CN101824092B - Soaking technology for preparing corn starch - Google Patents

Soaking technology for preparing corn starch Download PDF

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Publication number
CN101824092B
CN101824092B CN2009100169362A CN200910016936A CN101824092B CN 101824092 B CN101824092 B CN 101824092B CN 2009100169362 A CN2009100169362 A CN 2009100169362A CN 200910016936 A CN200910016936 A CN 200910016936A CN 101824092 B CN101824092 B CN 101824092B
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China
Prior art keywords
corn
soaking
enzymolysis
starch
enzyme
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CN2009100169362A
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CN101824092A (en
Inventor
赵光辉
王秀娟
王成福
刘晓娟
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SHANDONG FUTASTE SUGAR ALCOHOL CO Ltd
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SHANDONG FUTASTE SUGAR ALCOHOL CO Ltd
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  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Enzymes And Modification Thereof (AREA)

Abstract

The invention relates to a soaking technology for preparing corn starch, belonging to the technical field of grain deep processing. The technological steps comprise: 1. soaking: corn grains are soaked in water to soften embryos; 2. pulp grinding: the soaked corn grains are coarsely ground to obtain corn pulp; 3. enzymolysis: one of acid protease and pepsin is added in the obtained corn pulp after coarse grinding to conduct enzymolysis to the corn pulp, and SO2 is fed at the same time to mainly take the effect of inhibiting activities of microorganisms on the premise that the enzymatic activity is not affected; and 4. fine grinding, separation and drying to obtain starch finished product. Through shortening soaking time and reducing the used amount of SO2, the invention has the advantages that the corrosion of equipment, the underground water pollution, the residual sulfurous acid in the product and the like are obviously reduced, the obstacles restricting enzyme to enter endosperm to react with protein particles are eliminated, the total soaking time is only 8-12h, the soaking time is shortened, the cost is reduced, the effect is good, and the popularization value and the application value are high.

Description

A kind of soaking technology for preparing W-Gum
Technical field
The invention belongs to technical field of grain deep processing, specifically a kind of preparation method of W-Gum.
Background technology
Producing W-Gum is the important channel of corn deep processing, and in the W-Gum production process, first road also is that most important operation is the immersion of corn, and its effect is softening corn kernel, reduces the physical strength of corn grain; Disperse the protein net in the maize somatocyte, weaken the connecting key that keeps starch; Corn kernel is expanded, more easily with cortex, plumule, endosperm separation etc.At present, adopt both at home and abroad usually be with corn under 48-54 ℃, with the sulfurous acid solution immersion of 0.1-0.25% 24-48 hour, through SO 2Diffusion, do not dissolve protein transduction to a part in the corn and become solubilising protein, and, make the protein molecule depolymerization through interrupting the connecting key between the protein molecule, impel starch granules from the protein that surrounds it, to discharge.But find SO through producing 2Be penetrated in the endosperm and with the protein network effect; It is a very time-consuming procedure; Usually need 24-36 hour, if soak time less than 24 hours, can make starch yield descend; Partial starch remains in fiber and the protein, and the sulfurous acid solution soaking corn of using higher concentration simultaneously can cause in corrosion on Equipment, groundwater pollution and the product problems such as sulfurous acid is residual to a certain extent.
At present, each enterprise or research institution just are being devoted to when guaranteeing to soak effect, reduce the sulfurous gas in the soaked in water, the research of shortening soak time.Disclose the working method that a kind of W-Gum enzyme process soaks like Chinese patent 200610016774.9, utilized this method can soak time be shortened to 20-24 hour, SO by 48 hours 2Consumption is reduced to 0.06% by 0.25%, and total energy consumption reduces by 25%, but has used lactobacillus inoculation and the higher bromeline of price through seed selection in this method, causes that operation is more loaded down with trivial details, production cost is higher, is difficult to aborning apply.
Summary of the invention
The purpose of this invention is to provide a kind of soaking technology for preparing W-Gum,, SO long with soak time in the soaking technology that solves the prior art for preparing W-Gum 2Cause equipment corrosion, groundwater pollution, product Central Asia vitriolic is residual and the enzyme process soaking technology in problem such as loaded down with trivial details, the production cost height of the operation that exists.
The technical scheme that technical solution problem of the present invention is adopted provides a kind of shortening soak time and reduces SO 2The novel process that the enzyme mill of consumption soaks, its process step is following:
1, soak: corn particle soaks in water, so that plumule is softening, is unlikely broken in pass, and the time of corn soaking is 1-10h, and soaking temperature is 45-60 ℃;
2, defibrination: the corn grain after will soaking is roughly ground and is obtained steeping water;
3, enzymolysis: add a kind of in aspartic protease, the stomach en-in the steeping water that after corase grind, obtains, steeping water is carried out enzymolysis, make the albumen substrate degraded, discharge starch, the enzyme dosage is the 0.25%-1.0% of raw material corn quality, feeds SO simultaneously 2, SO 2Dosage is the 0.02%-0.06% of raw material corn quality, and mainly being is not influencing under the enzyme prerequisite alive, playing the effect that suppresses microbial activities, and hydrolysis temperature is 20-70 ℃, and enzymolysis pH value is 3.5-6.5, enzymolysis time 1-6h;
4, fine grinding separates: the steeping water after handling through enzyme is carried out germ separation, fine grinding, screening and spinning make wet starch, through dry, obtain finished product of starch again.
Description of drawings
Below in conjunction with accompanying drawing technology of the present invention is described further.
Fig. 1 is a process flow sheet.
Adopt this kind immersion way; Problems such as sulfurous acid is residual have significantly been reduced in corrosion on Equipment, groundwater pollution and the product; Got rid of the obstacle that enzyme gets into endosperm and reacts with protein particulate, whole soak time only needs 8-12h, has shortened soak time; Reduce cost, had good effect and application value.
Embodiment
Below in conjunction with specific embodiment the present invention is further described:
Used proteolytic enzyme during enzymolysis, preferred acid protease.
Embodiment 1:
The 100g corn soaks 6h in the water under 48 ℃, the corn after soaking is roughly ground, and adds SO in the steeping water after corase grind then 20.06g, aspartic protease 0.5g, and transfer pH4.0, under 25 ℃, enzymolysis 4h constantly stirs therebetween.Steeping water behind the enzymolysis makes finished product of starch through taking off embryo, fine grinding, screening, spinning, drying and other steps again.
Embodiment 2:
The 100g corn soaks 4h in the water under 50 ℃, the corn after soaking is roughly ground, and adds SO in the steeping water after corase grind then 20.02g, aspartic protease 0.3g, and transfer pH4.5, under 63 ℃, enzymolysis 2h constantly stirs therebetween.Steeping water behind the enzymolysis makes finished product of starch through taking off embryo, fine grinding, screening, spinning, drying and other steps again.
Embodiment 3:
The 100g corn soaks 7h in the water under 45 ℃, the corn after soaking is roughly ground, and adds SO in the steeping water after corase grind then 20.041g, stomach en-0.25g, and transfer pH3.5, under 50 ℃, enzymolysis 3h constantly stirs therebetween.Steeping water behind the enzymolysis makes finished product of starch through taking off embryo, fine grinding, screening, spinning, drying and other steps again.
Embodiment 4:
The 100g corn soaks 3h in the water under 58 ℃, the corn after soaking is roughly ground, and adds SO in the steeping water after corase grind then 20.035g, aspartic protease 0.72g, and transfer pH 5.5, under 48 ℃, enzymolysis 5h constantly stirs therebetween.Steeping water behind the enzymolysis makes finished product of starch through taking off embryo, fine grinding, screening, spinning, drying and other steps again.

Claims (2)

1. a soaking technology for preparing W-Gum is characterized in that shortening soak time and reduces SO 2Consumption, concrete process step is following:
(1) soak: corn particle soaks in water, so that plumule is softening, is unlikely broken in pass, and the time of corn soaking is 1-10h, and soaking temperature is 45-60 ℃;
(2) defibrination: the corn grain after will soaking is roughly ground and is obtained steeping water;
(3) enzymolysis: add aspartic protease in the steeping water that after corase grind, obtains, steeping water is carried out enzymolysis, make the albumen substrate degraded, discharge starch, the enzyme dosage is the 0.25%-1.0% of raw material corn quality, feeds SO simultaneously 2, SO 2Dosage is the 0.02%-0.06% of raw material corn quality, and mainly being is not influencing under the enzyme prerequisite alive, playing the effect that suppresses microbial activities, and hydrolysis temperature is 20-70 ℃, and enzymolysis pH value is 3.5-6.5, enzymolysis time 1-6h;
(4) fine grinding separates: the steeping water after handling through enzyme is carried out germ separation, fine grinding, screening and spinning make wet starch, through dry, obtain finished product of starch again.
2. a kind of soaking technology for preparing W-Gum as claimed in claim 1 is characterized in that the preferred stomach en-of aspartic protease.
CN2009100169362A 2009-06-30 2009-06-30 Soaking technology for preparing corn starch Expired - Fee Related CN101824092B (en)

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CN101824092B true CN101824092B (en) 2012-06-06

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Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102371197A (en) * 2010-08-13 2012-03-14 中粮生物化学(安徽)股份有限公司 Degerming method for corns
CN102443069B (en) * 2010-10-13 2013-06-19 中粮生物化学(安徽)股份有限公司 Corn processing method
CN102660513B (en) * 2012-05-10 2015-04-08 宁夏夏盛实业集团有限公司 Compound enzyme special for processing of corn starch
CN102850460B (en) * 2012-09-05 2014-12-17 施韧 Sectional corn dipping method
CN103665171B (en) * 2013-11-26 2016-05-18 郑州市中食农产品加工研究院 A kind of method of corn soaking in production of corn starch process
CN103992410B (en) * 2014-05-15 2016-01-06 菱花集团有限公司 Method and the device of power plant desulfurization water soaking corn is utilized in starch producing technology
CN108148142B (en) * 2018-02-02 2021-05-07 河南工业大学 Ultrasonic-assisted corn starch extraction method
CN109892549B (en) * 2019-04-11 2022-07-15 四川大学 Wet preparation method of instant whole-corn nutritional snowflake tablets
CN112279928B (en) * 2020-10-29 2021-08-10 秦皇岛骊骅淀粉股份有限公司 Starch production process

Citations (5)

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Publication number Priority date Publication date Assignee Title
CN1363610A (en) * 2001-11-16 2002-08-14 吉林省轻工业设计研究院 Improved immersion process in preparing straight-chain corn starch
CN1831013A (en) * 2006-04-18 2006-09-13 吉林大学 Corn starch soaking prodn. process of adding vegetable protease
CN101011119A (en) * 2007-02-01 2007-08-08 叶云侠 Corn-rice extra-strong powder treated by biological enzyme and preparation method thereof
CN101096696A (en) * 2007-07-06 2008-01-02 山东天久生物技术有限公司 Industrial production method of corn protein polypeptide from corn protein powder by enzymatical process
CN101372702A (en) * 2008-10-21 2009-02-25 吉林农业大学 Method for shortening maize immersion time in cornstarch production process

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1363610A (en) * 2001-11-16 2002-08-14 吉林省轻工业设计研究院 Improved immersion process in preparing straight-chain corn starch
CN1831013A (en) * 2006-04-18 2006-09-13 吉林大学 Corn starch soaking prodn. process of adding vegetable protease
CN101011119A (en) * 2007-02-01 2007-08-08 叶云侠 Corn-rice extra-strong powder treated by biological enzyme and preparation method thereof
CN101096696A (en) * 2007-07-06 2008-01-02 山东天久生物技术有限公司 Industrial production method of corn protein polypeptide from corn protein powder by enzymatical process
CN101372702A (en) * 2008-10-21 2009-02-25 吉林农业大学 Method for shortening maize immersion time in cornstarch production process

Non-Patent Citations (1)

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