CN101818278A - Device and method for preparing porous foam metal by metal melt inflation process - Google Patents

Device and method for preparing porous foam metal by metal melt inflation process Download PDF

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Publication number
CN101818278A
CN101818278A CN 201010173379 CN201010173379A CN101818278A CN 101818278 A CN101818278 A CN 101818278A CN 201010173379 CN201010173379 CN 201010173379 CN 201010173379 A CN201010173379 A CN 201010173379A CN 101818278 A CN101818278 A CN 101818278A
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metal
metal melt
high frequency
bubble
frequency ultrasound
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CN 201010173379
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Chinese (zh)
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高玉周
刘世永
张会臣
许晓磊
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Dalian Maritime University
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Dalian Maritime University
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Priority to CN 201010173379 priority Critical patent/CN101818278A/en
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Abstract

The invention discloses a device and a method for preparing porous foam metal by a metal melt inflation process. The device comprises a metal melt groove, a foaming chamber, a fluid hole, a release valve and a metal crystallizer. The middle of the metal crystallizer is provided with a high-frequency ultrasonic oscillator; and the high-frequency ultrasonic oscillator is connected with a high-frequency ultrasonic power source used for adjusting the oscillation frequency, amplitude and power of the high-frequency ultrasonic oscillator. The high-frequency ultrasonic oscillator is started, when the bubble-containing metal melt passes through the metal crystallizer, bubbles are subjected to ultrasonic oscillation for fragmentation under the action of the high-frequency ultrasonic oscillation, and a bubble is fragmented into several smaller bubbles; and the oscillation frequency and the amplitude of the high-frequency ultrasonic oscillator are adjusted, so that the fragmentation degree and the size of the bubbles meet the requirements. The bubbles formed by high-frequency ultrasonic oscillation have uniform size and distribution; and the device and the method have the advantages of simple process and low cost, and are suitable for large-scale production, promotion and application.

Description

A kind of Apparatus for () and method therefor for preparing porous foam metal with the metal melt inflation process
Technical field
The invention belongs to the metallic substance technology of preparing of mechanical engineering field, particularly a kind of Apparatus for () and method therefor for preparing porous foam metal with the metal melt inflation process.
Background technology
Porous metal material with foamy structure is because its special structure formation, not only have weldability, can conduct electricity, general metal properties such as extending, and more demonstrate self characteristic at aspects such as energy-absorbing damping, high damping, noise elimination noise reduction, heat insulation heat exchange, electromagnetic shielding, air-and water-permeables, be widely used in fields such as industry, health care, building trade, environmental protection cause and high and new technology.State according to metal in the preparation process divides, and the preparation method of porous foam metal mainly contains liquid phase method, solid phase method and metal deposition.The foaming of the liquid metal method such as method that can reduce foaming by direct gas-blowing foaming method, metal hydride realizes; The foaming of solid metal can be passed through methods such as powder metallurgic method, powder foam method, metal hollow ball method and metal-powder fiber sintering method and realize; Metal deposition is to adopt the method for chemistry or physics to realize.But all there are some problems in these methods:
1, metal hydride reduces foaming method because the metal hydride decomposition course is restive, and there is the cost problem of higher in the bubble of its formation equally with direct air blast foaming; Because the existence of H forms hydrogen embrittlement easily, worsen the mechanical property of metal again, only be suitable for the foaming of Al, Mg metal, then inapplicable to Ti metal and alloy thereof.
2, the foaming of Al metal can only use direct inflation foaming to prepare foamed metal, but in preparation process, because gathering, the merging of bubble, the pore size in the Al foamed metal is restive, pore size is not of uniform size, thereby the performance of material is produced adverse influence.
Summary of the invention
Be to solve the problems referred to above that prior art exists, the objective of the invention is to propose a kind of preparation technology simple, with low cost, go for that multiple metal foaming and pore size can control prepare the Apparatus for () and method therefor of porous foam metal with the metal melt inflation process.
To achieve these goals, technical scheme of the present invention is as follows: a kind of equipment for preparing porous foam metal with the metal melt inflation process, comprise the metal melt groove, foaming chamber, fluid bore, divider wall, snifting valve, the metallic crystal device, described metal melt groove separates with foaming chamber by the divider wall of band fluid bore, snifting valve is arranged at described foaming chamber top, the side links to each other with the metallic crystal device, the middle part of described metallic crystal device is equipped with the high frequency ultrasound vibrator, described high frequency ultrasound vibrator be used to regulate its vibrational frequency, the high frequency ultrasound power supply of amplitude and watt level connects.
Metallic crystal device of the present invention adopts bolt to be connected with the high frequency ultrasound vibrator.
The experiment power of high frequency ultrasound vibrator of the present invention is 400~500W, and vibrational frequency is 21.8kHz, and amplitude is 1.4~2.0 * 10 -5M, magnetzation current is 6~10A during experiment, screen current is 1~2A.
A kind ofly prepare the method for porous foam metal, may further comprise the steps with the metal melt inflation process:
A, with the METAL HEATING PROCESS in the metal melt groove to about 200-300 more than the fusing point ℃, form metal melt;
B, metal melt is charged into air by tracheae;
C, startup high frequency ultrasound vibrator, when making the metal melt that contains bubble pass through the metallic crystal device, under the high frequency ultrasound oscillating action, bubble is by ultrasonic vibration generation fragmentation, and a bubble fragmentation is several more tiny bubbles; Adjust the vibrational frequency and the amplitude of high frequency ultrasound vibrator, the fragmentation degree and the bubble of bubble are of the required size;
D, make the metal melt that contains tiny pore afterbody solidification and crystallization, form porous foam metal material at the metallic crystal device.
Compared with prior art, the present invention has following beneficial effect:
1, because the present invention adopts the high frequency ultrasound vibration that metal melt is carried out thermal vibration, make metal melt produce a large amount of bubbles, the gas that is dissolved in the liquid can be spread in the bubble; For direct air blast foaming, under the high frequency ultrasound vibration condition, bubble produces the fragmentation effect, is a large amount of small bubbles than the air pocket fragmentation.The bubble size that high frequency ultrasound vibration forms, be evenly distributed, this method technology is simple, and cost is low, and suitable scale operation is applied.
2, the present invention does not have strict restriction to the gas that is adopted, and adopts rare gas element Ar, He, N 2, CO 2Or the like, metal structure structure and mechanical property are had no adverse effects, overcome metal hydride and reduced foaming in the method H element to the detrimentally affect of metal structure structures such as Ti metal and alloy, iron and steel and mechanical property, applicable to the foaming of multiple metal.
3, the present invention is by adjusting frequency, the amplitude of high frequency ultrasound vibration, can adjust the reactive force of ultrasonic wave to bubble, the fragmentation degree and the bubble size of control bubble can change the aperture size size of part within a large range, are fit to large-scale industrial application.
Description of drawings
The present invention is 1 of drawings attached only, wherein:
Fig. 1 prepares the structural representation of the equipment of porous foam metal with the metal melt inflation process.
Among the figure, 1, the metal melt groove, 2, foaming chamber, 3, fluid bore, 4, divider wall, 5, snifting valve, 6, the metallic crystal device, 7, the high frequency ultrasound vibrator, 8, the high frequency ultrasound power supply, 9, metal melt, 10, tracheae, 11, bubble, 12, foam metal material.
Embodiment
Below in conjunction with accompanying drawing the present invention is described further, as shown in Figure 1, a kind of equipment for preparing porous foam metal with the metal melt inflation process, comprise metal melt groove 1, foaming chamber 2, fluid bore 3, divider wall 4, snifting valve 5, metallic crystal device 6, described metal melt groove 1 separates with foaming chamber 2 by the divider wall 4 of band fluid bore 3, snifting valve 5 is arranged at described foaming chamber 2 tops, the side links to each other with metallic crystal device 6, the middle part of described metallic crystal device 6 is equipped with high frequency ultrasound vibrator 7, described high frequency ultrasound vibrator 7 be used to regulate its vibrational frequency, the high frequency ultrasound power supply 8 of amplitude and watt level connects.Described metallic crystal device 6 adopts bolt to be connected with high frequency ultrasound vibrator 7.The experiment power of described high frequency ultrasound vibrator 7 is 400~500W, and vibrational frequency is 21.8kHz, and amplitude is 1.4~2.0 * 10 -5M, magnetzation current is 6~10A during experiment, screen current is 1~2A.
A kind ofly prepare the method for porous foam metal, may further comprise the steps with the metal melt inflation process:
A, with the METAL HEATING PROCESS in the metal melt groove 1 to about 200-300 more than the fusing point ℃, form metal melt 9;
B, metal melt 9 is charged into air by tracheae 10;
C, startup high frequency ultrasound vibrator 7, when making the metal melt 9 that contains bubble 11 pass through metallic crystal device 6, under the high frequency ultrasound oscillating action, bubble 11 is by ultrasonic vibration generation fragmentation, and bubble 11 fragmentations are several more tiny bubbles 11; Adjust the vibrational frequency and the amplitude of high frequency ultrasound vibrator 7, the fragmentation degree and the bubble of bubble 11 are of the required size;
D, make the metal melt 9 that contains tiny pore afterbody solidification and crystallization, form porous foam metal material 12 at metallic crystal device 6.

Claims (4)

1. equipment for preparing porous foam metal with the metal melt inflation process, comprise metal melt groove (1), foaming chamber (2), fluid bore (3), divider wall (4), snifting valve (5), metallic crystal device (6), described metal melt groove (1) separates with foaming chamber (2) by the divider wall (4) of band fluid bore (3), snifting valve (5) is arranged at described foaming chamber (2) top, the side links to each other with metallic crystal device (6), it is characterized in that: the middle part of described metallic crystal device (6) is equipped with high frequency ultrasound vibrator (7), described high frequency ultrasound vibrator (7) be used to regulate its vibrational frequency, the high frequency ultrasound power supply (8) of amplitude and watt level connects.
2. according to claim 1ly a kind ofly prepare the equipment of porous foam metal with the metal melt inflation process, it is characterized in that: described metallic crystal device (6) adopts bolt to be connected with high frequency ultrasound vibrator (7).
3. according to claim 1ly a kind ofly prepare the equipment of porous foam metal with the metal melt inflation process, it is characterized in that: the experiment power of described high frequency ultrasound vibrator (7) is 400~500W, and vibrational frequency is 21.8kHz, and amplitude is 1.4~2.0 * 10 -5M, magnetzation current is 6~10A during experiment, screen current is 1~2A.
4. one kind prepares the method for porous foam metal with the metal melt inflation process, it is characterized in that: may further comprise the steps:
A, with the METAL HEATING PROCESS in the metal melt groove (1) above about 200-300 ℃, formation metal melt (9) to fusing point;
B, metal melt (9) is charged into air by tracheae (10);
C, startup high frequency ultrasound vibrator (7), when making the metal melt (9) that contains bubble (11) pass through metallic crystal device (6), under the high frequency ultrasound oscillating action, bubble (11) is by ultrasonic vibration generation fragmentation, and a bubble (11) fragmentation is several more tiny bubbles (11); Adjust the vibrational frequency and the amplitude of high frequency ultrasound vibrator (7), the fragmentation degree and the bubble of bubble (11) are of the required size;
D, make the metal melt (9) that contains tiny pore afterbody solidification and crystallization, form porous foam metal material (12) at metallic crystal device (6).
CN 201010173379 2010-05-14 2010-05-14 Device and method for preparing porous foam metal by metal melt inflation process Pending CN101818278A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451230A (en) * 2014-11-17 2015-03-25 界首市一鸣新材料科技有限公司 Improved process for producing foamed aluminum by adopting ultrasonic melt-foaming method
CN104633291A (en) * 2014-12-22 2015-05-20 界首市一鸣新材料科技有限公司 High-strength light foamed aluminium steel pipe
CN105415566A (en) * 2015-12-22 2016-03-23 常州信息职业技术学院 Ultrasonic vibration micro-foaming injection moulding device and ultrasonic vibration micro-foaming injection moulding method for plastic inspection well
CN105463229A (en) * 2016-01-27 2016-04-06 东北大学 Preparation device of foamed aluminum capable of effectively inhibiting drainage phenomenon
CN106148747A (en) * 2016-07-14 2016-11-23 清华大学 Air blast prepares the preparation method of foamed aluminium device and foamed aluminium
CN106670474A (en) * 2016-12-29 2017-05-17 苏州大学 Preparation method of foam aluminum sandwich panel
CN107512865A (en) * 2017-09-26 2017-12-26 安徽斯威达建材科技有限公司 A kind of preparation method of foaming agent
ES2664614A1 (en) * 2016-10-20 2018-04-20 Alucoil, S.A. PROCEDURE FOR OBTAINING A SANDWICH PANEL WITH ALUMINUM FOAM IN THE CORE, INSTALLATION AND PRODUCT OBTAINED (Machine-translation by Google Translate, not legally binding)
WO2020124840A1 (en) * 2018-12-18 2020-06-25 武汉华星光电半导体显示技术有限公司 Substrate and display panel

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5334236A (en) * 1991-05-31 1994-08-02 Alcan International Limited Process for producing shaped slabs of particle stabilized foamed metal
CN1546696A (en) * 2003-12-03 2004-11-17 东南大学 Low porosity closed cell foam aluminum alloy and its preparation method
CN101109050A (en) * 2007-08-31 2008-01-23 清华大学 Method for continuously manufacturing stephanoporate aluminum product with gas direct blowing and blowing and device thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5334236A (en) * 1991-05-31 1994-08-02 Alcan International Limited Process for producing shaped slabs of particle stabilized foamed metal
CN1546696A (en) * 2003-12-03 2004-11-17 东南大学 Low porosity closed cell foam aluminum alloy and its preparation method
CN101109050A (en) * 2007-08-31 2008-01-23 清华大学 Method for continuously manufacturing stephanoporate aluminum product with gas direct blowing and blowing and device thereof

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451230A (en) * 2014-11-17 2015-03-25 界首市一鸣新材料科技有限公司 Improved process for producing foamed aluminum by adopting ultrasonic melt-foaming method
CN104633291A (en) * 2014-12-22 2015-05-20 界首市一鸣新材料科技有限公司 High-strength light foamed aluminium steel pipe
CN104633291B (en) * 2014-12-22 2016-05-25 界首市一鸣新材料科技有限公司 High-strength light foamed aluminium steel pipe
CN105415566A (en) * 2015-12-22 2016-03-23 常州信息职业技术学院 Ultrasonic vibration micro-foaming injection moulding device and ultrasonic vibration micro-foaming injection moulding method for plastic inspection well
CN105463229A (en) * 2016-01-27 2016-04-06 东北大学 Preparation device of foamed aluminum capable of effectively inhibiting drainage phenomenon
CN106148747A (en) * 2016-07-14 2016-11-23 清华大学 Air blast prepares the preparation method of foamed aluminium device and foamed aluminium
ES2664614A1 (en) * 2016-10-20 2018-04-20 Alucoil, S.A. PROCEDURE FOR OBTAINING A SANDWICH PANEL WITH ALUMINUM FOAM IN THE CORE, INSTALLATION AND PRODUCT OBTAINED (Machine-translation by Google Translate, not legally binding)
WO2018073471A1 (en) * 2016-10-20 2018-04-26 Alucoil, S.A. Method for obtaining a sandwich panel with aluminium foam in the core, installation and product obtained
CN106670474A (en) * 2016-12-29 2017-05-17 苏州大学 Preparation method of foam aluminum sandwich panel
CN107512865A (en) * 2017-09-26 2017-12-26 安徽斯威达建材科技有限公司 A kind of preparation method of foaming agent
WO2020124840A1 (en) * 2018-12-18 2020-06-25 武汉华星光电半导体显示技术有限公司 Substrate and display panel

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Open date: 20100901