CN101805156A - Steel slag radiation shield concrete and preparation method thereof - Google Patents

Steel slag radiation shield concrete and preparation method thereof Download PDF

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Publication number
CN101805156A
CN101805156A CN201010141289A CN201010141289A CN101805156A CN 101805156 A CN101805156 A CN 101805156A CN 201010141289 A CN201010141289 A CN 201010141289A CN 201010141289 A CN201010141289 A CN 201010141289A CN 101805156 A CN101805156 A CN 101805156A
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steel slag
radiation shield
slag sand
slag
shield concrete
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CN101805156B (en
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杨刚
王幼琴
金强
张健
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MCC Baosteel Technology Services Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/023Barium cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/06Aluminous cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/30Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing magnesium cements or similar cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/2038Resistance against physical degradation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention relates to a steel slag radiation shield concrete and a preparation method thereof. The steel slag radiation shield concrete comprises the following components in parts by weight: 1 part of cement, 0.4-0.5 part of water, 4-8 parts of steel slag sand, 0.01-0.03 part of water reducing agent, 0.01-2 parts of barite and 0.01-0.03 part of colemanite, wherein the steel slag sand comprises two kinds of steel slag sand with the particle size ranges of 0-5mm and 5-25mm according to the proportion of 1-3:1-3, and the f.CaO content of the steel slag sand is less than or equal to 3%; the water reducing agent is selected from an FDN water reducing agent and a polycarboxylate water reducing agent; and the apparent density of the steel slag radiation shield concrete is greater than 2900kg/m<3>. The steel slag radiation shield concrete of the invention has good compactness, large apparent density and high strength and meets the requirements of the radiation shield concrete; the invention changes waste steel slag into valuable resources, reduces the environment pollution, simultaneously lowers the consumption of mineral materials, and saves natural resources; and in addition, the steel slag used in the invention has abundant resources, low price and obvious economic benefit.

Description

A kind of steel slag radiation shield concrete and preparation method thereof
Technical field
The present invention relates to radiation shield concrete material field, more particularly, relating to a kind of is steel slag radiation shield concrete and preparation method thereof aggregate, that have shielding X ray, gamma-rays and neutron radiation effect with the slag.
Background technology
Radiation shield concrete is called shielding concrete, loaded concrete again, and it can effectively shield nuclear radiation.So-called nuclear radiation generally is meant alpha-ray, β ray, gamma-rays and neutron current.Because alpha-ray, β ray penetration power are lower, the protective material that thickness is very little also can block them fully, so the ray that radiation shield concrete will shield mainly is gamma-rays and neutron ray.The aggregate of common radiation shield concrete generally adopts mineral materials such as barite, magnetite, limonite, still, adopts these mineral materials to do to gather materials, easily emanate, the concrete construction poor performance, hydration heat of cement is big, concrete is easy to crack, poor durability, and the curing safe effect of nuke rubbish is poor; In addition, these mineral materials are natural resources in short supply, and excessive exploitation is unfavorable for Sustainable utilization of resources.On the other hand, along with the raising year by year of China's iron and steel output, the output of slag also increases thereupon, and a large amount of slags all need the big area soil to stack every year, all brings serious pollution for soil, water body, atmosphere etc., even people's health is constituted a threat to.In the international environment that is becoming tight energy day now, how to develop the high added value comprehensive Utilization Ways of solid waste, become the key that realizes iron and steel enterprise's cycle development.
Summary of the invention
The objective of the invention is to overcome deficiency of the prior art, a kind of steel slag radiation shield concrete and preparation method thereof is provided.
Know-why of the present invention is to utilize slag hardness height, manys micropore (the cement that passes through that can be more firm bonds than great, surperficial, increase compactness) characteristics, it is prepared the very fine and close superheavy concrete of structure as aggregate, to reach radiation-resistant effect.
Concrete technical scheme of the present invention is as follows:
A kind of steel slag radiation shield concrete, the parts by weight of its component are as follows: cement 1, water 0.4-0.5, slag sand 4-8, water reducer 0.01-0.03, barite 0.01-2, colemanite 0.01-0.03; Described slag sand by 0-5mm and two kinds of particle size range of 5-25mm in 1~3: 1~3 ratio is formed, and is preferably 1: 1, and f.CaO content≤3% of slag sand; Described water reducer is selected from FDN water reducer and polycarboxylate dehydragent; Described steel slag radiation shield concrete apparent density>2900kg/m 3
Described cement is selected from one or more of 42.5 ordinary Portland cements, high-alumina cement, barium cement, magnesia cement.
The ratio that the present invention adopts the slag sand of 0-5mm and two kinds of particle size range of 5-25mm preferably to adopt 1: 1 is carried out artificial grating, can farthest overcome the isolating problem of heavy aggregate, also have compactness, crushing resistance and water tolerance preferably when making the concrete that makes that high specific weight be arranged.
The preparation method of this steel slag radiation shield concrete comprises the steps:
(1) with slag crushing to 40mm, be the screen cloth of 25mm after the aperture, obtain the slag sand of particle diameter less than 25mm;
(2) particle diameter that obtains in the step (1) is crossed the screen cloth that the aperture is 5mm less than the slag sand of 25mm, obtaining particle size range is the coarse steel slag sand of 5-25mm and the thin slag sand that particle size range is 0-5mm;
(3) with the particle size range that obtains in the step (2) be the coarse steel slag sand of 5-25mm and thin slag sand that particle size range is 0-5mm and cement, water, water reducer, barite, colemanite mixed steel slag radiation shield concrete.
Among the preparation method of steel slag radiation shield concrete of the present invention, because the relative sandstone of slag proportion is big, when therefore preparing, the slag consumption of every dish (1 cube) is the 60-70% of normal concrete sandstone consumption, and the slump is controlled at 120 ± 20mm.
The invention has the beneficial effects as follows: (1) steel slag radiation shield concrete compactness of the present invention is good, and apparent density can reach 2900kg/m 3More than, strength grade is C10-C40, satisfies the requirement of different stage radiation shield concrete; (2) slag is turned waste into wealth, increase substantially its added value, also reduce slag simultaneously and throw aside pollution on the environment; (3) consumption of minimizing mineral material is saved natural resources; (4) slag is as the steel-making solid waste, aboundresources, cheap, and its relative heavy aggregate price has distinct economic still not as good as 1/10.
Embodiment
To dispose 1 cube of steel slag radiation shield concrete is example, carries out following three embodiment, and preparation process is carried out as follows:
(1) with slag crushing to 40mm, be the screen cloth of 25mm after the aperture, obtain the slag sand of particle diameter less than 25mm;
(2) particle diameter that obtains in the step (1) is crossed the screen cloth that the aperture is 5mm less than the slag sand of 25mm, obtaining particle size range is the coarse steel slag sand of 5-25mm and the thin slag sand that particle size range is 0-5mm;
(3) be that the coarse steel slag sand of 5-25mm and thin slag sand and cement, water, water reducer, barite, colemanite that particle size range is 0-5mm make steel slag radiation shield concrete by listed mixed in the table 1 with the particle size range that obtains in the step (2).
Material therefor and proportioning in the example 1~3 are executed in table 1 expression.
Table 1 proportioning raw materials
Material component Embodiment 1 (weight part) Embodiment 2 (weight part) Embodiment 3 (weight part)
Cement ??1 ??1 ??1
Water ??0.4 ??0.45 ??0.5
Thin slag sand 0-5mm ??4 ??3 ??2
Coarse steel slag sand 5-25mm ??4 ??3 ??2
Barite ??0.01 ??1 ??2
Water reducer ??0.01 ??0.02 ??0.03
Material component Embodiment 1 (weight part) Embodiment 2 (weight part) Embodiment 3 (weight part)
Colemanite ??0.03 ??0.02 ??0.01
The performance perameter of the product that each embodiment of table 2 expression makes comprises indexs such as apparent density, ultimate compression strength, folding strength.
Table 2 product performance index
Processing parameter Apparent density>2900kg/m 3 28 days ultimate compression strength (MPa) 28 days folding strengths (MPa)
Embodiment 1 ??2989 ??34.5 ??5.6
Embodiment 2 ??3225 ??33.9 ??5.5
Embodiment 3 ??3677 ??31.2 ??4.8
As can be seen from Table 2, steel slag radiation shield concrete apparent density of the present invention can reach 2900kg/m 3More than, strength grade is C10-C40, can satisfy the requirement of different stage radiation shield concrete.
Embodiment 4
Adopt the set of dispense ratio as table 3 expression to carry out 5 groups of optimization Test, preparation process is the same.
Thin slag sand is meant that particle size range is the slag sand of 0-5mm in the table 3, and coarse steel slag sand is meant that particle size range is the slag sand of 5-25mm.
Table 3 test composition of raw materials
Figure GSA00000074576300041
Every index of the radiation shield concrete that makes in 5 groups of tests of table 4 expression comprises projects such as apparent density, ultimate compression strength, folding strength.
Table 4 trial production contrast
Numbering Thickness slag sand grains footpath Thickness slag sand ratio Apparent density>2900kg/m 3 28 days ultimate compression strength (MPa) 28 days folding strengths (MPa)
??1# ??5-25mm/0-5mm ??1∶1 ??3599 ??41.5 ??6.7
??2# ??5-25mm/0-5mm ??1∶2 ??3567 ??37.8 ??5.2
??3# ??5-25mm/0-5mm ??1∶3 ??3543 ??34.0 ??5.4
??4# ??5-25mm/0-5mm ??2∶1 ??3218 ??39.3 ??5.9
??5# ??5-25mm/0-5mm ??3∶1 ??3075 ??37.7 ??5.0
As can be seen from Table 4, the every index effect of the radiation shield concrete optimum that the slag sand of 0-5mm and two kinds of particle size range of 5-25mm makes by 1: 1 proportioning, therefore, the present invention is in preparation during radiation shield concrete, and the ratio that preferably adopted 1: 1 is carried out proportioning to the slag sand of 0-5mm and two kinds of particle size range of 5-25mm.
Embodiment 5
Adopt the set of dispense ratio as table 5 expression to carry out 4 groups of simultaneous tests, preparation process is carried out as follows:
(1) with slag crushing to 40mm, be the screen cloth of 35mm after the aperture, obtain particle size range and be the slag sand of 35-40mm and particle diameter slag sand less than 35mm;
(2) particle diameter that obtains in the step (1) is crossed the screen cloth that the aperture is 30mm less than the slag sand of 35mm, obtain particle size range and be the slag sand of 30-35mm and particle diameter slag sand less than 30mm;
(3) particle diameter that obtains in the step (2) is crossed the screen cloth that the aperture is 25mm less than the slag sand of 30mm, obtain particle size range and be the slag sand of 25-30mm and particle diameter slag sand less than 25mm;
(4) particle diameter that obtains in the step (3) is crossed the screen cloth that the aperture is 5mm less than the slag sand of 25mm, obtaining particle size range is the slag sand of 5-25mm and the slag sand that particle size range is 0-5mm;
(5) be that the coarse steel slag sand of 35-40mm, 30-35mm, 25-30mm, 5-25mm carried out proportioning with the thin slag sand of 0-5mm by 1: 1 respectively with the particle size range that obtains in above each step, and then make four set products with cement, water, water reducer, barite, colemanite by listed mixed in the table 5 respectively.
Thin slag sand is meant that particle size range is the slag sand of 0-5mm in the table 5, and coarse steel slag sand is meant that particle size range is four kinds of slag sand of 35-40mm, 30-35mm, 25-30mm, 5-25mm.
Table 5 test composition of raw materials
Figure GSA00000074576300051
Every index of 4 groups of products that make of table 6 expression, comprise projects such as apparent density, ultimate compression strength, folding strength, as can be seen from Table 6, the slag sand that adopts 5-25mm and two kinds of particle size range of 0-5mm is more excellent by the product effect that 1: 1 proportioning makes, and satisfies the requirement of radiation shield concrete; And adopt particle size range is that the slag sand of 35-40mm, 30-35mm, 25-30mm and slag sand that particle size range is 0-5mm carry out proportioning, though ratio is 1: 1, but prepared product all can not reach the requirement of radiation shield concrete, and the present invention serves as preferred with the slag sand of 5-25mm and two kinds of particle size range of 0-5mm by 1: 1 proportioning thus.
Table 6 trial production contrast
Numbering Thickness slag sand grains footpath Thickness slag sand ratio Apparent density 28 days ultimate compression strength (MPa) 28 days folding strengths (MPa)
??1# ??5-25mm/0-5mm ??1∶1 ??3008 ??34.9 ??5.3
??2# ??25-30mm/0-5mm ??1∶1 ??2420 ??26.2 ??4.3
??3# ??30-35mm/0-5mm ??1∶1 ??2219 ??26.1 ??4.4
??4# ??35-40mm/0-5mm ??1∶1 ??2318 ??24.9 ??4.3

Claims (3)

1. steel slag radiation shield concrete, the parts by weight of its component are as follows: cement 1, water 0.4-0.5, slag sand 4-8, water reducer 0.01-0.03, barite 0.01-2, colemanite 0.01-0.03; Described slag sand by 0-5mm and two kinds of particle size range of 5-25mm in 1~3: 1~3 ratio is formed, and f.CaO content≤3% of slag sand; Described water reducer is selected from FDN water reducer and polycarboxylate dehydragent; Described steel slag radiation shield concrete apparent density>2900kg/m 3
2. steel slag radiation shield concrete according to claim 1 is characterized in that, described cement is selected from one or more of 42.5 ordinary Portland cements, high-alumina cement, barium cement, magnesia cement.
3. the preparation method of claim 1 or 2 described steel slag radiation shield concretes is characterized in that, comprise the steps: (1) with slag crushing to 40mm, be the screen cloth of 25mm after the aperture, obtain the slag sand of particle diameter less than 25mm;
(2) particle diameter that obtains in the step (1) is crossed the screen cloth that the aperture is 5mm less than the slag sand of 25mm, obtaining particle size range is the coarse steel slag sand of 5-25mm and the thin slag sand that particle size range is 0-5mm;
(3) with the particle size range that obtains in the step (2) be the coarse steel slag sand of 5-25mm and thin slag sand that particle size range is 0-5mm and cement, water, water reducer, barite, colemanite mixed steel slag radiation shield concrete.
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Cited By (24)

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Publication number Priority date Publication date Assignee Title
CN101921094A (en) * 2010-08-30 2010-12-22 武汉海剑工贸有限责任公司 High-iron ground steel slag lightweight high-toughness wave absorption concrete and preparation method thereof
CN102219459A (en) * 2011-04-02 2011-10-19 武汉理工大学 Radiation shield concrete and preparation method thereof
CN102432246A (en) * 2011-09-16 2012-05-02 上海浦莲预拌混凝土有限公司 Anti-radiation anticorrosion concrete and its preparation method
CN102701645A (en) * 2011-03-28 2012-10-03 中冶宝钢技术服务有限公司 Cement-based steel slag granite product and preparation method thereof
CN102733607A (en) * 2012-05-18 2012-10-17 山东起凤建工股份有限公司 Method for preparing high-density concrete with uniform aggregate and aggregate thereof
CN103601452A (en) * 2013-10-19 2014-02-26 宿州典跃新型建筑材料有限公司 Radiation-resistant dry-mixed mortar and manufacturing method thereof
EP3095769A1 (en) * 2015-05-22 2016-11-23 Arraela, S.L. Mass preparation for the manufacture of technical concretes for shielding against radiation and method to obtain said preparation
CN107089813A (en) * 2017-03-25 2017-08-25 杭州科安辐射防护工程有限公司 A kind of radiation-proof plate
CN107352945A (en) * 2017-08-30 2017-11-17 北京军秀咨询有限公司 A kind of thermal insulation concrete of radiation proof anticracking
CN108424017A (en) * 2018-04-03 2018-08-21 济南大学 A kind of radiation shield concrete active aggregates and preparation method thereof
CN108894544A (en) * 2018-06-19 2018-11-27 隆生国际建设集团有限公司 A kind of baryte radiation protection therapeutic room and its construction method
CN109053093A (en) * 2018-10-16 2018-12-21 成都宏基建材股份有限公司 A kind of ungauged regions micro-expansion cement base radiation shield concrete and preparation method thereof
CN109133803A (en) * 2018-10-16 2019-01-04 成都宏基建材股份有限公司 A kind of C40 ordinary portland cement base radiation shield concrete and preparation method thereof
CN109231931A (en) * 2018-10-16 2019-01-18 成都宏基建材股份有限公司 A kind of aluminous cement base radiation shield concrete and preparation method thereof
CN109231920A (en) * 2018-10-16 2019-01-18 成都宏基建材股份有限公司 A kind of C20 ordinary portland cement base radiation shield concrete and preparation method thereof
CN109231933A (en) * 2018-10-16 2019-01-18 成都宏基建材股份有限公司 A kind of radiation shield concrete and preparation method thereof
CN109231932A (en) * 2018-10-16 2019-01-18 成都宏基建材股份有限公司 A kind of barium aluminate cement base radiation shield concrete and preparation method thereof
CN109231934A (en) * 2018-10-16 2019-01-18 成都宏基建材股份有限公司 A kind of fast calcium sulphoaluminate cement base radiation shield concrete and preparation method thereof firmly
CN109320172A (en) * 2018-10-16 2019-02-12 成都宏基建材股份有限公司 A kind of quick setting and rapid hardening calcium aluminum fluoride cement base radiation shield concrete and preparation method thereof
CN109320159A (en) * 2018-10-16 2019-02-12 成都宏基建材股份有限公司 A kind of low heat micro expanding cement base radiation shield concrete and preparation method thereof
CN109336496A (en) * 2018-10-16 2019-02-15 成都宏基建材股份有限公司 A kind of ordinary portland cement base radiation shield concrete and preparation method thereof
CN113213845A (en) * 2021-05-17 2021-08-06 广西路建工程集团有限公司 Environment-friendly C30 cement concrete and preparation method thereof
CN113754341A (en) * 2021-09-24 2021-12-07 上海中冶环境工程科技有限公司 Modifier for concrete, counterweight concrete, preparation method and application thereof
CN117263613A (en) * 2023-09-22 2023-12-22 邯郸市盛建新型建材股份有限公司 Concrete based on solid waste material and preparation method thereof

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CN101921094B (en) * 2010-08-30 2012-08-29 武汉海剑工贸有限责任公司 High-iron ground steel slag lightweight high-toughness wave absorption concrete and preparation method thereof
CN101921094A (en) * 2010-08-30 2010-12-22 武汉海剑工贸有限责任公司 High-iron ground steel slag lightweight high-toughness wave absorption concrete and preparation method thereof
CN102701645A (en) * 2011-03-28 2012-10-03 中冶宝钢技术服务有限公司 Cement-based steel slag granite product and preparation method thereof
CN102219459A (en) * 2011-04-02 2011-10-19 武汉理工大学 Radiation shield concrete and preparation method thereof
CN102432246A (en) * 2011-09-16 2012-05-02 上海浦莲预拌混凝土有限公司 Anti-radiation anticorrosion concrete and its preparation method
CN102733607B (en) * 2012-05-18 2015-01-21 山东起凤建工股份有限公司 Method for preparing high-density concrete with uniform aggregate and aggregate thereof
CN102733607A (en) * 2012-05-18 2012-10-17 山东起凤建工股份有限公司 Method for preparing high-density concrete with uniform aggregate and aggregate thereof
CN103601452B (en) * 2013-10-19 2015-11-18 宿州典跃新型建筑材料有限公司 A kind of radioprotective dry-mix and preparation method thereof
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EP3095769A1 (en) * 2015-05-22 2016-11-23 Arraela, S.L. Mass preparation for the manufacture of technical concretes for shielding against radiation and method to obtain said preparation
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