CN101864281B - Cold preserving agent and preparation method thereof - Google Patents

Cold preserving agent and preparation method thereof Download PDF

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Publication number
CN101864281B
CN101864281B CN 201010218161 CN201010218161A CN101864281B CN 101864281 B CN101864281 B CN 101864281B CN 201010218161 CN201010218161 CN 201010218161 CN 201010218161 A CN201010218161 A CN 201010218161A CN 101864281 B CN101864281 B CN 101864281B
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China
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cold
mass parts
retaining agent
water
styrene
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Expired - Fee Related
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CN 201010218161
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CN101864281A (en
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鞠文军
王道元
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BINZHOU CHUANGYUAN EQUIPMENT MECHANICAL MANUFACTURE Co Ltd
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BINZHOU CHUANGYUAN EQUIPMENT MECHANICAL MANUFACTURE Co Ltd
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Publication of CN101864281A publication Critical patent/CN101864281A/en
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  • Medicinal Preparation (AREA)
  • Thermotherapy And Cooling Therapy Devices (AREA)

Abstract

The invention relates to a cold preserving agent and a preparation method thereof. The cold preserving agent comprises bentonite, polyacrylate, glycerol, absolute alcohol, water, salt, butylbenzene emulsion and bamboo charcoal powder. The cold preserving agent is ice free at a temperature of -20 DEG C and has long cold preserving time more than 4h, and can be prepared at a normal temperature. The invention has better effect on the aspects of medicinal cold treatment, family health and the like.

Description

Cold-retaining agent and preparation method thereof
Technical field
The present invention relates to a kind of cold-retaining agent and preparation method thereof, especially a kind ofly can prepare at normal temperatures and have cold-retaining agent of long-time cold insulation effect and preparation method thereof.
Background technology
At present, Physical temperature-lowering in medical science or family health care is processed the ice bag that is mostly of use, ice bag in use dispels the heat comparatively fast, and be not suitable for the elderly and infirm and use, storage needs freezing environment, produces and need to expend time in, when cold treatment owing to being solid, lack flexibility, can not accomplish that maximum area contacts with skin, comfort level is poor.The cold-retaining agent of other type exists mostly also that similar preparation is complicated, the storage environment is strict, the shortcomings such as freezing point temperature is low, rewarming time short (common 1~2 hour).
Summary of the invention
Thus, the invention provides the cold-retaining agent that a kind of preparation method's simple and fast, freezing point temperature are low, rewarming time is long.
The present invention is achieved through the following technical solutions:
The present invention relates to a kind of cold-retaining agent, it is characterized in that: comprising: wilkinite, polyacrylate, glycerine, dehydrated alcohol, water, salt, styrene-butadiene emulsion and bamboo charcoal powder.
Wherein, glycerine and dehydrated alcohol can be substituted by polyvinyl alcohol and ethylene glycol respectively.
Cold-retaining agent of the present invention prepares simple and fast, just can carry out under normal temperature; Do not freeze when-20 spend, freezing point temperature is low; Cold insulation is stored at shady and cool environment and gets final product for up to more than 4 hours; Have flexibility, can accomplish that maximum area contacts with skin during use, and to human body constitution without strict demand.Can be applicable to easily the Medical cold therapies such as wound cold compress, fever is reduced phlegm and internal heat, body part is cooling and family health care aspect.
Embodiment
The present invention will be described in more detail below.
Cold-retaining agent main component of the present invention comprises: wilkinite, polyacrylate, glycerine, dehydrated alcohol, water, salt, styrene-butadiene emulsion, bamboo charcoal powder.In mass parts, the proportioning of each component can be wilkinite 150~250 mass parts, polyacrylate 700~1000 mass parts, glycerine 350~450 mass parts, dehydrated alcohol 350~450 mass parts, water are 900~1200 mass parts, and salt is 50~150 mass parts; styrene-butadiene emulsion 350~450 mass parts, bamboo charcoal powder 50~150 mass parts.
Preferably, the ratio of each component is: wilkinite 170~200 mass parts, polyacrylate 750~850 mass parts, glycerine 400~450 mass parts, dehydrated alcohol 400~450 mass parts, water are 950~1000 mass parts, and salt is 80~120 mass parts; styrene-butadiene emulsion 380~420 mass parts, bamboo charcoal powder 80~120 mass parts.
Above-mentioned wilkinite can be common medical wilkinite, and its granularity is preferably 80~150 orders, more preferably 100~120 orders.
The granularity of above-mentioned bamboo charcoal powder is preferably 80~150 orders, more preferably 100~120 orders.Bamboo charcoal powder can produce far infrared rays, and the most suitable absorption of human body of wavelength can make human body produce low-grade fever, promotes the metabolism of human body, accelerates blood circulation, improves histocyte nutrition, improves the human internal environment.
Above-mentioned styrene-butadiene emulsion can be the styrene-butadiene emulsion of common market sale, and its concentration is preferably 35~45wt%, preferred 40wt%.
Cold-retaining agent of the present invention can not freeze when-20 spend.
In addition, the glycerine in the present invention and dehydrated alcohol can be substituted by polyvinyl alcohol and ethylene glycol respectively, and the proportioning separately after substituting is with replacement is front not identical.
Cold-retaining agent of the present invention can be produced simply by following method, the method comprise the steps: at normal temperatures the wilkinite water is moistening after, be stirred to evenly; Then with the polyacrylate salts of dilute with water with wetting after wilkinite mix; Then add glycerine, dehydrated alcohol, and the salt solution of dilute with water; Continue to stir, after forming pasty state, add styrene-butadiene emulsion; Add at last bamboo charcoal powder.
The present invention is described by the following examples.The invention is not restricted to following embodiment, can change in the scope that the present invention requires.
Embodiment:
Embodiment 1
Under the condition of temperature 24 degree, in mixing tank with 180 gram particle degree be 100~120 purpose wilkinites at first water moistening after, stir.Then, then with 800 gram sodium polyacrylates of dilute with water with wetting after wilkinite mix.Then, the salt solution that contains 100 gram salt that adds 410 gram glycerine, 410 gram dehydrated alcohols and dilute with water.Continue to stir, after becoming pasty state to raw material, adding 400 gram concentration is the styrene-butadiene emulsion of 40wt%, stirs.Adding at last 100 gram particle degree is 80~150 purpose bamboo charcoals, is stirred well to evenly, obtains cold-retaining agent A.In whole process, whole consumptions of water are 980 grams.
Cold-retaining agent A is stored in refrigerator, is cooled to-20 degree, take out this cold-retaining agent A and pack with flexible bags from refrigerator.Cold-retaining agent after packing is applied in the patient injury, approximately just reach room temperature by-20 degree through 5.5 hours this cold-retaining agent A, given play to excellent cold insulation effect.
Embodiment 2
Under the condition of temperature 23 degree, in mixing tank with 150 gram particle degree be 80~150 purpose wilkinites at first water moistening after, stir.Then, then with 900 gram sodium polyacrylates of dilute with water with wetting after wilkinite mix.Then, the salt solution that contains 80 gram salt that adds 380 gram glycerine, 400 gram dehydrated alcohols and dilute with water.Continue to stir, after becoming pasty state to raw material, adding 380 gram concentration is the styrene-butadiene emulsion of 40wt%, stirs.Adding at last 80 gram particle degree is 80~150 purpose bamboo charcoals, is stirred well to evenly, obtains cold-retaining agent B.In whole process, whole consumptions of water are 950 grams.
Cold-retaining agent B is stored in refrigerator, is cooled to-20 degree, take out this cold-retaining agent A and pack with flexible bags from refrigerator.Cold-retaining agent after packing is applied in the patient injury, approximately just reach room temperature by-20 degree through 4.2 hours this cold-retaining agent B, given play to excellent cold insulation effect.
Embodiment 3
Under the condition of temperature 23 degree, in mixing tank with 200 gram particle degree be 80~150 purpose wilkinites at first water moistening after, stir.Then, then with 950 gram sodium polyacrylates of dilute with water with wetting after wilkinite mix.Then, the salt solution that contains 120 gram salt that adds 420 gram glycerine, 430 gram dehydrated alcohols and dilute with water.Continue to stir, after becoming pasty state to raw material, adding 420 gram concentration is the styrene-butadiene emulsion of 40wt%, stirs.Adding at last 140 gram particle degree is 80~150 purpose bamboo charcoals, is stirred well to evenly, obtains cold-retaining agent C.In whole process, whole consumptions of water are 1100 grams.
Cold-retaining agent C is stored in refrigerator, is cooled to-20 degree, take out this cold-retaining agent A and pack with flexible bags from refrigerator.Cold-retaining agent after packing is applied in the patient injury, approximately just reach room temperature by-20 degree through 6 hours this cold-retaining agent C, given play to excellent cold insulation effect.
Can know by above-described embodiment, cold-retaining agent of the present invention can prepare at normal temperatures simply, does not freeze when-20 spend, and the cold insulation time was more than 4 hours.And, owing to having added bamboo charcoal powder, can produce far infrared rays, can make human body produce low-grade fever, promote the metabolism of human body, accelerate blood circulation, improve histocyte nutrition, improve the human internal environment.Cold-retaining agent of the present invention has good effect at aspects such as Medical cold therapy, family health cares.

Claims (9)

1. a cold-retaining agent, is characterized in that: comprising: wilkinite, polyacrylate, glycerine, dehydrated alcohol, water, salt, styrene-butadiene emulsion and bamboo charcoal powder; In mass parts, the ratio of each component is: wilkinite 150~250 mass parts, polyacrylate 700~1000 mass parts, glycerine 350~450 mass parts, dehydrated alcohol 350~450 mass parts, water are 900~1200 mass parts, and salt is 50~150 mass parts; styrene-butadiene emulsion 350~450 mass parts, bamboo charcoal powder 50~150 mass parts.
2. cold-retaining agent according to claim 1, it is characterized in that, in mass parts, the ratio of each component is: wilkinite 170~200 mass parts, polyacrylate 750~850 mass parts, glycerine 400~450 mass parts, dehydrated alcohol 400~450 mass parts, water are 950~1000 mass parts, and salt is 80~120 mass parts; styrene-butadiene emulsion 380~420 mass parts, bamboo charcoal powder 80~120 mass parts.
3. cold-retaining agent according to claim 1, is characterized in that, described bentonitic granularity is 80~150 orders.
4. cold-retaining agent according to claim 3, is characterized in that, described bentonitic granularity is 100~120 orders.
5. cold-retaining agent according to claim 1, is characterized in that, the granularity of described bamboo charcoal powder is 80~150 orders.
6. cold-retaining agent according to claim 1, is characterized in that, the concentration of described styrene-butadiene emulsion is 35~45wt%.
7. cold-retaining agent according to claim 1, is characterized in that, the concentration of described styrene-butadiene emulsion is 40wt%.
8. the described cold-retaining agent of any one according to claim 1~7, is characterized in that, described polyacrylate is sodium polyacrylate.
9. the described cold-retaining agent of any one according to claim 1~7, is characterized in that, described glycerine and dehydrated alcohol are substituted by polyvinyl alcohol and ethylene glycol respectively.
CN 201010218161 2010-07-06 2010-07-06 Cold preserving agent and preparation method thereof Expired - Fee Related CN101864281B (en)

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CN101864281B true CN101864281B (en) 2013-06-05

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Publication number Priority date Publication date Assignee Title
CN103727726A (en) * 2013-11-26 2014-04-16 成都心海汇才生物科技有限公司 Low-temperature ice bag with temperature ranging from -27 DEG C to -36 DEG C
CN105038722B (en) * 2015-06-30 2018-06-29 桂林融通科技有限公司 A kind of durable chemical cold bag and preparation method thereof
CN105802588A (en) * 2016-04-14 2016-07-27 成都嘉宝祥生物科技有限公司 Cold accumulation agent used for medical cold compress physiotherapy and preparation method thereof
CN107307070A (en) * 2017-08-01 2017-11-03 合肥帧讯低温科技有限公司 A kind of compound cryosar antistaling agent and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1065878A (en) * 1992-05-23 1992-11-04 李俊 The manufacture method of cold-retaining agent and goods thereof
CN1415687A (en) * 2002-08-26 2003-05-07 迪斯肯特化学工业(南通)有限公司 Cool Keeping
CN1510099A (en) * 2002-12-26 2004-07-07 天津康乐产业有限公司 Reuse human warming composition with microwave oven heat
US7967999B2 (en) * 2005-06-08 2011-06-28 Jfe Engineering Corporation Heat storage substance, heat storage agent, heat reservoir, heat transport medium, cold insulation agent, cold insulator, melting point control agent for heat storage agent and supercooling preventive agent for heat storage agent
CN101229087A (en) * 2007-12-10 2008-07-30 大进电热制品有限公司 Cold and heat compress bag

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