CN101831807A - Three-prevention finishing method of wool fabric - Google Patents

Three-prevention finishing method of wool fabric Download PDF

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Publication number
CN101831807A
CN101831807A CN201010127074A CN201010127074A CN101831807A CN 101831807 A CN101831807 A CN 101831807A CN 201010127074 A CN201010127074 A CN 201010127074A CN 201010127074 A CN201010127074 A CN 201010127074A CN 101831807 A CN101831807 A CN 101831807A
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CN
China
Prior art keywords
wool fabric
grams per
per liters
minutes
dipping
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201010127074A
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Chinese (zh)
Inventor
马印
曲娴
许并社
狄友波
罗群芳
王淑花
李忠
贾虎生
秦记珍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PINDAR INDUSTRIAL (TAIYUAN) Co Ltd
Taiyuan University of Technology
Original Assignee
PINDAR INDUSTRIAL (TAIYUAN) Co Ltd
Taiyuan University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by PINDAR INDUSTRIAL (TAIYUAN) Co Ltd, Taiyuan University of Technology filed Critical PINDAR INDUSTRIAL (TAIYUAN) Co Ltd
Priority to CN201010127074A priority Critical patent/CN101831807A/en
Publication of CN101831807A publication Critical patent/CN101831807A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a three-prevention finishing method of a wool fabric, which is used for finishing the wool fabric by adopting a dipping-rolling method. In a dipping-rolling process, the dipping temperature of the wool fabric in a finishing solution is 25-40 DEG C, the dipping time is 0.5-2 minutes, and the solution carrying rate of the padded wool fabric is 75%-80%. The three-prevention finishing method of the wool fabric comprises the following steps of: firstly dipping and rolling the wool fabric in an organic silicone quaternary ammonium salt finishing solution and then prebaking for 1-2 minutes at 80-110 DEG C; carrying out dipping-rolling finishing on the wool fabric by using a fluorine-containing macromolecular copolymer dispersing solution and then prebaking for 1-2 minutes at 80-110 DEG C; and finally baking for 3-8 minutes at 120-160 DEG C. The invention enables the finished wool fabric to achieve three-prevention functions of water repellence, oil repellence and dirt prevention, simultaneously enables the fabric to be far away from various harmful bacteria and pollution and achieve good durability and washing fastness, is very beneficial to the wearability and appearance of the wool fabric, and can keep the heat retention and the bulkiness of the wool fabric.

Description

A kind of three-prevention finishing method of wool fabric
Technical field
The present invention relates to a kind of water of refusing of wool fabric, refuse oil, soil resistant finish method.
Background technology
At present, the following finishing agent of the main employing of fabric waterproof arrangement both at home and abroad: paraffin-aluminum soap class, pyridine quaternary ammonium salt class, melamine methylol derivative, stearate chromium complex etc.Though three anti-effects are arranged, and washability is poor.In recent years, along with the further investigation of macromolecular material performance.Application on its textiles also more and more is subjected to researcher's attention, it is different from common material is because its very big surface-activity, has the unexistent superiority of traditional material, therefore have favorable durability and washability, notification number is the method for sorting that CN1424456A discloses a kind of nanometer three anti-dacrons, its principal character is three anti-handle of nano material to dacron, does not then appear in the newspapers with the processing of fluoro-containing macromolecule material to wool fabric.
Summary of the invention
The purpose of this invention is to provide a kind of fluoro-containing macromolecule material carries out three-prevention finishing to wool fabric method, technical problem to be solved be wool fabric had through arrangement good refuse water, refuse oil, antifouling three anti-functions, simultaneously can make fabric again, and have good durability and washability away from various harmful bacterias and pollution.
For addressing the above problem, the technical method that the present invention adopts is as follows:
A kind of three-prevention finishing method of wool fabric is method to be padded in the wool fabric employing put in order.Be that the dressing liquid one of 10~30 grams per liters soaks one and rolls processing with the organosilicon quaternary ammonium salt finish content earlier with wool fabric, in temperature is 80~110 ℃ of following preliminary dryings 0.5~2 minute, and then soak one with fluoro containing polymers copolymer dispersion one and roll arrangement, the liquid carrying rate that pads the back wool fabric is 75~80%, 80~110 ℃ of following preliminary dryings 1~2 minute, under 120~160 ℃, baked 3~8 minutes at last.Fluoro containing polymers copolymer 30~100 grams per liters in the above-mentioned fluoro containing polymers copolymer dispersion preparation, synergist consumption 3~8 grams per liters, soft crosslinking agent 5~10 grams per liters, all the other are water.
The invention has the advantages that and adopt the macromolecule fluorinated copolymer, it has high surface, and surface tension is very little, is lower than the surface tension of water and oil stain, makes water, wet goods can not be wetting on the wool fabric surface, has waterproof, grease proofing, anti-pollution function.Adopt synergist and soft crosslinking agent to strengthen three anti-effects.Adopt organosilicon quaternary ammonium salt then to play waterproof, grease proofing, antibacterial effect.Because the synergistic function of organosilicon and fluoro containing polymers copolymer, give three anti-functions of wool fabric excellence, wool fabric after employing the present invention arrangement is refused the water effect and is reached as high as 100 fens, refuse oil and reach as high as 8 grades, soil resistance can reach 4 grades, and anti-microbial property significantly improves, and has good durability and washability.The technology of the present invention route is reasonable, the technology simple possible, and easy to operate, production cost is low, can be widely used in the woollen and cashmere fabric, can reduce the washing times of fabric, and its wearability and outward appearance all are highly profitable, and keeps the warmth retention property and the bulkiness of wool fabric.
The specific embodiment:
Embodiment 1
1. wool fabric being adopted the organosilicon quaternary ammonium salt finish content is that the dressing liquid one of 10 grams per liters soaks one and rolls processing; 105 ℃ of preliminary dryings of temperature 2 minutes;
2. macromolecule fluorinated copolymer dispersion liquid preparation: fluoro containing polymers copolymer 30 grams per liters, synergist consumption 5 grams per liters, soft crosslinking agent 8 grams per liters, all the other are water, continuous stirring 30 minutes.With this dispersion liquid wool fabric is carried out soaking one and roll, 25 ℃ of temperature, dip time 1 minute pads back liquid carrying rate 75%;
3. 105 ℃ of preliminary dryings of temperature 1 minute, baked 5 minutes at 150 ℃;
Embodiment 2
1. wool fabric being adopted the organosilicon quaternary ammonium salt finish content is that the dressing liquid one of 18 grams per liters soaks one and rolls processing; 100 ℃ of preliminary dryings of temperature 1 minute;
2. macromolecule fluorinated copolymer dispersion liquid preparation: fluoro containing polymers copolymer 50 grams per liters, synergist consumption 7 grams per liters, soft crosslinking agent 5 grams per liters, all the other are water, continuous stirring 30 minutes.With this dispersion liquid wool fabric is carried out soaking one and roll, 30 ℃ of temperature, dip time 1 minute pads back liquid carrying rate 78%;
3. 100 ℃ of preliminary dryings of temperature 1 minute, baked 8 minutes at 130 ℃;
Embodiment 3
1. wool fabric being adopted the organosilicon quaternary ammonium salt finish content is that the dressing liquid one of 30 grams per liters soaks one and rolls processing; 110 ℃ of preliminary dryings of temperature 1 minute;
2. macromolecule fluorinated copolymer dispersion liquid preparation: fluoro containing polymers copolymer 65 grams per liters, synergist consumption 8 grams per liters, soft crosslinking agent 3 grams per liters, all the other are water, continuous stirring 30 minutes.With this dispersion liquid wool fabric is carried out soaking one and roll, 38 ℃ of temperature, dip time 1 minute pads back liquid carrying rate 75%;
3. 105 ℃ of preliminary dryings of temperature 2 minutes, baked 3 minutes at 160 ℃.

Claims (4)

1. the three-prevention finishing method of a wool fabric, it is characterized in that: method is padded in the wool fabric employing it is put in order, pad that the dipping temperature of wool fabric in dressing liquid is 25~40 ℃ in the process, dip time is 0.5~2 minute, the liquid carrying rate that pads the back wool fabric is 75~80%, earlier wool fabric is carried out soaking one in the organosilicon quaternary ammonium salt dressing liquid and roll processing, then in 80~110 ℃ of following preliminary dryings 1~2 minute, soak one with fluoro containing polymers copolymer dispersion one again and roll arrangement, in 80~110 ℃ of following preliminary dryings 1~2 minute, under 120~160 ℃, baked 3~8 minutes at last then.
Above-mentioned dressing liquid is organosilicon quaternary ammonium salt consumption 10~30 grams per liters in preparation, and all the other are water; In the fluoro containing polymers copolymer dispersion, fluoro containing polymers copolymer 30~100 grams per liters, synergist consumption 3~8 grams per liters, soft dosage of crosslinking agent 5~10 grams per liters, all the other are water.
2. method for sorting according to claim 1 is characterized in that: above-mentioned dressing liquid is in when preparation,
(1) add organosilicon quaternary ammonium salt 10~30 grams per liters in reactor, all the other are water, stir 30 minutes, and blowing is stand-by.
(2) in reactor, add fluoro containing polymers copolymer 30~100 grams per liters successively, synergist consumption 3~8 grams per liters, soft crosslinking agent 5~10 grams per liters, all the other are water, continuous stirring 30 minutes, blowing is stand-by.
3. method for sorting according to claim 1 and 2 is characterized in that; The above-mentioned method of padding is to pad processing twice, and its treatment conditions are: 25~40 ℃ of temperature, dip time are 0.5~2 minute, and the pH value is 5~7.
4. method for sorting according to claim 1 is characterized in that in the above-mentioned arrangement, and preliminary drying adopts the noncontact drying mode, heated-air drying, and the time is 1~2 minute.
CN201010127074A 2010-03-18 2010-03-18 Three-prevention finishing method of wool fabric Pending CN101831807A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201010127074A CN101831807A (en) 2010-03-18 2010-03-18 Three-prevention finishing method of wool fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201010127074A CN101831807A (en) 2010-03-18 2010-03-18 Three-prevention finishing method of wool fabric

Publications (1)

Publication Number Publication Date
CN101831807A true CN101831807A (en) 2010-09-15

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102277746A (en) * 2011-07-28 2011-12-14 杭州贝斯特化纤有限公司 Antimicrobial emulsion used for textile fibers and application method thereof
CN102465403A (en) * 2011-06-09 2012-05-23 上海嘉乐股份有限公司 Novel finishing process of co-polymerization fluorine antifouling and soil-releasing finishing liquor
CN102864641A (en) * 2012-10-19 2013-01-09 无锡百和织造股份有限公司 Antifouling quick-drying elastic band and manufacture method thereof
CN103290683A (en) * 2012-02-28 2013-09-11 南通斯得福纺织装饰有限公司 Production method of antibacterial waterproof, oil-proof and antifouling fabric
CN103361979A (en) * 2013-05-21 2013-10-23 如皋市协和印染有限公司 Method for increasing washing durability of three-proof or waterproof fabric
CN103882700A (en) * 2014-03-20 2014-06-25 辛集市梅花皮业有限公司 Waterproof, antifouling and oil-proof treatment technology for knitting wool
CN103952904A (en) * 2014-04-17 2014-07-30 东华大学 Surface modifying and finishing method of wool fabric
CN104024512A (en) * 2011-12-23 2014-09-03 赵殷孝 Fiber product provided with water repellant coating layer and method for manufacturing the fiber product
CN104562351A (en) * 2015-02-09 2015-04-29 苏州陈恒织造有限公司 Production process of stainless steel fiber-containing wool
CN105951426A (en) * 2016-06-12 2016-09-21 合肥市再德高分子材料有限公司 Environment-friendly antibacterial flame-retardant hydrophobic fabric
CN106120308A (en) * 2016-06-12 2016-11-16 合肥市再德高分子材料有限公司 A kind of water-proof antibiotic composite functional fabric
CN107841872A (en) * 2017-11-27 2018-03-27 无锡昊瑜节能环保设备有限公司 A kind of wool fabric antifouling and antibiosis finishing technique
CN110016802A (en) * 2019-03-12 2019-07-16 江苏丹毛纺织股份有限公司 A kind of production method of Machine Washable three proofings worsted fabric

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102465403A (en) * 2011-06-09 2012-05-23 上海嘉乐股份有限公司 Novel finishing process of co-polymerization fluorine antifouling and soil-releasing finishing liquor
CN102277746A (en) * 2011-07-28 2011-12-14 杭州贝斯特化纤有限公司 Antimicrobial emulsion used for textile fibers and application method thereof
CN104024512A (en) * 2011-12-23 2014-09-03 赵殷孝 Fiber product provided with water repellant coating layer and method for manufacturing the fiber product
CN103290683A (en) * 2012-02-28 2013-09-11 南通斯得福纺织装饰有限公司 Production method of antibacterial waterproof, oil-proof and antifouling fabric
CN102864641A (en) * 2012-10-19 2013-01-09 无锡百和织造股份有限公司 Antifouling quick-drying elastic band and manufacture method thereof
CN103361979A (en) * 2013-05-21 2013-10-23 如皋市协和印染有限公司 Method for increasing washing durability of three-proof or waterproof fabric
CN103882700A (en) * 2014-03-20 2014-06-25 辛集市梅花皮业有限公司 Waterproof, antifouling and oil-proof treatment technology for knitting wool
CN103952904A (en) * 2014-04-17 2014-07-30 东华大学 Surface modifying and finishing method of wool fabric
CN104562351A (en) * 2015-02-09 2015-04-29 苏州陈恒织造有限公司 Production process of stainless steel fiber-containing wool
CN105951426A (en) * 2016-06-12 2016-09-21 合肥市再德高分子材料有限公司 Environment-friendly antibacterial flame-retardant hydrophobic fabric
CN106120308A (en) * 2016-06-12 2016-11-16 合肥市再德高分子材料有限公司 A kind of water-proof antibiotic composite functional fabric
CN107841872A (en) * 2017-11-27 2018-03-27 无锡昊瑜节能环保设备有限公司 A kind of wool fabric antifouling and antibiosis finishing technique
CN110016802A (en) * 2019-03-12 2019-07-16 江苏丹毛纺织股份有限公司 A kind of production method of Machine Washable three proofings worsted fabric

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Open date: 20100915