CN101750515B - Non-contact type measuring method for measuring liquid parameters - Google Patents

Non-contact type measuring method for measuring liquid parameters Download PDF

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Publication number
CN101750515B
CN101750515B CN2008102279822A CN200810227982A CN101750515B CN 101750515 B CN101750515 B CN 101750515B CN 2008102279822 A CN2008102279822 A CN 2008102279822A CN 200810227982 A CN200810227982 A CN 200810227982A CN 101750515 B CN101750515 B CN 101750515B
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liquid
capillary
image
measured
image data
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CN101750515A (en
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刘静
杨阳
王昊
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Technical Institute of Physics and Chemistry of CAS
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Technical Institute of Physics and Chemistry of CAS
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Abstract

The invention provides a non-contact measuring method for measuring liquid parameters, which comprises the following steps: 1) horizontally placing one end of a transparent capillary tube into the liquid to be detected; 2) recording the image data of the laminar flow process of the detected liquid in the capillary; 3) vertically placing the capillary tube; 4) capturing an image of a liquid column having a stable height; 5) calibrating the corresponding relation between the number of pixels in the imaging equipment and the length of a shot object, and carrying out image processing on image data to obtain the radius a of the capillary tube, the change process of the displacement S (t) of the liquid interface along with the time t, the height H of a liquid column formed in the capillary tube and the curvature radius R of the liquid interface; 6) and (5) calculating the fluid mechanics parameter of the measured liquid according to the data obtained by image processing in the step 5). The method does not depend on large-scale equipment, is simple and easy to implement, has low cost and small sample consumption. The invention can easily realize the measurement of the capillary array and can also simultaneously measure various liquid parameters.

Description

A kind of measuring method of non-contact measurement liquid parameter
Technical field
The invention belongs to biological chemistry and medical science detection range, specifically, the present invention relates to a kind of measuring method of liquid parameter.
Background technology
Flowing liquid in the pipeline is carried out the measurement of flow velocity, flow and other parameters and feature, be not only problem common in the commercial production, also rise day by day in the application in fields such as biological chemistry, medical science detection.And the size of fluid to be measured also not only is confined under the macro-scale, and along with the fast development of whole world micro-/ nano technical field, the liquid parameter measurement that is flowing in the micro-tube is the focus that researchers pay close attention to equally.
For micro-tube, the measuring technique of liquid fluid parameter and method have a variety of, and the measurement state according between surveying instrument and fluid to be measured mainly can be divided into contact type measurement and non-contact measurement.Contact type measurement is meant that the sensing device of surveying instrument places liquid, directly measures the special parameter of liquid, by data collector measured parameter is imported computing machine and is calculated other correlation parameters again.When taking this kind metering system, because the yardstick of liquid own is small, therefore very high to the size and the degree of accuracy requirement of sensor, simultaneously, the flow state of liquid also can produce a very large impact measurement result.In addition,, therefore all can bring very big influence reliability and the serviceable life to sensor, for example have corrosive liquid and may make the senser element that is exposed in the liquid that corrosion or damage take place because liquid directly contacts with sensor.And in the biochemical medicine field, directly the senser element that contacts with liquid also may pollute sample, thereby influences measurement result.
Non-contact measurement is meant that sensing device does not directly contact with liquid in the surveying instrument, but utilize the emitter in the instrument that liquid is launched certain signal, receive the reflection liquid signal by receiving sensing device, by data collector reflected signal is imported computing machine again and handle, and then obtain the correlation parameter of a series of liquid.Method such as the definite flow of liquid variable element that uses ultrasonic Doppler technique to realize, its cardinal principle is utilizes the ultrasonic generator emission to have the ultrasonic signal of at least one first frequency f1 given in advance, re-using ultrasonic receiver receives by the ultrasonic signal behind the reflection liquid, and this signal has at least one second frequency f2 that reflects this corresponding region feature, this frequency has been offset a corresponding frequency displacement Δ f with respect to frequency f 1, and then the liquid velocity of this corresponding region can be calculated by Δ f.When taking this method, though avoided sensor to contact, not only comprised in the surveying instrument also needing signal generator and receiver by signal processing apparatus with the direct of fluid to be measured, it forms relative bulky complex, and, being the degree of accuracy of guaranteeing to measure, the design concept of surveying instrument and structure are very complicated, not only cost is higher, program is loaded down with trivial details, and is random relatively poor, also is difficult to realize microminiaturized and integrated with micro-tube simultaneously.
Capillary viscosimeter is the instrument of measurement fluid flow characteristics relatively commonly used in present actual engineering and the commercial production.The measuring method of this viscosity meter has multiple, the liquid that can measure certain volume flows through the time capillaceous under certain pressure reduction, in also can measuring unit's time under certain pressure reduction the volume of trickle, can also stipulate the pressure reduction at certain flow measurement kapillary two ends.Can be according to measuring gained parameter and equation μ=(π r 4Pt)/(8Lv) converse the viscosity coefficient of liquid, wherein μ is a viscosity coefficient, and r is a capillary radius, and L is a capillary pipe length, and P is the pressure differential at kapillary two ends, and v is the volume that flows through liquid, and t is a flushing time.Capillary viscosimeter need possess corresponding attachment device for the needed special time of said method, flow, volume and pressure reduction are provided, and has increased the volume and the complexity of this device.In addition, the measurement parameter of capillary viscosimeter is single, and viscosity is unique measurement target of this instrument.
In addition, for the measurement of fluid velocity, there is a kind of PIV technology (particle image velocimetry method) at present.The PIV technology is a kind of based on the contactless two-dimensional flow field measuring technique of flow field figure as correlation analysis.When utilizing PIV commercial measurement flow field, need in the flow field, to disseminate the trace particle that proportion is suitable and followability is good, reflect the motion of water particle by the motion of trace particle; And with natural light or laser institute's lining face is shone, form the illumination plane, use picture pick-up device such as CCD to obtain the image of trace particle.Gained imagery exploitation two dimension quick Fourier transformation is realized the calculating of relevance function, and utilizes the basic definition of speed, realizes the water particle velocity survey by measuring the displacement of water particle in known interval.The PIV technology need possess corresponding light source (as generating laser), CCD camera, the PC of image processing system etc. is installed for above-mentioned functions is provided, so the PIV measuring system often also has huge volume and complicated structure.In addition, the Flame Image Process principle of PIV technology is also very complicated.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, Image Acquisition and treatment technology are introduced the liquid parameter measurement cheaply, thereby provide a kind of and only need promptly can obtain the contactless liquid parameter measuring method of parameters such as flow rate of liquid, density, surface tension, viscosity in the micro-tube by portable domestic image documentation equipment and simple computing system.
The measuring method of non-contact measurement liquid parameter provided by the invention comprises the steps:
1) the transparent capillary level is inserted in the fluid to be measured, made fluid to be measured that capillarity take place in transparent capillary and begin laminar flow;
2) image data of the laminar flow process of use portable type image equipment records fluid to be measured in kapillary;
3) transparent capillary described in the step 1) is vertically placed, kept its inlet end still to be immersed in the fluid to be measured, fluid to be measured forms the fluid column with level altitude because of the interaction of gravity and capillary force in the transparent capillary bottom.
4) use portable type image equipment to take fluid to be measured forms the level altitude fluid column in the kapillary bottom image.
5) to step 2) in the record image data carry out Flame Image Process, draw in radius a capillaceous and the laminar flow liquid surface displacement S (t) change procedure of t in time, the image document that writes down in the step 4) is carried out Flame Image Process, draw fluid to be measured forms fluid column in kapillary height H with and the radius of curvature R of liquid surface; Measure the gained data according to all, by Flame Image Process and parameter analysis software and then draw the hydrodynamic parameters of fluid to be measured.
In the technique scheme, described step 1) and 3) in, described fluid to be measured also needs to add suitable coloring agent according to the ambient lighting condition.
In the technique scheme, described step 1) and 3) in, described transparent capillary pipe range is certain and known.
In the technique scheme, described step 2) and 4) in, when the recording image data, described portable type image equipment camera lens axis direction keeps vertical with described kapillary axis direction.
In the technique scheme, described step 2) in, before the recording image data, adjust described portable type image equipment focal length or and transparent capillary between distance, make portable type image equipment to the maximum panoramic imagery of transparent capillary.
In the technique scheme, in the described step 4), when record liquid-column height image document, keep portable type image equipment focal length or with transparent capillary between distance and described step 2) consistent.
In the technique scheme, described step 2) and 4) in, the background of the image of gathering should not have moving object and single as far as possible.
In the technique scheme, in the described step 5), the dynamic image data adopts the method for difference to analyze.During to the still image analysis, can utilize click liquid level top and bottom to obtain liquid-column height shared pixel count in image and also store, 3 residing location of pixels and storage are write down in same click liquid surface curved surface two ends and bottom.
In the technique scheme, in the described step 5), the hydrodynamic parameters of fluid to be measured comprises the flow velocity of fluid to be measured, density, viscosity and surface tension.
In the technique scheme, in the described step 5), the density p of described fluid to be measured=(2 σ)/(RgH), g is an acceleration of gravity in the formula, σ is tested surface tension coefficient.
In the technique scheme, in the described step 5), the instantaneous velocity V (t) of described fluid to be measured=dS (t)/dt, surface tension F=σ/2R, viscosity, mu On average=(a 2σ)/(4RV On average), V in the formula On averageBe the mean value of instantaneous velocity V (t), σ is the surface tension coefficient of fluid to be measured.
In the technique scheme, described step 1) and 3) in, described fluid to be measured and kapillary can be the arrays that a plurality of samples and kapillary are formed; Described step 2) in, described portable type image equipment writes down the image data of the laminar flow process in each kapillary in the described array simultaneously; In the described step 4), described portable type image equipment writes down the image document of the interior liquid-column height of each kapillary in the described array simultaneously.
In the technique scheme, described fluid to be measured can be the human body fluid sample, as blood, saliva, urine, tear etc., also can be any one biochemical samples.For improving the contrast of colors of image, these fluid samples can add coloring agent according to measuring needs.
In the technique scheme, described transparent capillary can be for making kapillary by glass or other transparent materials, and caliber can be between the 0.01mm-1.5mm scope, and pipe range can be between the 50mm-150mm scope.
In the technique scheme, described portable type image equipment can be mobile phone, digital camera or Digital Video etc. can take the continuous image data, but and the digital equipment of data immediate access, its resolution need be higher than 200,000 pixels.The image data of taking gained can be passed in the data processing equipment through the signal transmission form of data line, bluetooth or maturation such as infrared.
In the technique scheme, use the data processing equipment that Flame Image Process and parameter analysis software are installed to carry out Flame Image Process and calculating.Described Flame Image Process and parameter analysis software be integrated image processing capacity and liquid fluid parameter analytic function in the software of one, corresponding constant data in the distinguishable picture of publishing picture of image processing function wherein.
In the technique scheme, except directly flowing based on swabbing action drive fluid capillaceous, the also purpose that can be used for reaching drive fluid by the outfield that initiatively applies such as electric field, magnetic field, sound field, laser action and even localized heat.Like this, according to adding outfield strength and the response characteristic of fluid, can identify more the physical-chemical parameters.
With respect to prior art, the present invention has following technique effect:
Contactless liquid fluid measurement method of parameters provided by the invention, only need by the portable domestic image documentation equipment that is seen everywhere, can measure and analyze parameters such as flow rate of liquid, density, viscosity, this method does not rely on main equipment, simple, cost is low, and amount of samples is small.The present invention can realize the measurement of capillary array easily, also can measure various different liquids parameters simultaneously.
Description of drawings
Below, describe embodiments of the invention in conjunction with the accompanying drawings in detail, wherein:
Accompanying drawing 1 is the course of work synoptic diagram of a kind of contactless fluid flow parameter measuring method provided by the invention;
Accompanying drawing 2 is the system architecture synoptic diagram of contactless fluid flow parameter measuring method provided by the invention;
Accompanying drawing 3 is the portable system structural representation of contactless fluid flow parameter measuring method provided by the invention;
Accompanying drawing 4 is the synoptic diagram of contactless capillary array fluid flow parameter measuring method provided by the invention;
Accompanying drawing 5 is the process synoptic diagram that contactless fluid flow parameter measuring method provided by the invention is measured fluid density.Wherein Fig. 5 A is for measuring initial time; Fig. 5 B stops to rise constantly for the liquid flow interface.
Accompanying drawing 6 is the process synoptic diagram that contactless fluid flow parameter measuring method provided by the invention is measured liquid velocity and viscosity; Wherein Fig. 6 A is for measuring initial time; Fig. 6 B is that the displacement of liquid flow interface is S (t 1) the moment; Fig. 6 C is that the displacement of liquid flow interface is S (t 2) the moment; Fig. 6 D is that the displacement of liquid flow interface is S (t 3) the moment.
Accompanying drawing 7 is the process flow diagram of Flame Image Process and parameter analysis software 4 in the contactless fluid flow parameter measuring method provided by the invention.
Embodiment
Further describe the present invention below in conjunction with the drawings and specific embodiments:
Embodiment 1
Fig. 1 is the course of work synoptic diagram of the contactless fluid flow parameter measuring method of one embodiment of the invention.
Fig. 2 is the system architecture synoptic diagram of contactless fluid flow parameter measuring method among the embodiment, when portable domestic image documentation equipment 3 was regular handset, digital camera or Digital Video, Flame Image Process and parameter analysis software 4 were installed in the computing machine 5.
With reference to figure 1 and Fig. 2, the measuring method of liquid parameter is as follows:
One end level of transparent capillary 2 is inserted in the fluid to be measured 1, and at this moment, capillarity takes place and begins laminar flow in fluid to be measured in transparent capillary, opens this all processes that flows of portable domestic image documentation equipment 3 records simultaneously.Again the transparent capillary in the above-mentioned steps 2 is vertically placed, keep its inlet end still to be immersed in the fluid to be measured, fluid to be measured 1 forms fluid column because of the interaction of gravity and capillary force in the bottom of transparent capillary 2, after treating fluid column highly stable, use portable type image equipment 3 to take the image of the fluid column that fluids to be measured 1 form in transparent capillary 2 bottoms.After finishing above-mentioned all images and image acquisition, use Flame Image Process and 4 pairs of gained image datas of parameter analysis software to handle, draw the correlation parameter of liquid in image, pool Xiao Ye (Poiseuille) law that flows according to the kapillary laminate is realized every fluid parameters such as flow rate of liquid, density, viscosity are analyzed again.The image that the family expenses image documentation equipment is gathered can adopt as bluetooth, wireless data transmission mode such as infrared, sends to designated computer and handles (as shown in Figure 2).Also can directly carry out Flame Image Process and calculating in this locality.As shown in Figure 3, portable domestic image documentation equipment 3 can be a portable intelligent mobile phone 6, use portable intelligent mobile phone 6 to take fluids to be measured 1 continuous laminar flow image (video) in the transparent capillary 2 of horizontal positioned, and the image of fluid column after highly stable in the transparent capillary of vertically placing 2.Be installed on then the Flame Image Process taken in the formula smart mobile phone 6 and parameter analysis software 4 just directly analytical calculation draw the parameters of fluid to be measured 1.Because the image processing process required memory is bigger, therefore, when adopting this portable system, higher for the configuration requirement of portable intelligent mobile phone 6.
Referring to figs. 2 and 3, the specific operation process of carrying out the liquid parameter measurement is as follows:
1. according to the configuration of practical application selective system, when needs are exported the parameters of fluid to be measured 1 at once, can select the portable system configuration for use, promptly portable smart mobile phone 6 integrates portable domestic image documentation equipment 3 and Flame Image Process and parameter analysis software 4; When need not to export the parameters of fluid to be measured 1 at once, can reach portable domestic image documentation equipment 3 and select regular handset, digital camera or video camera for use, and Flame Image Process and parameter analysis software 4 be installed in the computing machine 5 earlier with the modular system configuration.
2. get an amount of fluid to be measured 1, and place transparent capillary 2 according to the parameter of required measurement.When needs are measured fluid density, vertically place transparent capillary 2.When needs were measured liquid viscosity, first horizontal positioned transparent capillary 2 was after finishing image data and taking, again with its vertical placement.The situation that following steps are measured liquid viscosity with needs is that example is described.
Horizontal positioned transparent capillary 2 and apply fluid to be measured 1 after, capillarity takes place and begins laminar flow in fluid to be measured 1 in transparent capillary 2, open portable domestic image documentation equipment 3 simultaneously, the image data of record fluid to be measured 1 flow process.
4. behind the completing steps 3, transparent capillary 2 is vertically placed, keep its inlet end still to be immersed in the fluid to be measured 1, at this moment, fluid to be measured 1 because of the interaction of gravity and capillary force the bottom of transparent capillary 2 form have the fluid column of level altitude after, use 3 pairs of transparent capillaries of portable domestic image documentation equipment 2 to carry out image acquisition.According to concrete measurement needs, determine whether implementation step 3).
5. the image data input picture that is write down is handled and parameter analysis software 4, just can be obtained the corresponding liquid parameter.
Embodiment 2
Fig. 4 is an alternative embodiment of the invention.For the parameter measurement of finishing multiple liquid rapidly and efficiently, can make various fluids to be measured 1 capillarity take place in the array of horizontal positioned transparent capillary 2 and begin laminar flow, use this all processes that flows of portable domestic image documentation equipment 3 records simultaneously and store image data because of capillary action.Again the array of above-mentioned transparent capillary 2 is vertically placed, keep its inlet end still to be immersed in the fluid to be measured, when various fluids to be measured 1 because of the interaction of gravity and capillary force the bottom of the array of transparent capillary 2 form have the fluid column of level altitude after, re-use portable type image equipment 3 and take various fluids to be measured 1 form the level altitude fluid column in the bottom of the array of transparent capillary 2 image.When using present embodiment, portable domestic image documentation equipment 3 camera lens axis directions need vertical with the capillary array plane, make portable domestic image documentation equipment 3 horizontal directions parallel with transparent capillary 2 axis directions simultaneously.When obtaining liquid at image data that in kapillary, flows and image document thereof at the formed level altitude fluid column in kapillary bottom, the focal length of portable domestic image documentation equipment 3 or need remain unchanged with the interplanar distance of capillary array.After finishing above-mentioned all images and image acquisition, use Flame Image Process and 4 pairs of gained image datas of parameter analysis software to handle, draw the correlation parameter of liquid in image, pool Xiao Ye (Poiseuille) law that flows according to the kapillary laminate is realized parameters such as flow rate of liquid, density, viscosity are analyzed again.
Embodiment 3
Present embodiment is an embodiment that only need measure fluid density.As shown in Figure 5, when the present invention is used to realize the measurement of fluid density, with transparent capillary 2 vertical insertions in the fluid to be measured 1, when the liquid surface of fluid to be measured 1 after transparent capillary 2 stops to rise, 3 pairs of transparent capillaries of portable domestic image documentation equipment 2 carry out image acquisition, and the image processing function in use Flame Image Process and the parameter analysis software 4 obtains the related data in the image data, as: the radius a of transparent capillary 2, the radius of curvature R of fluid to be measured 1 liquid surface in transparent capillary 2, and fluid to be measured 1 formed liquid-column height H in transparent capillary 2; Re-use the liquid parameter analytic function in Flame Image Process and the parameter analysis software 4, pool Xiao Ye (Poiseuille) law that flows according to the kapillary laminate calculates density of liquid ρ=(2 σ)/(RgH), wherein σ is the surface tension coefficient of liquid, and g is an acceleration of gravity.
Embodiment 4
Present embodiment is the embodiment that measures flow rate of liquid and viscosity.As shown in Figure 6, when needs are measured the measurement of flow rate of liquid and viscosity, need, and open the image data that portable domestic image documentation equipment 3 recording liquids flow in kapillary earlier with these transparent capillary 2 horizontal positioned.After treating that fluid to be measured 1 is full of transparent capillary 2, stop image collection.Then transparent capillary 2 is vertically placed, keep its inlet end still to be immersed in the fluid to be measured, when fluid to be measured 1 because of the interaction of gravity and capillary force the bottom of transparent capillary 2 form have the fluid column of level altitude after, use 3 pairs of transparent capillaries of portable domestic image documentation equipment 2 to carry out image acquisition.After finishing above-mentioned all images and image acquisition, image processing function in use Flame Image Process and the parameter analysis software 4 at first obtains the corresponding constant data in the image document, as: the radius of curvature R of the radius a of transparent capillary 2, fluid to be measured 1 liquid surface in transparent capillary 2; Be time step cut-away view picture from image data with Δ t again, utilize the method for closing on two width of cloth image subtractions to obtain the time dependent displacement process of liquid surface S (t) in the laminar flow; Use the liquid parameter analytic function in Flame Image Process and the parameter analysis software 4 at last, calculate instantaneous velocity (V (t)=dS (t)/dt), the mean flow rate of liquid according to mobile pool Xiao Ye (Poiseuille) law of kapillary laminate
Figure G2008102279822D00091
Surface tension F=σ/2R and viscosity, mu On average=(a 2σ)/(4RV On average), wherein σ is the surface tension coefficient of liquid, can search the correlation parameter table according to the kind of measuring liquid and temperature and learn that these parameter lists can be stored in the data processing equipment that described Flame Image Process and parameter analysis software are installed in advance.
Fig. 7 is for realizing the software flow synoptic diagram of Flame Image Process and parameter analytic function.When the image data of fluid to be measured 1 flow process in the transparent capillary 2 that processing horizontal is placed, the background of the video of gathering should not have moving object and single as far as possible, adopt the method for difference, video is divided into several time periods, the image that will end up the time period and this time period, initial image compared, just can draw the pixel count that liquid moves in this time period, at last that the displacement situation of all time periods is average, can obtain accurate relatively result.When fluid to be measured 1 forms the image document of fixing fluid column in handling the vertical transparent capillary of placing 2, can utilize click liquid level top and bottom to obtain liquid-column height shared pixel count in image also stores, 3 residing location of pixels and storage are write down in same click liquid surface curved surface two ends and bottom.Because computing velocity is less demanding to video resolution, keep under the bigger prerequisite of kapillary proportion in video pictures (figure image width 15cm for example, about capillary pipe length 10cm), per second 15 frame left and right sides images can satisfy accuracy requirement, can adopt lower video sampling rate (for example 15fps) and less picture altitude and width (for example 160 pixels * 120 pixels) during images acquired.Because capillary pipe length is fixed, the sum of all pixels that liquid moves in the Video processing promptly is similar to capillary pipe length, so can be similar to demarcation (rice/pixel) to camera.Comprehensive above gained result can calculate and obtain vertical hair tubule liquid level, radius-of-curvature and horizontal capillary liquid flowing velocity.
Concrete processing procedure comprises the steps: as shown in Figure 7
1, reads vertical hair tubule image;
2, obtain the shared number of pixels of liquid-column height;
3, obtain the location parameter of liquid surface curve; Described location parameter is generally got 3 the residing location of pixels in liquid surface curved surface two ends and bottom;
4, read level kapillary video;
5, calculate the number of pictures per second of video;
6, grasp film frame A and the frame B after the Δ t time;
7, transfer A, B to gray level image, conversion back A, B are the two dimensional gray matrix, are convenient to calculate;
8, with two width of cloth image subtractions, draw C, the situation of change that two width of cloth figure are taken place before and after can observing by C; Gray-scale map is a numerical matrix, every gray-scale value in the numerical value correspondence image in the matrix;
9, binaryzation C promptly sets a threshold value, and the point that gray scale surpasses this threshold value is 1, otherwise is 0;
10, calculating the capable pixel count in the zone that changes, promptly is 1 pixel number in the horizontal direction after the image C binaryzation, and this pixel count is exactly the pixel count that flow of liquid is crossed;
11, judge whether to handle all frames, if the judgment is Yes, enter step 12; Otherwise enter step 110;
110, will increase Δ t the time, get back to step 6;
12, camera is demarcated, set number of pixels with and length in kind between concern that one to one the unit of calibration coefficient is a rice/pixel in the present embodiment;
13, the liquid flow velocity of each time period of calculated level kapillary; This speed equals the product of calibration coefficient, pixel count and number of pictures per second;
14, calculate vertical hair tubule liquid level, radius-of-curvature and level average velocity capillaceous.
In the above embodiment of the present invention, fluid to be measured 1 can be the human body fluid sample, as blood, saliva, urine, tear etc., also can be any one biochemical samples.For improving the contrast of colors of image, these fluid samples can add coloring agent according to measuring needs.
In the above embodiment of the present invention, transparent capillary 2 can be for making kapillary by glass or other transparent materials, and caliber can be between the 0.1mm-1.5mm scope, and pipe range can be between the 50mm-150mm scope.
The image documentation equipment of portable domestic described in the present invention 3 can be smart mobile phone, digital camera or Digital Video etc. can take the continuous image data, but and the digital equipment of data immediate access, its digital resolution need be higher than 200,000 pixels.When image documentation equipment 3 was regular handset, digital camera or Digital Video, the processing of image data can be finished in computing machine 5; When image documentation equipment 3 was smart mobile phone 6, the collection of image data and processing can be finished in smart mobile phone 6 simultaneously.
The present invention has lot of advantages.At first, the present invention can realize the measurement of the multiple parameter of liquid on identical device, as surface tension, flow velocity, viscosity and the density etc. of liquid in kapillary.Utilize the present invention not only can finish the non-cpntact measurement of above-mentioned multiple parameter, can also provide different system configuration according to different demands simultaneously, it can be played a role under more occasions; Secondly, the present invention is simple in structure, has adopted the most common image documentation equipment, is easy to realize, and is safe and reliable, with low cost, can select the measurement material of different size according to the volume of sample; The 3rd, the method can also realize the array measurement easily, thereby increases substantially the speed and the efficient of measurement.
Among the present invention, when using portable domestic image documentation equipment 3, need take to prevent the shake measure, with the influence of avoiding the image shake that image processing process is brought; Simultaneously, the relative distance between portable domestic image documentation equipment 3 and photographic subjects need guarantee that portable domestic image documentation equipment 3 can carry out maximum panoramic imagery to photographic subjects.Therefore portable domestic image documentation equipment 3 can be fixed on the tripod, to address the above problem.
The contactless liquid fluid measurement method of parameters that the foregoing description provides is to obtain liquid at transparent fluid device (image data that flows in as kapillary) by means of the portable domestic image documentation equipment that is seen everywhere, the Hydrodynamics Theory that flows by Flame Image Process and kapillary laminate is measured and is analyzed parameters such as flow rate of liquid, density, viscosity as pool Xiao Ye (Poiseuille) law.Adopt the measuring method described in the present invention, not only enough can finish the measurement of the every flow parameter of liquid quickly and easily, also overcome the intrinsic drawback in the method that traditional measurement depends on main equipment, improved accuracy and the reliability measured.Meanwhile, method proposed by the invention also has advantages such as simple, that cost is low, and amount of samples is small, measures when more can realize in the capillary array various different liquids parameter easily.In addition, the present invention can the expanded application occasion, as by the function Characteristics of test and appraisal liquid to multiple two dimension, three-dimensional material, determines the respective attributes of material.
It should be noted last that above embodiment is only unrestricted in order to technical scheme of the present invention to be described.Although the present invention is had been described in detail with reference to embodiment, those of ordinary skill in the art is to be understood that, technical scheme of the present invention is made amendment or is equal to replacement, do not break away from the spirit and scope of technical solution of the present invention, it all should be encompassed in the middle of the claim scope of the present invention.

Claims (11)

1.一种非接触式测量液体参数的测量方法,包括如下步骤:1. A method for measuring a non-contact measurement liquid parameter, comprising the steps of: 1)将透明毛细管的一端水平置入被测液体中,使被测液体在透明毛细管中发生毛细现象并开始层状流动;1) Place one end of the transparent capillary horizontally into the liquid to be measured, so that the liquid to be measured will undergo capillary phenomenon in the transparent capillary and start laminar flow; 2)使用便携式影像设备记录被测液体在毛细管内的层状流动过程的影像资料;2) Use portable imaging equipment to record the image data of the laminar flow process of the measured liquid in the capillary; 3)将步骤1)中所述透明毛细管垂直放置,保持所述毛细管的入口端仍然浸没于被测液体中;3) placing the transparent capillary in step 1) vertically, keeping the inlet end of the capillary still immersed in the liquid to be tested; 4)待所述毛细管内液柱高度稳定后,使用便携式影像设备拍摄具有稳定高度的液柱的图像;4) After the height of the liquid column in the capillary is stable, use a portable imaging device to take an image of the liquid column with a stable height; 5)标定所述便携式影像设备中像素个数与所摄物体长度的对应关系,对步骤2)中记录的影像资料进行图像处理,得出毛细管的半径a以及层状流动中液体界面位移S(t)随时间t的变化过程,对步骤4)中记录的图像资料进行图像处理,得出被测液体在毛细管中形成液柱的高度H以及其液体界面的曲率半径R;5) Calibrate the corresponding relationship between the number of pixels in the portable imaging device and the length of the captured object, and perform image processing on the image data recorded in step 2), to obtain the radius a of the capillary and the displacement S of the liquid interface in the laminar flow ( t) process of changing with time t, image processing is performed on the image data recorded in step 4), and the height H of the liquid column formed by the measured liquid in the capillary and the radius of curvature R of the liquid interface thereof are obtained; 6)根据所述步骤5)中经图像处理所得出的数据,计算得出被测液体的流体力学参数,所述流体力学参数包括被测液体的流速、密度、粘度、表面张力中的任意一个或多个。6) According to the data obtained through image processing in the step 5), the hydrodynamic parameters of the measured liquid are calculated, and the hydrodynamic parameters include any one of the flow velocity, density, viscosity, and surface tension of the measured liquid or more. 2.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤1)中,所述被测液体还需要根据环境光照条件添加适当的染色剂。2. The method for non-contact measurement of liquid parameters according to claim 1, characterized in that, in the step 1), the liquid to be measured also needs to add an appropriate coloring agent according to ambient light conditions. 3.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤2)与4)中,在记录图像及影像资料时,所述便携式影像设备镜头轴线方向与所述毛细管轴线方向保持垂直。3. The method for measuring non-contact liquid parameters according to claim 1, characterized in that, in the steps 2) and 4), when recording images and video data, the direction of the lens axis of the portable imaging device is the same as the The direction of the capillary axis remains vertical. 4.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤2)中,在记录影像资料前,调整所述便携式影像设备的焦距或与透明毛细管间的距离,使便携式影像设备对透明毛细管最大全景成像。4. The non-contact measuring method for measuring liquid parameters according to claim 1, characterized in that, in the step 2), before recording the image data, adjust the focal length of the portable image device or the distance between the portable image device and the transparent capillary. The distance enables the portable imaging device to image the maximum panoramic view of the transparent capillary. 5.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤4)中,在记录液柱高度图像资料时,保持便携式影像设备的焦距一致或与所述透明毛细管间的距离与所述步骤2)一致。 5. The measuring method of non-contact measuring liquid parameters according to claim 1, characterized in that, in the step 4), when recording the liquid column height image data, keep the focal length of the portable imaging device consistent or with the described The distance between the transparent capillaries is consistent with the step 2). the 6.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤5)中,采用差分法处理动态影像资料,获得所述位移S(t)随时间t的变化过程;处理静态图像时,利用鼠标点击液面顶端和底端获得液柱高度在图像中所占的像素数并存储,从而获取所述液柱的高度H,利用鼠标点击液体界面曲面两端和底部,记录三点所处的像素位置并存储,然后再通过计算获取所述曲率半径R。6. The measuring method of non-contact measuring liquid parameters according to claim 1, characterized in that, in the step 5), the difference method is used to process the dynamic image data, and the displacement S (t) is obtained over time t Change process; when processing a static image, use the mouse to click on the top and bottom of the liquid surface to obtain the number of pixels occupied by the height of the liquid column in the image and store it, so as to obtain the height H of the liquid column, and use the mouse to click on both ends of the curved surface of the liquid interface and the bottom, record and store the pixel positions of the three points, and then obtain the curvature radius R by calculation. 7.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤6)中,所述被测液体的密度ρ=(2σ)/(RgH),式中g是重力加速度,σ是被测液体的表面张力系数。7. The method for non-contact measurement of liquid parameters according to claim 1, characterized in that, in the step 6), the density of the measured liquid ρ=(2σ)/(RgH), where g is the acceleration of gravity, and σ is the surface tension coefficient of the measured liquid. 8.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤6)中,所述被测液体的瞬时流速V(t)=dS(t)/dt,表面张力F=σ/2R,粘度μ平均=(a2·σ)/(4RV平均),式中V平均是瞬时流速V(t)的平均值,σ是被测液体的表面张力系数。8. The non-contact measuring method for measuring liquid parameters according to claim 1, characterized in that, in the step 6), the instantaneous flow velocity V(t)=dS(t)/dt of the measured liquid, Surface tension F=σ/2R, viscosity μ average =(a 2 ·σ)/(4RV average ), where V average is the average value of instantaneous flow velocity V(t), and σ is the surface tension coefficient of the measured liquid. 9.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述步骤1)与3)中,所述被测液体和毛细管是多个样品和毛细管组成的阵列;所述步骤2)中,所述便携式影像设备同时记录所述阵列中的各毛细管内的层状流动过程的影像资料;所述步骤4)中,所述便携式影像设备同时记录所述阵列中各毛细管内液柱高度的图像资料。9. The method for measuring non-contact measurement liquid parameters according to claim 1, characterized in that, in the steps 1) and 3), the liquid to be measured and the capillary are arrays composed of a plurality of samples and capillaries; In the step 2), the portable imaging device simultaneously records the image data of the laminar flow process in each capillary in the array; in the step 4), the portable imaging device simultaneously records the image data of each capillary in the array. Image data of the height of the liquid column in the capillary. 10.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述被测液体为人体体液样品或其它任意一种生物化学样品。10. The method for non-contact measurement of liquid parameters according to claim 1, wherein the liquid to be measured is a human body fluid sample or any other biochemical sample. 11.根据权利要求1所述的非接触式测量液体参数的测量方法,其特征在于,所述毛细管管径为0.01mm-1.5mm,管长为50mm-150mm;所述便携式影像设备为手机、数码照相机或数码摄像机,或者是其它可拍摄连续影像资料的数码影像设备;所述便携式影像设备的静态图像分辨率高于20万像素。 11. The non-contact measuring method for measuring liquid parameters according to claim 1, characterized in that, the diameter of the capillary is 0.01mm-1.5mm, and the length of the tube is 50mm-150mm; the portable imaging device is a mobile phone, A digital camera or a digital video camera, or other digital imaging equipment capable of shooting continuous image data; the still image resolution of the portable imaging equipment is higher than 200,000 pixels. the
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