 |
| 甲基毒死蜱 | 0.8 | 98.9 | 99.3 | 100.0 | 100.0 |
| 实例(II) | 0.3 | 81.2 | 92.3 | 96.4 | 96.7 |
实施例3
将约5年大的幼小橙树栽培种“Valencia”在通过涂抹活性物质进行树干施用之后进行三个重复处理以抵抗红肾圆盾蚧(Aonidiella aurantii)。此处，对活性物质(II)(SC 240)与市售标准品吡虫啉相比较在详述的施用率下进行试验。在处理之后第205天通过评估对该果树的侵染而进行评价。
Claims (8)
1.式(I)或(II)的化合物
用于在树干处理，茎、分枝、幼枝和芽处理，及注射到花蕾和花序中之后防治昆虫和蛛螨的用途。
2.权利要求1要求保护的式(I)或(II)的化合物用于花序处理之后防治蓟马的用途。
3.权利要求1要求保护的式(I)或(II)的化合物用于蓓蕾处理之后防治蓟马的用途。
4.权利要求1要求保护的式(I)或(II)的化合物用于树干处理之后防治粉蚧科(Pseudococcidae)的用途。
5.权利要求1要求保护的式(I)或(II)的化合物用于树干处理之后防治蚧科(Cococcidae)的用途。
6.权利要求1要求保护的式(I)或(II)的化合物用于树干处理之后防治盾蚧科(Diaspididae)的用途。
7.权利要求1-6要求保护的式(I)化合物的用途。
8.权利要求1-6要求保护的式(I)化合物的用途。
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| EP08151372.3 | 2008-02-13 | ||
| EP08151372A EP2090167A1 (de) | 2008-02-13 | 2008-02-13 | Verwendung von Tetramsäurederivaten zur Bekämpfung von tierischen Schädlingen nach Stamm-, Zweig-, Blütenstand- und Knospenbehandlungen |
| PCT/EP2009/000816 WO2009100851A1 (de) | 2008-02-13 | 2009-02-06 | Verwendung von tetramsäurederivaten zur bekämpfung von tierischen schädlingen nach stamm-, zweig-, blütenstand- und knospenbehandlungen |
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| EP (2) | EP2090167A1 (zh) |
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| EP2071952A1 (de) * | 2007-12-21 | 2009-06-24 | Bayer CropScience AG | Verwendung von Tetramsäurederivaten zur Bekämpfung von Schaderregern durch Angiessen oder Tröpfchenapplikation |
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| WO2007112845A1 (de) * | 2006-03-29 | 2007-10-11 | Bayer Cropscience Ag | Wirkstoffkombinationen mit insektiziden und akariziden eigenschaften |
| WO2007126691A2 (en) * | 2006-03-28 | 2007-11-08 | Bayer Cropscience Ag | Use of tetramic acid derivatives for controlling pests by drenching, drip application, dip application or soil injection |
| WO2007131681A2 (de) * | 2006-05-12 | 2007-11-22 | Bayer Cropscience Ag | Verwendung von tetramsäurederivaten zur bekämpfung von insekten |
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| DE10024934A1 (de) * | 2000-05-19 | 2001-11-22 | Bayer Ag | Wirkstoffkombinationen mit insektiziden akariziden Eigenschaften |
| DE10231333A1 (de) | 2002-07-11 | 2004-01-22 | Bayer Cropscience Ag | Cis-Alkoxysubstituierte spirocyclische 1-H-Pyrrolidin-2,4-dion-Derivate |
| DE102005003076A1 (de) * | 2005-01-22 | 2006-07-27 | Bayer Cropscience Ag | Verwendung von Tetramsäurederivaten zur Bekämpfung von Insekten aus der Gattung der Pflanzenläuse (Sternorrhyncha) |
| DE102005044826A1 (de) * | 2005-09-20 | 2007-03-29 | Bayer Cropscience Ag | Nikotinyle, Pyrethroide und Ketoenole als Gel- oder Schaumformulierung für mehrjährige Kulturen |
| DE102006033154A1 (de) * | 2006-07-18 | 2008-01-24 | Bayer Cropscience Ag | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
| DE102007009957A1 (de) * | 2006-12-27 | 2008-07-03 | Bayer Cropscience Ag | Verfahren zur verbesserten Nutzung des Produktionsptentials transgener Pflanzen |
| EP2071952A1 (de) * | 2007-12-21 | 2009-06-24 | Bayer CropScience AG | Verwendung von Tetramsäurederivaten zur Bekämpfung von Schaderregern durch Angiessen oder Tröpfchenapplikation |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007126691A2 (en) * | 2006-03-28 | 2007-11-08 | Bayer Cropscience Ag | Use of tetramic acid derivatives for controlling pests by drenching, drip application, dip application or soil injection |
| WO2007112845A1 (de) * | 2006-03-29 | 2007-10-11 | Bayer Cropscience Ag | Wirkstoffkombinationen mit insektiziden und akariziden eigenschaften |
| WO2007131681A2 (de) * | 2006-05-12 | 2007-11-22 | Bayer Cropscience Ag | Verwendung von tetramsäurederivaten zur bekämpfung von insekten |
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| CL2009000297A1 (es) | 2010-03-05 |
| ZA201005721B (en) | 2011-10-26 |
| US20130296395A1 (en) | 2013-11-07 |
| JP5567500B2 (ja) | 2014-08-06 |
| AU2009214378B2 (en) | 2015-03-26 |
| AU2009214378A1 (en) | 2009-08-20 |
| BRPI0907854A2 (pt) | 2015-07-21 |
| EP2090167A1 (de) | 2009-08-19 |
| NZ587308A (en) | 2012-04-27 |
| JP2011511815A (ja) | 2011-04-14 |
| MA32072B1 (fr) | 2011-02-01 |
| WO2009100851A1 (de) | 2009-08-20 |
| BRPI0907854A8 (pt) | 2016-03-01 |
| EP2242363A1 (de) | 2010-10-27 |
| US20100324303A1 (en) | 2010-12-23 |
| WO2009100851A8 (de) | 2010-08-19 |
| KR20100115777A (ko) | 2010-10-28 |
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