CN101829033B - Three-component tooth stain scavenging agent - Google Patents
Three-component tooth stain scavenging agent Download PDFInfo
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- CN101829033B CN101829033B CN2010101732831A CN201010173283A CN101829033B CN 101829033 B CN101829033 B CN 101829033B CN 2010101732831 A CN2010101732831 A CN 2010101732831A CN 201010173283 A CN201010173283 A CN 201010173283A CN 101829033 B CN101829033 B CN 101829033B
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- sodium
- peroxide
- agent
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Links
- 239000002516 radical scavenger Substances 0.000 title claims abstract description 10
- 150000002978 peroxides Chemical class 0.000 claims abstract description 22
- 239000000084 colloidal system Substances 0.000 claims abstract description 12
- 230000000694 effects Effects 0.000 claims abstract description 8
- 239000001301 oxygen Substances 0.000 claims abstract description 3
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- 229920000136 polysorbate Polymers 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 239000000043 antiallergic agent Substances 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 235000019264 food flavour enhancer Nutrition 0.000 claims description 8
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 claims description 8
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 8
- 239000000080 wetting agent Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 229910001631 strontium chloride Inorganic materials 0.000 claims description 5
- AHBGXTDRMVNFER-UHFFFAOYSA-L strontium dichloride Chemical compound [Cl-].[Cl-].[Sr+2] AHBGXTDRMVNFER-UHFFFAOYSA-L 0.000 claims description 5
- XGRSAFKZAGGXJV-UHFFFAOYSA-N 3-azaniumyl-3-cyclohexylpropanoate Chemical compound OC(=O)CC(N)C1CCCCC1 XGRSAFKZAGGXJV-UHFFFAOYSA-N 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 4
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- 229950008882 polysorbate Drugs 0.000 claims description 4
- 239000011698 potassium fluoride Substances 0.000 claims description 4
- 235000003270 potassium fluoride Nutrition 0.000 claims description 4
- 239000011775 sodium fluoride Substances 0.000 claims description 4
- 235000013024 sodium fluoride Nutrition 0.000 claims description 4
- 229960004711 sodium monofluorophosphate Drugs 0.000 claims description 4
- 239000004094 surface-active agent Substances 0.000 claims description 4
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 108010011485 Aspartame Proteins 0.000 claims description 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims description 3
- 239000000605 aspartame Substances 0.000 claims description 3
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 claims description 3
- 235000010357 aspartame Nutrition 0.000 claims description 3
- 229960003438 aspartame Drugs 0.000 claims description 3
- 229960001631 carbomer Drugs 0.000 claims description 3
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 3
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 3
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 3
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 3
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 3
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 3
- 229940085605 saccharin sodium Drugs 0.000 claims description 3
- 229940013618 stevioside Drugs 0.000 claims description 3
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims description 3
- 235000019202 steviosides Nutrition 0.000 claims description 3
- AQLJVWUFPCUVLO-UHFFFAOYSA-N urea hydrogen peroxide Chemical compound OO.NC(N)=O AQLJVWUFPCUVLO-UHFFFAOYSA-N 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- 244000246386 Mentha pulegium Species 0.000 claims description 2
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 2
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 2
- 239000004376 Sucralose Substances 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 210000004556 brain Anatomy 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- MMCOUVMKNAHQOY-UHFFFAOYSA-N carbonoperoxoic acid Chemical compound OOC(O)=O MMCOUVMKNAHQOY-UHFFFAOYSA-N 0.000 claims description 2
- VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 claims description 2
- 235000001050 hortel pimenta Nutrition 0.000 claims description 2
- 229920000609 methyl cellulose Polymers 0.000 claims description 2
- 239000001923 methylcellulose Substances 0.000 claims description 2
- 229940045872 sodium percarbonate Drugs 0.000 claims description 2
- 235000019408 sucralose Nutrition 0.000 claims description 2
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract 2
- 239000004480 active ingredient Substances 0.000 abstract 1
- 230000002000 scavenging effect Effects 0.000 abstract 1
- 238000005303 weighing Methods 0.000 description 9
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 4
- 235000010333 potassium nitrate Nutrition 0.000 description 4
- 239000004323 potassium nitrate Substances 0.000 description 4
- 238000011160 research Methods 0.000 description 3
- 239000012530 fluid Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- -1 preferred 1%-5% Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 229940013553 strontium chloride Drugs 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 229940068965 polysorbates Drugs 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a three-component tooth stain scavenging agent, which belongs to the technical field of oral health preparations. A component 1 is a substance capable of quickly forming a gel or a colloid; a component 2 is a substance capable of generating oxygen radicals; a component 3 can enable the three components to form the colloid or the gel and improves the activity of a peroxide after the three components are blended; and the three components are hermetically packed in different containers respectively; and the peroxide-containing gel or the peroxide-containing colloid is formed by mixing the three components before the three components are used. The three-component tooth stain scavenging agent of the invention can be prepared when used and is simple in preparation method; the content of active ingredients, namely the peroxide, is high and stable after the three components are blended, so good tooth stain scavenging effect can be achieved; and the three components which are not blended can be stored for a long time.
Description
Technical field
The invention belongs to the preparing technical field of oral cavity health preparation, particularly a kind of is effective ingredient with the peroxide, is carrier with non-Newtonian fluid such as gel or Newtonian fluid such as colloid, is used to remove three components compositions of teeth stains.
Background technology
Improving constantly of Along with people's living standard, People more and more are paid close attention to the oral hygiene of oneself with healthy, have the pure white tooth of a bite more to become the target that many people pursue.Removing teeth stains has become the essential of American-European consumer daily life, and popularizes in China gradually.Since U.S. odontologist in 1981 was used to hydrogen peroxide to remove teeth stains for the first time, peroxide was cleared into branch with the standard mottle that its obvious effects and safety become American-European dental clinic.Yet, directly use peroxide not only the patient to be produced stimulation, but also can because action time the short mottle that causes remove not exclusively.Be that the mottle of carrier is removed compositions and removed mottle comprehensively, advantages such as user's oral stimulation is little have been obtained the favor of American-European dental clinic with it at present, and become its standard and remove the teeth stains prescription with colloid or gel.The height of peroxide content has conclusive effect to the dental bleaching effect in the formula system, so a lot of researchs are being done aspect the raising peroxide effectiveness by various countries research institution.Wherein studying maximum is to select for use suitable carriers to prolong time of peroxide contact dental surface, yet effectively stablize content and improves teeth stains removing Research on effect and also do not appear in the newspapers through improving peroxide.
Summary of the invention
The invention provides a kind of three-component tooth stain scavenging agent; Component 1 is for can form gel or colloidal material fast; Component 2 forms colloid or gel for producing the material of oxygen-derived free radicals after component 3 can make three components be mixed, and improves the activity of peroxide; Enclosed package is in different containers respectively for three components, and preceding three components are mixed of use promptly forms gel or the colloid that contains peroxide; It directly is coated onto on the tooth or does carrier with dens supporter be applied on the tooth and use.
Said component 1 shared percentage by weight in three components is 0.3%-15%, and preferred 0.5%-10% is specially in polyvinylpyrrolidone, carbomer, methylcellulose, the carboxymethyl cellulose one or more.
Said component 2 shared percentage by weight in three components is 5%-50%, and preferred 10%-45% is specially in hydrogen peroxide, percarbamide (claiming urea peroxide again), SODIUM PERCARBONATE, the percarbonic acid calcium one or more.
Said component 3 is concrete form and in three components shared percentage by weight following:
A.0.1%-2% pH value regulator, preferred 0.2%-1%, the pH value that is used to regulate composition system is near neutral, and the pH value regulator is one or more in sodium hydroxide, potassium hydroxide, sodium carbonate, sodium bicarbonate, the triethanolamine;
B.0.5%-10% wetting agent, preferred 1%-5%, wetting agent is a surfactant, is specially in glycerol, Polyethylene Glycol, polysorbate, the tween one or more;
C.0.05%-10% anti-allergic agent, preferred 0.1%-8%, anti-allergic agent is one or more in sodium fluoride, potassium fluoride, sodium monofluorophosphate, strontium chloride, the potassium nitrate;
D. deionized water, surplus is a deionized water.
Said component 3 can also be added flavour enhancer.Component 3 add behind the flavour enhancer concrete form and in three components shared percentage by weight following:
A) the pH value regulator of 0.1%-2%, preferred 0.2%-1%, the pH value that is used to regulate composition system is near neutral, and the pH value regulator is one or more in sodium hydroxide, potassium hydroxide, sodium carbonate, sodium bicarbonate, the triethanolamine;
B) wetting agent of 0.5%-10%, preferred 1%-5%, wetting agent is a surfactant, is specially in glycerol, Polyethylene Glycol, polysorbate, the tween one or more;
C) anti-allergic agent of 0.05%-10%, preferred 0.1%-8%, anti-allergic agent is one or more in sodium fluoride, potassium fluoride, sodium monofluorophosphate, strontium chloride, the potassium nitrate;
D) flavour enhancer of 0.02%-2%, preferred 0.1%-2%, flavour enhancer is one or more in water solublity Herba Menthae brain, peppermint essence, fruity essence, saccharin sodium, aspartame, sucralose, the stevioside;
E) deionized water, surplus are deionized water.
Described mixed method adds component 3 then and fully mixes gel or the colloid that i.e. formation contains peroxide for component 2 being added component 1 and stirring.
Compared with prior art, three-component tooth stain scavenging agent of the present invention can join existing usefulness at present and compound method easy, the content that three components are mixed back effective ingredient peroxide is high and stable, can reach good teeth stains and remove effect; But long-term storage when three components are unmixed.
The specific embodiment
Following non-limiting example is further narrated the preferred embodiment in the scope of the invention.Under the situation that does not deviate from the scope of the invention, a lot of variations of present embodiment are possible.
Embodiment 1
Component 1 carbomer 13.00%
Component 2 hydrogen peroxide 40.00%
Sodium hydroxide 0.35%
Component 3 glycerol 8.00%
Saccharin sodium 0.12%
Potassium nitrate 3.4%
Water 35.13%
Compound method is following: a) with component 1 weighing and be packaged in hermetic container.B) with component 2 weighings and be packaged in hermetic container.C) with component 3 weighings, mixing, dissolve and be packaged in hermetic container.
Component 2 is added components 1 and stirs, add component 3 then and fully mix and promptly form the gel that contains peroxide, test content of hydrogen peroxide 38%.
Embodiment 2
Component 1 carboxymethyl cellulose 10.00%
Plain
Component 2 hydrogen peroxide 45.00%
Triethanolamine 0.80%
Component 3 polysorbates 2.00%
Potassium nitrate 3.20%
Stevioside 0.10%
Water 38.9%
Compound method is following: a) with component 1 weighing and be packaged in hermetic container.B) with component 2 weighings and be packaged in hermetic container.C) with component 3 weighings, mixing, dissolve and be packaged in hermetic container.
Component 2 is added components 1 and stirs, add component 3 then and fully mix and promptly form the gel that contains peroxide, test content of hydrogen peroxide 42%.
Embodiment 3
Component 1 polyvinylpyrrolidone 8.00%
Component 2 percarbamides 36.00%
Tween 4.00%
Component 3 sodium carbonate 0.65%
Strontium chloride 2.10%
Aspartame 0.10%
Water 49.15%
Compound method is following: a) with component 1 weighing and be packaged in hermetic container.B) with component 2 weighings and be packaged in hermetic container.C) with component 3 weighings, mixing, dissolve and be packaged in hermetic container.
Component 2 is added components 1 and stirs, add component 3 then and fully mix and promptly form the colloid that contains peroxide, test peroxide contents 35%.
Claims (4)
1. three-component tooth stain scavenging agent; It is characterized in that component 1 is for can form gel or colloidal material fast, component 2 is for producing the material of oxygen-derived free radicals; Form colloid or gel after component 3 can make three components be mixed, and improve the activity of peroxide; Enclosed package is in different containers respectively for three components, and preceding three components are mixed of use promptly forms gel or the colloid that contains peroxide;
Said component 1 shared percentage by weight in three components is 0.3%-15%, is specially in polyvinylpyrrolidone, carbomer, methylcellulose, the carboxymethyl cellulose one or more;
Said component 2 shared percentage by weight in three components is 5%-50%, is specially in hydrogen peroxide, percarbamide, SODIUM PERCARBONATE, the percarbonic acid calcium one or more;
Said component 3 is concrete form and in three components shared percentage by weight following:
A.0.1%-2% pH value regulator, the pH value that is used to regulate composition system is near neutral, and the pH value regulator is one or more in sodium hydroxide, potassium hydroxide, sodium carbonate, sodium bicarbonate, the triethanolamine;
B.0.5%-10% wetting agent, wetting agent is a surfactant, is specially in glycerol, Polyethylene Glycol, polysorbate, the tween one or more;
C.0.05%-10% anti-allergic agent, anti-allergic agent are one or more in sodium fluoride, potassium fluoride, sodium monofluorophosphate, the strontium chloride;
D. deionized water, surplus is a deionized water.
2. a kind of three-component tooth stain scavenging agent according to claim 1 is characterized in that, said component 3 also comprises flavour enhancer.
3. a kind of three-component tooth stain scavenging agent according to claim 2 is characterized in that, said component 3 add behind the flavour enhancer concrete form and in three components shared percentage by weight following:
A.0.1%-2% pH value regulator, the pH value that is used to regulate composition system is near neutral, and the pH value regulator is one or more in sodium hydroxide, potassium hydroxide, sodium carbonate, sodium bicarbonate, the triethanolamine;
B.0.5%-10% wetting agent, wetting agent is a surfactant, is specially in glycerol, Polyethylene Glycol, polysorbate, the tween one or more;
C.0.05%-10% anti-allergic agent, anti-allergic agent are one or more in sodium fluoride, potassium fluoride, sodium monofluorophosphate, the strontium chloride;
D.0.02%-2% flavour enhancer, flavour enhancer are one or more in water solublity Herba Menthae brain, peppermint essence, fruity essence, saccharin sodium, aspartame, sucralose, the stevioside;
E. deionized water, surplus is a deionized water.
4. the mixed method of claim 1 and 3 arbitrary described three-component tooth stain scavenging agents is characterized in that, component 2 is added components 1 and stirs, and adds component 3 then and fully mixes and promptly form gel or the colloid that contains peroxide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101732831A CN101829033B (en) | 2010-05-11 | 2010-05-11 | Three-component tooth stain scavenging agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101732831A CN101829033B (en) | 2010-05-11 | 2010-05-11 | Three-component tooth stain scavenging agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101829033A CN101829033A (en) | 2010-09-15 |
| CN101829033B true CN101829033B (en) | 2012-05-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010101732831A Expired - Fee Related CN101829033B (en) | 2010-05-11 | 2010-05-11 | Three-component tooth stain scavenging agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101829033B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3811922A1 (en) * | 2019-10-24 | 2021-04-28 | Koninklijke Philips N.V. | Kit, system and method for preparing and use of a peroxide-containing composition |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1499955A (en) * | 2001-04-04 | 2004-05-26 | Kits for whitening teeth |
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2010
- 2010-05-11 CN CN2010101732831A patent/CN101829033B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1499955A (en) * | 2001-04-04 | 2004-05-26 | Kits for whitening teeth |
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| Publication number | Publication date |
|---|---|
| CN101829033A (en) | 2010-09-15 |
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