CN101780353A - Micropore ceramic filter element and preparation method thereof - Google Patents
Micropore ceramic filter element and preparation method thereof Download PDFInfo
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- CN101780353A CN101780353A CN200910036782A CN200910036782A CN101780353A CN 101780353 A CN101780353 A CN 101780353A CN 200910036782 A CN200910036782 A CN 200910036782A CN 200910036782 A CN200910036782 A CN 200910036782A CN 101780353 A CN101780353 A CN 101780353A
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Abstract
The invention relates to a micropore ceramic filter element, in particular to a micropore ceramic filter element and a preparation method thereof. In the process of preparing the micropore ceramic filter element, raw materials are weighed according to the percentage in the formula, are added, mixed and uniformly stirred according to specified steps, and then are extruded or punched by an extruder or a punching machine into a blank, then the blank is dried at certain temperature to be shaped, and then the polyporous micropore ceramic filter element is formed. The micropore ceramic filter element is made of kaolin and diatomaceous earth which are bonded by a water-based adhesive, and has the advantages of low manufacturing cost, safety and environment protection. Simultaneously, the blank is molded by extrusion or punching, so cumbersome technology in the grouting process is eliminated, only moisture in the blank needs to be removed in the molding process, the existing energy-consuming process of long-time high-temperature calcination is avoided, and the production cost is greatly reduced.
Description
Skill this area
The present invention relates to a kind of candle, particularly relate to a kind of micropore ceramic filter element and preparation method thereof.
Background technology
At present, the preparation method of the ceramic element that purifying drinking water is used mainly is that kaolin, diatomite are through abrasive dust, add water pugging pulping, slurry is injected in the good mould of prepared beforehand makes idiosome, again the moisture in the idiosome is carried out drying, and then the idiosome of drying sent in the above high temperature furnace of 700 degree calcine moulding.This production technology not only production process is loaded down with trivial details, produce to drop into greatlyyer, and calcination process also is the process of a high energy consumption, causes the finished product production cost high always.
Summary of the invention
The present invention is in order to solve some loaded down with trivial details operating process and the expensive production cost that exists in the above-mentioned production process, a kind of new micropore ceramic filter element and preparation method thereof is provided, especially a kind of with water base adhesive as binding agent, method with extruding or punching press is made embryo fast, the moisture typing under cryogenic conditions in the oven dry idiosome.This micropore ceramic filter element production efficiency height, production cost is low, and the composition after the glue dries is silica, and composition is identical with diatomite or kaolinic composition, do not change the character of original ceramic element, simultaneously cheap, the safety of the cost of manufacture of water accack, environmental protection.
An object of the present invention is to provide a kind of micropore ceramic filter element.
Another object of the present invention provides the preparation method of described micropore ceramic filter element.
The objective of the invention is to be achieved through the following technical solutions:
A kind of preparation method of micropore ceramic filter element, it is formed by the feedstock production that comprises following mass percent;
Filter raw material 10-90 binding agent 10-90 plasticizer 1-30 curing agent 0.05-15
Preferably, a kind of preparation method of micropore ceramic filter element, it is formed by the feedstock production that comprises following mass percent;
Filter raw material 25-75 binding agent 30-70 plasticizer 5-20 curing agent 0.1-5
More preferably, a kind of preparation method of micropore ceramic filter element, it is formed by the feedstock production that comprises following mass percent;
Filter raw material 43 binding agents 38 plasticizer 18 curing agent 1
Filtration raw material described in the present invention are that making potteries such as kaolin, diatomite are used raw material, and its order number is greater than 30 orders.Binding agent described in the present invention is a Ludox, and the active ingredient dioxide-containing silica is between the 5%-60%, and preferred active ingredient dioxide-containing silica is 40%, and it is silica that Ludox solidifies the back main component, and is identical with kaolin, diatomaceous composition.Plasticizer described in the present invention is 0.1-15% polyvinyl alcohol water solution or 0.1-5% sodium carboxymethyl cellulose solution, preferred 10% polyvinyl alcohol water solution, be insoluble to cold water after polyvinyl alcohol solidifies, and prevent in solidification process that filter core local heating is uneven and ftracture.
Curing agent described in the present invention is food carbonic hydroammonium, sodium acid carbonate, sodium carbonate, is used to improve the gelation rate of Ludox, is convenient to the stable of formed product, preferred food product carbonic hydroammonium.
The preparation method of a kind of micropore ceramic filter element of the present invention, it may further comprise the steps;
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture of drying at a certain temperature in the idiosome is finalized the design again, promptly becomes the micropore ceramic filter element with regulation shape of porous.The preparation method's of a kind of micropore ceramic filter element of the present invention solidification temperature is as the criterion to be no more than 200 degree, and be as the criterion less than 1% with the moisture of drying to the type body hardening time.
The preparation method of a kind of micropore ceramic filter element of the present invention utilizes ceramic raw material and inorganic water-based adhesive to be made, and has production cost and drops into lowly, and production efficiency height and cost of manufacture are cheap, safety, environmental protection two big technical characterstics.(1) low, the production efficiency of production cost is high do not need in the production process to refer to high-temperature calcination equipment and numerous grouting moulds, has removed the huge energy consumption in the production process from.The system embryo is with pushing or the pressing equipment rapid shaping, and solidification process only needs the moisture in the drying-type body to get final product, and has removed loaded down with trivial details grouting process from and this process of calcining and heat up slowly, lower the temperature for a long time.(2) the water accack cost of manufacture is low, raw material sources extensively and production process safety, environmental protection, there is not the discharging of refuse and danger, and discarded filtrate is lost in environment and environment is not produced any influence, solidification temperature is no more than 200 degree simultaneously, belong to low-temperature setting, both reduced industrial cost, meet the production requirement of industrial energy saving again.
The specific embodiment
Following examples are in order further to describe the present invention for example, rather than limit the present invention by any way.
Embodiment 1
Diatomite (greater than 60 orders) 30 kaolin, 10 Ludox (30% dioxide-containing silica) 35
10% content polyvinyl alcohol water solution, 24 carbonic hydroammonium 1
Its preparation method is as follows:
Take by weighing each raw material by formula ratio percentage, operating procedure is as follows:
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture of drying at a certain temperature in the idiosome is finalized the design again, promptly becomes the micropore ceramic filter element with regulation shape of porous.
Embodiment 2
Diatomite (greater than 100 orders) 25 kaolin, 20 Ludox (40% dioxide-containing silica) 40
10% content polyvinyl alcohol water solution, 14 carbonic hydroammonium 1
Its preparation method is as follows:
Take by weighing each raw material by formula ratio percentage, operating procedure is as follows:
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture in the drying-type body is finalized the design at a certain temperature again, promptly becomes the micropore ceramic filter element with regulation shape of porous.
Embodiment 3
Diatomite (greater than 100 orders) 35 kaolin, 10 Ludox (40% dioxide-containing silica) 40
2% content sodium carboxymethyl cellulose solution, 12 sodium acid carbonates 3
Its preparation method is as follows:
Take by weighing each raw material by formula ratio percentage, operating procedure is as follows:
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture in the drying-type body is finalized the design at a certain temperature again, promptly becomes the micropore ceramic filter element with regulation shape of porous.
Embodiment 4
Diatomite (greater than 200 orders) 45 Ludox (30% dioxide-containing silica) 40
10% content polyvinyl alcohol water solution, 14 carbonic hydroammonium 1
Its preparation method is as follows:
Take by weighing each raw material by formula ratio percentage, operating procedure is as follows:
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture in the drying-type body is finalized the design at a certain temperature again, promptly becomes the micropore ceramic filter element with regulation shape of porous.
Claims (9)
1. micropore ceramic filter element, it is by comprising that following raw materials by weight percent is prepared from;
Filter raw material 10-90 binding agent 10-90 plasticizer 1-30 curing agent 0.05-15
2. a kind of micropore ceramic filter element according to claim 1, it is by comprising that following raw materials by weight percent is prepared from;
Filter raw material 25-75 binding agent 30-70 plasticizer 5-20 curing agent 0.1-5
3. a kind of micropore ceramic filter element according to claim 2, it is by comprising that following raw materials by weight percent is prepared from;
Filter raw material 43 binding agents 38 plasticizer 18 curing agent 1
4. a kind of micropore ceramic filter element according to claim 1, wherein said filtration raw material are mixing of one or more materials in the ceramic raw materials such as diatomite, kaolin, its order number is greater than 30 orders.
5. a kind of micropore ceramic filter element according to claim 4, wherein said binding agent is Ludox, waterglass etc., wherein the content of silica is between 5-60%.
6. a kind of micropore ceramic filter element according to claim 5, wherein said plasticizer are wherein one or more such as polyvinyl alcohol, sodium carboxymethylcellulose, modified starch.
7. a kind of micropore ceramic filter element according to claim 6, wherein said curing agent are wherein one or more such as carbonic hydroammonium, sodium carbonate, sodium acid carbonate, ammoniacal liquor.
8. the preparation method of a kind of micropore ceramic filter element according to claim 1, it may further comprise the steps;
1. take by weighing each raw material by formula ratio percentage.
2. with binding agent and plasticizer mixing and stirring.
3. curing agent is joined mixing and stirring in the raw material that 2. step mixed.
4. the raw material that step is mixed in 3. joins immediately and filters mixing and stirring in the raw material.
5. the raw material that step is mixed in is 4. put into prepared beforehand good mould is pushed or strike out embryo, and the moisture of drying at a certain temperature in the idiosome is finalized the design again, promptly becomes the micropore ceramic filter element with regulation shape of porous.
9. the preparation method of a kind of micropore ceramic filter element according to claim 8, wherein said baking temperature is as the criterion not damage the physicochemical property of filtering raw material and binding agent in the body, and stoving time is as the criterion less than 1% with the moisture in the type body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN200910036782A CN101780353A (en) | 2009-01-19 | 2009-01-19 | Micropore ceramic filter element and preparation method thereof |
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| CN200910036782A CN101780353A (en) | 2009-01-19 | 2009-01-19 | Micropore ceramic filter element and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101948301A (en) * | 2010-08-26 | 2011-01-19 | 东莞乔隆家具配件制品有限公司 | Diatomite ceramic filter and manufacture method thereof |
| CN102153337A (en) * | 2010-12-30 | 2011-08-17 | 东莞荃祥陶瓷原料有限公司 | Environment-friendly ceramic material and preparation method thereof |
| CN103382127A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Composite ceramic filter core and preparation method thereof |
| CN103382120A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Porous ceramic filter core and preparation method thereof |
| CN103382125A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Diatomite ceramic filter core and preparation method thereof |
| CN103382119A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Rare earth oxide ceramic filter core and preparation method thereof |
| CN104003754A (en) * | 2014-05-26 | 2014-08-27 | 芜湖市华泰实业有限公司 | Ultralight porous ceramic water-purification filter element material and manufacturing method thereof |
| CN104016705A (en) * | 2014-06-17 | 2014-09-03 | 深圳市智瓷科技有限公司 | Preparation method of environment-friendly ceramic filter element |
| CN105294053A (en) * | 2015-10-26 | 2016-02-03 | 郭任彬 | Ceramic floor drain and manufacturing method thereof |
| CN105854415A (en) * | 2016-04-20 | 2016-08-17 | 潘能红 | Compound sintered filtering core for water purifier and preparing method of compound sintered filtering core |
| CN107398125A (en) * | 2017-06-29 | 2017-11-28 | 无锡市京锡冶金液压机电有限公司 | A kind of Production of Ceramics filter |
-
2009
- 2009-01-19 CN CN200910036782A patent/CN101780353A/en active Pending
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101948301A (en) * | 2010-08-26 | 2011-01-19 | 东莞乔隆家具配件制品有限公司 | Diatomite ceramic filter and manufacture method thereof |
| CN102153337A (en) * | 2010-12-30 | 2011-08-17 | 东莞荃祥陶瓷原料有限公司 | Environment-friendly ceramic material and preparation method thereof |
| CN102153337B (en) * | 2010-12-30 | 2013-07-17 | 东莞荃祥陶瓷原料有限公司 | Environment-friendly ceramic material and preparation method thereof |
| CN103382125A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Diatomite ceramic filter core and preparation method thereof |
| CN103382127A (en) * | 2013-06-25 | 2013-11-06 | 蚌埠凤凰滤清器有限责任公司 | Composite ceramic filter core and preparation method thereof |
| CN103382119A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Rare earth oxide ceramic filter core and preparation method thereof |
| CN103382120A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠德美过滤技术有限公司 | Porous ceramic filter core and preparation method thereof |
| CN103382119B (en) * | 2013-06-26 | 2014-11-26 | 蚌埠德美过滤技术有限公司 | Rare earth oxide ceramic filter core and preparation method thereof |
| CN104003754A (en) * | 2014-05-26 | 2014-08-27 | 芜湖市华泰实业有限公司 | Ultralight porous ceramic water-purification filter element material and manufacturing method thereof |
| CN104016705A (en) * | 2014-06-17 | 2014-09-03 | 深圳市智瓷科技有限公司 | Preparation method of environment-friendly ceramic filter element |
| CN105294053A (en) * | 2015-10-26 | 2016-02-03 | 郭任彬 | Ceramic floor drain and manufacturing method thereof |
| CN105854415A (en) * | 2016-04-20 | 2016-08-17 | 潘能红 | Compound sintered filtering core for water purifier and preparing method of compound sintered filtering core |
| CN107398125A (en) * | 2017-06-29 | 2017-11-28 | 无锡市京锡冶金液压机电有限公司 | A kind of Production of Ceramics filter |
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Application publication date: 20100721 |