CN101768476A - 一种工业炉用清洁醇基燃料 - Google Patents

一种工业炉用清洁醇基燃料 Download PDF

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CN101768476A
CN101768476A CN201010107348A CN201010107348A CN101768476A CN 101768476 A CN101768476 A CN 101768476A CN 201010107348 A CN201010107348 A CN 201010107348A CN 201010107348 A CN201010107348 A CN 201010107348A CN 101768476 A CN101768476 A CN 101768476A
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李超平
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SHANGHAI SHUNTIAN CHEMISTERY TECHNOLOGY Co Ltd
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Abstract

本发明公开了一种工业炉用清洁醇基燃料，其组成配方如下：甲醇30～80％、酯化植物油18～65％、增氧剂0.5～3％、热值增加剂0.5～2％、消烟节能剂0.1～0.5％、金属腐蚀抑制剂0.01～0.05％；所述酯化植物油是以植物油脚料为原料，经过提取其中的酸油，再由酸油经常压快速水解制取混合脂肪酸，再依次经酯化、蒸馏、再酯化制得。本发明的工业炉用醇基燃料不仅具有点火迅速、火力强、热值高的优点，还具有燃烧完全、燃烧时无烟无毒、制备工艺简单、操作安全、生产成本低等优势，解决了工业炉用燃料对石油资源的依赖和植物油脚料等废弃物所产生的资源浪费和环境污染问题，具有显著的市场和经济效益。

Description

一种工业炉用清洁醇基燃料
技术领域
本发明涉及一种工业炉用清洁醇基燃料，属于醇基燃料技术领域。
背景技术
目前，各种工业炉用燃料主要是柴油，而柴油来源于石油，不仅存在价格高、供应趋紧等问题，还存在燃烧后产生的黑烟较多，对环境污染严重的缺陷。
而当今世界，能源和环境是影响全球经济社会可持续发展的主要因素，随着世界经济的高速发展，对石油的需求量也在不断增加，随着石油储量的减少和对环保要求的越来越严格，寻求柴油的代用燃料受到广泛的关注。众所周知，我国的国情是缺油、少气、相对富煤，而替代能源的首要条件必须具备两大要素：一是储量大，二是燃烧洁净。由于我国有着丰富的闲弃少用的高硫煤及储量丰富的煤层气和炼焦炭的副产品焦炉气，可利用它们制成甲醇。另外，我国油料作物总产量居世界前列，在植物油加工过程中，会产生大量的脚料，以往只作肥料使用，对脚料中有用的成分没有合理利用，不仅造成资源的浪费，而且脚料易变质发臭，严重污染环境。若能有效利用这些脚料资源，不仅可解决因其造成的环境污染问题，还能减少资源的浪费，具有重要的经济效益和社会效益。中国专利CN90106762虽然公开了一种利用植物油脚料制备燃料甲酯的技术，但该技术所制得的甲酯燃料的性能仅相当于0号柴油，燃烧产生的环境污染问题仍很严重。
发明内容
本发明针对上述现有技术所存在的缺陷和市场需求，提供一种能替代柴油，且具有原料来源广、成本低、清洁环保优点的工业炉用醇基燃料。
为实现上述发明目的，本发明采用的技术方案如下：
本发明提供的工业炉用清洁醇基燃料，其组成及各组成的重量百分比如下：
甲醇                  30～80％
酯化植物油            18～65％
增氧剂                0.5～3％
热值增加剂            0.5～2％
消烟节能剂            0.1～0.5％
金属腐蚀抑制剂        0.01～0.05％
上述各组成的重量百分比之和为100％；所述酯化植物油是以植物油脚料为原料，经过提取其中的酸油，再由酸油经常压快速水解制取混合脂肪酸，再依次经酯化、蒸馏、再酯化制得。
所述植物油脚料是指油菜籽、米糠、棉籽、大豆、花生及向日葵中的一种或几种在精炼加工中产生的油脚料。
所述增氧剂可选自双氧水或高锰酸钾，优选双氧水。
所述热值增加剂可选自丙酮或石油醚，优选丙酮。
所述消烟节能剂可选自植酸盐，优选植酸钙。
所述金属腐蚀抑制剂可选自三乙醇胺。
本发明所述的工业炉用清洁醇基燃料的制备，是首先按照中国专利文献CN90106762所述方法制备酯化植物油，再按配比将增氧剂、热值增加剂、消烟节能剂及金属腐蚀抑制剂加入酯化植物油中，在室温下搅拌均匀后，再加入甲醇，在室温下继续搅拌均匀即可。
与现有技术相比，本发明的有益效果如下：
1、由于本发明的工业炉用醇基燃料所用的主原料：甲醇可由闲弃少用的高硫煤及储量丰富的煤层气和炼焦炭的副产品焦炉气制备而得，所用的酯化植物油是利用植物油脚料为原料制备而得，因此，本发明不仅存在原料来源广泛、成本低廉的优势，而且解决了上述废弃物所产生的资源浪费和环境污染问题，最大程度的解决了工业炉用醇基燃料对石油资源的依赖。
2、本发明配方所制得的工业炉用醇基燃料，不仅具有点火迅速、火力强、热值高，热值可高达6500～7500千卡/小时，中心火焰温度达1200℃的优点，还具有燃烧完全、燃烧时无烟、无毒等优点，属于清洁环保能源。
3、本发明燃料制备工艺简单，操作安全，无需特殊设备，生产成本低，适合规模化生产和推广应用，具有显著的市场和经济效益。
具体实施方式
下面通过实施例对本发明作进一步说明，其目的仅在于更好理解本发明的内容而非限制本发明的保护范围：
实施例1
本实施例的工业炉用清洁醇基燃料，其组成配方如下：
甲醇                      30重量份
酯化植物油                65重量份
增氧剂                    3重量份
热值增加剂                1.8重量份
消烟节能剂                0.15重量份
金属腐蚀抑制剂            0.05重量份
所述酯化植物油是以植物油脚料为原料，经过提取其中的酸油，再由酸油经常压快速水解制取混合脂肪酸，再依次经酯化、蒸馏、再酯化制得；所述植物油脚料是指油菜籽、米糠、棉籽、大豆、花生及向日葵中的一种或几种在精炼加工中产生的油脚料。
所述增氧剂可选自双氧水或高锰酸钾，优选双氧水。
所述热值增加剂可选自丙酮或石油醚，优选丙酮。
所述消烟节能剂可选自植酸盐，优选植酸钙。
所述金属腐蚀抑制剂可选自三乙醇胺。
所述的工业炉用清洁醇基燃料的制备，是首先按照中国专利文献CN90106762所述方法制备酯化植物油，再按配比将增氧剂、热值增加剂、消烟节能剂及金属腐蚀抑制剂加入酯化植物油中，在室温下搅拌均匀后，再加入甲醇，在室温下继续搅拌均匀即可。
实施例2
本实施例的工业炉用清洁醇基燃料，其组成配方如下：
甲醇                      55重量份
酯化植物油                42重量份
增氧剂                    1.7重量份
热值增加剂                1.0重量份
消烟节能剂                0.27重量份
金属腐蚀抑制剂            0.03重量份，
其它内容同实施例1中所述。
实施例3
本实施例的工业炉用清洁醇基燃料，其组成配方如下：
甲醇                      80重量份
酯化植物油                18重量份
增氧剂                    1.0重量份
热值增加剂                0.5重量份
消烟节能剂                0.49重量份
金属腐蚀抑制剂            0.01重量份，
其它内容同实施例1中所述。
将上述实施例所制得的醇基燃料抽样进行理化性能检测，检测结果见表1所示：
表1理化性能检测结果
  检测项目名称   单位   技术要求   检测结果
  密度(20℃)   g/cm3   ≤0.83   0.80
  低热值   KJ/kg   ≥21000   32000
  硫含量(％)   ＜0.01   0.003
  引燃温度   ℃   ＞200   380
  凝点   ℃   ＜0   -48
  pH值   6～8   6.5
  稳定性(-20℃)   不分层   不分层
由表1可见：本发明的醇基燃料的理化性能优于现有普通柴油的性能技术指标，完全可替代现有普通柴油作为工业炉用燃料。
将本发明的醇基燃料的燃烧尾气进行测定，测定结果如表2所示；
表2本发明燃料燃烧尾气测定结果(毫克/万立方米)
  取样时间   CO   CH3OH   HCHO   NOX
  本底   1.83   未检出   未检出   未检出
  60分钟   6.50   0.83   0.005   0.01
  120分钟  7.80   0.65   0.01   0.02
  熄火后30分钟  4.30   0.35   未检出   未检出
  国家标准  ＜10   ＜3   ＜0.1   ＜0.15
  检测标准  TJ36-79   TJ36-79   GP670-88   TJ36-79
由表2可见，本发明的醇基燃料燃烧后的排放符合国家标准，属于高清洁环保能源，完全可以替代现有普通柴油作为工业炉用燃料使用。

Claims (9)

1.一种工业炉用清洁醇基燃料，其特征在于，其组成及各组成的重量百分比如下：
甲醇              30～80％
酯化植物油        18～65％
增氧剂            0.5～3％
热值增加剂        0.5～2％
消烟节能剂        0.1～0.5％
金属腐蚀抑制剂    0.01～0.05％
上述各组成的重量百分比之和为100％；所述酯化植物油是以植物油脚料为原料，经过提取其中的酸油，再由酸油经常压快速水解制取混合脂肪酸，再依次经酯化、蒸馏、再酯化制得。
2.根据权利要求1所述的工业炉用清洁醇基燃料，其特征在于，所述植物油脚料是指油菜籽、米糠、棉籽、大豆、花生及向日葵中的一种或几种在精炼加工中产生的油脚料。
3.根据权利要求1所述的工业炉用清洁醇基燃料，其特征在于，所述增氧剂为双氧水或高锰酸钾。
4.根据权利要求3所述的工业炉用清洁醇基燃料，其特征在于，所述增氧剂为双氧水。
5.根据权利要求1所述的工业炉用清洁醇基燃料，其特征在于，所述热值增加剂为丙酮或石油醚。
6.根据权利要求5所述的工业炉用清洁醇基燃料，其特征在于，所述热值增加剂为丙酮。
7.根据权利要求1所述的工业炉用清洁醇基燃料，其特征在于，所述消烟节能剂为植酸盐。
8.根据权利要求7所述的工业炉用清洁醇基燃料，其特征在于，所述消烟节能剂为植酸钙。
9.根据权利要求1所述的工业炉用清洁醇基燃料，其特征在于，所述金属腐蚀抑制剂为三乙醇胺。
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ITRM20110317A1 (it) * 2011-06-17 2012-12-18 Enea Floris Processo metodo e formulazioni per la produzione di un biocarburante a base di olii di natura vegetale anche esausti rigenerati e/o geneticamente modificati alghe e microalghe e/o olii da esse derivati addizionati ad alcoli primari e/o secondari e/o
CN103343964A (zh) * 2013-07-10 2013-10-09 宋贵中 使用醇基清洁燃料大幅提高工业炉窑热效率的燃烧方法
WO2015003300A1 (zh) * 2013-07-08 2015-01-15 Song Guizhong 使用醇基清洁燃料大幅提高工业炉窑热效率的燃烧方法
CN106675668A (zh) * 2016-12-09 2017-05-17 广西北海浩邦新能源科技有限公司 一种可再生醇基环保燃料
CN106675669A (zh) * 2016-12-09 2017-05-17 广西北海浩邦新能源科技有限公司 可再生醇基环保燃料的制备方法
CN111778073A (zh) * 2020-06-15 2020-10-16 四川勇创盛世新能源科技有限公司 一种植物油燃料

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Publication number Priority date Publication date Assignee Title
ITRM20110317A1 (it) * 2011-06-17 2012-12-18 Enea Floris Processo metodo e formulazioni per la produzione di un biocarburante a base di olii di natura vegetale anche esausti rigenerati e/o geneticamente modificati alghe e microalghe e/o olii da esse derivati addizionati ad alcoli primari e/o secondari e/o
WO2015003300A1 (zh) * 2013-07-08 2015-01-15 Song Guizhong 使用醇基清洁燃料大幅提高工业炉窑热效率的燃烧方法
CN103343964A (zh) * 2013-07-10 2013-10-09 宋贵中 使用醇基清洁燃料大幅提高工业炉窑热效率的燃烧方法
CN103343964B (zh) * 2013-07-10 2014-01-08 宋贵中 使用醇基清洁燃料提高工业炉窑热效率的燃烧方法
CN106675668A (zh) * 2016-12-09 2017-05-17 广西北海浩邦新能源科技有限公司 一种可再生醇基环保燃料
CN106675669A (zh) * 2016-12-09 2017-05-17 广西北海浩邦新能源科技有限公司 可再生醇基环保燃料的制备方法
CN111778073A (zh) * 2020-06-15 2020-10-16 四川勇创盛世新能源科技有限公司 一种植物油燃料

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