CN101747978A - Clean fired coal saving agent - Google Patents
Clean fired coal saving agent Download PDFInfo
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- CN101747978A CN101747978A CN200910114694A CN200910114694A CN101747978A CN 101747978 A CN101747978 A CN 101747978A CN 200910114694 A CN200910114694 A CN 200910114694A CN 200910114694 A CN200910114694 A CN 200910114694A CN 101747978 A CN101747978 A CN 101747978A
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- coal
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- liquid
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L10/00—Use of additives to fuels or fires for particular purposes
- C10L10/02—Use of additives to fuels or fires for particular purposes for reducing smoke development
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- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Solid Fuels And Fuel-Associated Substances (AREA)
Abstract
The invention provides a clean fired coal saving agent with the effects of sulfur fixation, dust fall, heat increment and coal saving which is prepared and produced by industrially produced waste liquid and waste residues and chemical and mineral product raw materials. The clean fired coal saving agent is divided into two forms, namely a liquid product and a powder product; the liquid product is obtained by dissolving sodium nitrite, potassium nitrite, potassium nitrate, sodium nitrate, sodium sulfonate and sodium dodecyl benzene sulfonate into mixed liquid of paper making black liquid, alcohol waste liquid and fired coal fume water film dust removal and desulfurization alkali regeneration fluid; and the power product is obtained by absorbing and preparing the liquid product by utilizing hot fired coal slag, then allocating the chemical and mineral product raw materials and finally uniformly mixing, drying and crushing. The invention achieves cyclic resource utilization of industrial wastes, effectively solves the difficult problems of complete control of fired coal pollution and paper making and alcohol waste liquid pollution, has the advantages of innocuity, odorless, no three-waste emission, no increased investment and convenient operation and can use the device required not to be improved, save the coals per ton by 20-50 yuan and be used for all industrial and civil fired coals.
Description
Technical field:
The present invention relates to a kind of clean fired coal saving agent that utilizes black liquid, alcohol slops, coal-fired flue-gas dust removal with desulfurization by water film waste liquid, waste residue preparation to produce a kind of efficiency of sulfur retention, depositing dust, the gain of heat, economize on coal.
Background technology:
Rich coal resources in China, it is the big country of world's producing coal and consumption of coal, because China's economic construction is extensive high energy consumption, the Development patterns of high pollution, make China's economy when increasing, pay huge Energy resources cost, the serious environmental cost of pollution.For stopping this trend, and at the specific national conditions of the vast middle-size and small-size coal-fired enterprise of China, development is efficient, clean coal-saving agent researchs and develops especially that to utilize industrial production to produce a large amount of liquid and waste slag produced, it mainly is the black liquor that the paper mill produced, the waste liquid that Alcohol Production produced, coal-fired flue-gas dust-removing and desulfurization is administered the waste liquid that is produced, cinder production preparation clean fired coal saving agent, it is a little instant effect of investment, high efficiency, can produce a huge treatment of wastes with processes of wastes against one another, the technological invention of the new technique industrial colony of turning waste into wealth has not yet to see the relevant black liquid that utilizes, alcohol slops, the liquid and waste slag produced technology report that is used to produce the preparation clean fired coal saving agent of coal-fired flue-gas dust-removing and desulfurization.
Summary of the invention:
The purpose of this invention is to provide a kind of utilization is main base-material raw material with paper mill black liquor, alcohol slops, the coal-fired slag of coal-fired flue-gas dust-removing and desulfurization waste liquid and mineral products, allocates the method for a certain amount of industrial chemicals production preparation clean fired coal saving agent into.Reaching the treatment of wastes with processes of wastes against one another, turn waste into wealth, efficiently to utilize, Gu sulphur, depositing dust, the gain of heat, the effect of economizing on coal.
The technical solution adopted in the present invention:
Clean fired coal saving agent is divided into liquor, two kinds of form products of pulvis.Earlier the waste liquid with various productions dischargings is concentrated to certain concentration range, and the coal-fired slag after coal-fired flue-gas dust removal with desulfurization by water film waste liquid alkali manipulation of regeneration liquid and the perfect combustion as main raw material, is mixed with the clean fired coal saving agent of liquor type with industrial chemicals; Reusable heat stove cinder absorbs the liquor product and mends chemical mineral product raw material drying and pulverize the clean fired coal saving agent that promptly obtains pulvis.
The raw material of clean fired coal saving agent liquor is formed and part by weight is:
Alcohol slops (degree Beaume 25-35) 30-60%
Black liquid (degree Beaume 15-21) 30-60%
Sodium Nitrite (NaNO
2) 1-10%
Potassium nitrite (KNO
2) 1-10%
Saltpetre (KNO
3) 1-10%
SODIUMNITRATE (NaNO
3) 1-10%
Sodium dodecylbenzene sulfonate, sodium sulfonate 0.5-2%.
The raw material of clean fired coal saving agent pulvis is formed and part by weight is:
Coal-fired cinder 30-60%
Clean fired coal saving agent liquor product 30-50%
Manganse Dioxide breeze (MnO
2) 10-30%
Ferric oxide breeze (Fe
2O
3) 5-10%
Sodium Nitrite (NaNO
2) 1-10%
Potassium nitrite (KNO
2) 1-10%
Saltpetre (KNO
3) 1-10%
SODIUMNITRATE (NaNO
3) 1-10%.
The compound method of clean fired coal saving agent liquor product:
With Sodium Nitrite (NaNO
2), potassium nitrite (KNO
2), saltpetre (KNO
3), SODIUMNITRATE (NaNO
3), dissolve in black liquid or coal-fired flue-gas dust removal with desulfurization by water film regenerated liquid, alcohol slops behind the industrial chemicals uniform mixing such as Sodium dodecylbenzene sulfonate in proportion in spissated mixed concentrated liquid, stirring fully, dissolving back barrelling promptly gets the liquor product.
The compound method of clean fired coal saving agent powder product:
Hot coal slag with after-flame fully absorbs the liquor product that has been mixed with, allocates Sodium Nitrite (NaNO after drying into
2), potassium nitrite (KNO
2), saltpetre (KNO
3), SODIUMNITRATE (NaNO
3), Manganse Dioxide breeze (MnO
2), ferric oxide breeze (Fe
2O
3) pulverize the back pack that stirs and promptly get powder product.
The preparation method of coal-fired flue-gas dust removal with desulfurization by water film alkaline regeneration solution:
Coal-fired flue-gas dust removal with desulfurization by water film circulation fluid is placed the settling tank sediment, get then in the supernatant liquor suction agitator, under condition of stirring, add lime putty, when acidity-basicity ph value reaches 10-14, with regenerated liquid suction frame filter, the stillness of night of discharge is coal-fired dust removal with desulfurization by water film alkaline regeneration solution stock liquid.
The solids of discharging from pressure filter after depositing oxidation as building materials with and the gypsum raw material used of manufacture of cement.
The clean fired coal saving agent that adopts the technology of the present invention method to produce uses on various fire coals, and can obtain following clean coal saving combustion effect: sulfur-fixing rate is at 30-70%; Dust reduction rate is at 30-60%; Coal saving rate at 10-35%, subtract carbon emission 10-35%.
The present invention realize black liquid, alcohol slops, coal-fired dust-removal and desulfurizing waste liquid and coal-fired slag utilization fully, reach zero release, the treatment of wastes with processes of wastes against one another, turn waste into wealth.It not only effectively solves coal burning pollution and papermaking, alcohol slops and pollutes three big world property difficult problems of thoroughly administering, and has solved these liquid and waste slag produced new ways of utilizing, and the raw material of abundant cheapness is provided for the additive for fire coal market of heavy demand simultaneously.This clean fired coal saving agent is nontoxic, odorless, not spontaneous combustion, do not explode, non-corrosiveness, three-waste free discharge, applicable to the fire coal of various stoves.Use and not need reforming equipment, do not increase investment, do not increase the production use cost, a ton coal can save and prop up a 20-50 unit, and easy to use, operative technique is simple, can use in all industry and civil, reaches the high-efficiency multi-function energy-saving and emission-reduction, subtracts the purpose of carbon.
Embodiment:
Clean fired coal saving agent is divided into liquor, two kinds of form products of pulvis, liquor product industrial chemicals Sodium Nitrite (NaNO
2), potassium nitrite (KNO
2), saltpetre (KNO
3), SODIUMNITRATE (NaNO
3), sodium sulfonate, Sodium dodecylbenzene sulfonate be dissolved in the mixed solution of black liquid, alcohol slops, coal-fired flue-gas dust removal with desulfurization by water film alkaline regeneration solution and promptly get the liquor product.The liquor product that the coal-fired slag absorption of reusable heat is mixed with is allocated chemical mineral product raw material uniform mixing drying and crushing again into and is promptly obtained powder product.
Production application blank determination coal saving rate is at same boiler, uses same coal, and liquor, the pulvis clean fired coal saving agent product incendiary producing steam amount of allocating the different ratios amount in identical coal amount into contrast calculating.
Elaborate below in conjunction with embodiment.
Coal sample is got the raw materials ready: get 6 tons of same coal charges, through pulverize the mangcorn fine coal of granularity＜8mm, through fully mixing, be divided into 7 groups.
First group of coal 840kg is unworthy of clean fired coal saving agent and is processed into moulded coal, measures in contrast.
Second group of coal 840kg allocates 2.0% liquor clean fired coal saving agent 16.8kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
The 3rd group of coal 840kg allocates 3.0% liquor clean fired coal saving agent 25.2kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
The 4th group of coal 840kg allocates 4.0% liquor clean fired coal saving agent 33.6kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
The 5th group of coal 840kg allocates 3.2% liquor clean fired coal saving agent 17.3376kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
The 6th group of coal 840kg allocates 4.86% liquor clean fired coal saving agent 40.824kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
The 7th group of coal 840kg allocates 3.0% pulvis clean fired coal saving agent 25.2kg into, fully mixes the post-treatment shaped coal, measures as the ingredients coal.
| Second group | The 3rd group | The 4th group | |
| In the 840kg coal, allocate liquor clean fired coal saving agent amount ratio into | ??2.0％ | ??3.0％ | ??4.0％ |
| Dust removal with desulfurization by water film alkaline regeneration solution 45% | ??7.56kg | ??11.34kg | ??15.12Kg |
| Black liquid 40% | ??6.72Kg | ??10.08Kg | ??13.44Kg |
| Sodium Nitrite (NaNO 2)2％ | ??0.336Kg | ??0.504Kg | ??0.672Kg |
| Potassium nitrite (KNO 2)2％ | ??0.336Kg | ??0.504Kg | ??0.672Kg |
| Saltpetre (KNO 3)5％ | ??0.84Kg | ??1.26Kg | ??1.68Kg |
| SODIUMNITRATE (NaNO 3)5％ | ??0.84Kg | ??1.26Kg | ??1.68Kg |
| Sodium dodecylbenzene sulfonate 1% | ??0.168kg | ??0.252Kg | ??0.336Kg |
| Add up to total amount | ??16.8kg | ??25.2Kg | ??33.6kg |
| Coal saving rate | ??9.995％ | ??21.3％ | ??28.6998％ |
| In the 840kg coal, allocate liquor clean fired coal saving agent amount ratio into | ??3.2％ | The 5th group |
| Alcohol slops | ??30％ | ??8.064kg |
| In the 840kg coal, allocate liquor clean fired coal saving agent amount ratio into | ??3.2％ | The 5th group |
| Black liquid | ??30％ | ??8.064Kg |
| Sodium Nitrite (NaNO 2) | ??1％ | ??0.2688Kg |
| Potassium nitrite (KNO 2) | ??1％ | ??0.2688Kg |
| Saltpetre (KNO 3) | ??1％ | ??0.2688Kg |
| SODIUMNITRATE (NaNO 3) | ??1％ | ??0.2688Kg |
| Sodium dodecylbenzene sulfonate | ??0.5％ | ??0.1344kg |
| Add up to total amount | ??17.3376kg | |
| Coal saving rate | ??10.31％ |
| In the 840kg coal, allocate liquor clean fired coal saving agent amount ratio into | ??4.86％ | The 6th group |
| Alcohol slops | ??60％ | ??15.12kg |
| Black liquid | ??60％ | ??15.12Kg |
| Sodium Nitrite (NaNO 2) | ??10％ | ??2.52Kg |
| Potassium nitrite (KNO 2) | ??10％ | ??2.52Kg |
| Saltpetre (KNO 3) | ??10％ | ??2.52Kg |
| SODIUMNITRATE (NaNO 3) | ??10％ | ??2.52Kg |
| Sodium dodecylbenzene sulfonate | ??2％ | ??0.504Kg |
| Add up to total amount | ??40.824Kg | |
| Coal saving rate | ??31.34％ |
| In the 840kg coal, allocate pulvis clean fired coal saving agent amount ratio into | ??3.0％ | The 7th group |
| Coal-fired cinder | ??35％ | ??8.82kg |
| In the 840kg coal, allocate pulvis clean fired coal saving agent amount ratio into | ??3.0％ | The 7th group |
| The liquor clean fired coal saving agent | ??30％ | ??7.56Kg |
| Manganse Dioxide (MnO 2) | ??10％ | ??2.52kg |
| Ferric oxide (Fe 2O 3) | ??5％ | ??1.26kg |
| Sodium Nitrite (NaNO 2) | ??5％ | ??1.26kg |
| Potassium nitrite (KNO 2) | ??5％ | ??1.26kg |
| Saltpetre (KNO 3) | ??5％ | ??1.26kg |
| SODIUMNITRATE (NaNO 3) | ??5％ | ??1.26kg |
| Add up to total amount | ??25.2Kg | |
| Coal saving rate | ??20.35％ |
Above ingredients coal is fully mixed in agitator, measure the producing steam amount of identical coal amount respectively on same 10 tons of chain furnaces, by the front and back reading demonstration of same steam-flow meter, producing steam is as follows:
First group of ingredients blank determination group not, 840kg coal producing steam amount 26.9901-22.1608=4.8293 ton;
Second group of coal 840kg+ liquor clean fired coal saving agent 16.8kg producing steam amount 30.818-25.506=5.312 ton;
The 3rd group of coal 840kg+ liquor clean fired coal saving agent 25.2kg producing steam amount 35.123-29.265=5.858 ton;
The 4th group of coal 840kg+ liquor clean fired coal saving agent 33.6kg producing steam amount 40.154-33.9384=6.2153 ton;
The 5th group of coal 840kg+ liquor clean fired coal saving agent 17.3376kg producing steam amount 50.326-44.9988=5.3272 ton;
The 6th group of coal 840kg+ liquor clean fired coal saving agent 40.824kg producing steam amount 62.788-56.4452=6.3428 ton;
The 7th group of coal 840kg+ pulvis clean fired coal saving agent 25.2kg producing steam amount 80.233-74.4209=5.8121 ton.
Steam production calculates coal saving rate after measured:
The second assembly liquor clean fired coal saving agent 16.8kg,
The 3rd assembly liquor clean fired coal saving agent 25.2kg,
The 4th assembly liquor clean fired coal saving agent 33.6kg,
The 5th assembly liquor clean fired coal saving agent 17.3376kg,
The 6th assembly liquor clean fired coal saving agent 40.824kg,
The 7th assembly pulvis clean fired coal saving agent 25.2kg,
Detect data:
Table 1. clean fired coal saving agent falls sulphur and uses contrast test result statistics in fired coal combustion
Table 2. clean fired coal saving agent depositing dust in fired coal combustion is used contrast test result statistics
Table 3. clean fired coal saving agent is economized on coal in fired coal combustion and is used contrast test result statistics
Table 4. clean fired coal saving agent is economized on coal in fired coal combustion and is used contrast test result statistics
The captured sulfur result contrast test result statistics of table 5. clean fired coal saving agent in fired coal combustion
The addition optimization test result statistics of table 6. " clean fired coal saving agent " (solid powder/liquid agent)
The pulvis clean fired coal saving agent is suitable in the fire coal of powder coal stove boiler, manufacture of cement.The liquor clean fired coal saving agent is applicable to the Bed for Fine Coal of fluidizing furnace and specially burns in the coal-fired moulded coal of the chain furnace of moulded coal, reciprocating furnace, manual grate furnace, is applicable to the adapted of Beijing enamel kiln coal, brickkiln coal.
Claims (4)
1. clean fired coal saving agent is characterized in that: be divided into liquor, two kinds of form products of pulvis,
The raw material of clean fired coal saving agent liquor is formed and part by weight is:
Alcohol slops 30-60%
Black liquid 30-60%
Sodium Nitrite 1-10%
Potassium nitrite 1-10%
Saltpetre 1-10%
SODIUMNITRATE 1-10%
Sodium dodecylbenzene sulfonate, sodium sulfonate 0.5-2%;
The raw material of clean fired coal saving agent pulvis is formed and part by weight is:
Coal-fired cinder 30-60%
Clean fired coal saving agent liquor product 30-50%
Manganse Dioxide breeze 10-30%
Ferric oxide breeze 5-10%
Sodium Nitrite 1-10%
Potassium nitrite 1-10%
Saltpetre 1-10%
SODIUMNITRATE 1-10%.
2. clean fired coal saving agent according to claim 1, the compound method that it is characterized in that clean fired coal saving agent liquor product is: will dissolve in black liquid or coal-fired flue-gas dust removal with desulfurization by water film regenerated liquid, alcohol slops behind SODIUMNITRATE, potassium nitrite, saltpetre, SODIUMNITRATE, the Sodium dodecylbenzene sulfonate raw material uniform mixing according to the above ratio in spissated mixed concentrated liquid, stirring fully, dissolving back barrelling promptly gets the liquor product.
3. clean fired coal saving agent according to claim 1, the compound method that it is characterized in that the clean fired coal saving agent powder product is: the hot coal slag with after-flame fully absorbs the liquor product that has been mixed with, allocates SODIUMNITRATE, potassium nitrite, saltpetre, SODIUMNITRATE, Manganse Dioxide breeze, ferric oxide breeze after drying into and pulverizes the back pack that stirs and promptly get powder product.
4. clean fired coal saving agent according to claim 1, the preparation method who it is characterized in that coal-fired flue-gas dust removal with desulfurization by water film alkaline regeneration solution is: coal-fired flue-gas dust removal with desulfurization by water film circulation fluid is placed the settling tank sediment, get then in the supernatant liquor suction agitator, under condition of stirring, add lime putty, when acidity-basicity ph value reaches 10-14, with regenerated liquid suction frame filter, the stillness of night of discharge is coal-fired dust removal with desulfurization by water film alkaline regeneration solution stock liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910114694A CN101747978A (en) | 2009-12-31 | 2009-12-31 | Clean fired coal saving agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910114694A CN101747978A (en) | 2009-12-31 | 2009-12-31 | Clean fired coal saving agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101747978A true CN101747978A (en) | 2010-06-23 |
Family
ID=42475598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910114694A Pending CN101747978A (en) | 2009-12-31 | 2009-12-31 | Clean fired coal saving agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101747978A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102757836A (en) * | 2012-06-28 | 2012-10-31 | 李庆才 | Coal combustion improver |
| CN105038899A (en) * | 2015-05-16 | 2015-11-11 | 张金海 | Fuel coal composite catalyst and use method of same |
| CN108722492A (en) * | 2017-04-21 | 2018-11-02 | 中国石油化工股份有限公司 | One kind being suitable for smokeless catalytic coal gasifaction catalyst and preparation method thereof |
| CN109207231A (en) * | 2018-11-12 | 2019-01-15 | 山东东阿润生粘合剂有限公司 | A kind of coal-saving comburant improving efficiency of fire coal |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197106A (en) * | 1998-03-06 | 1998-10-28 | 呼世滨 | Fuel oil additive and its prodn. method |
| CN1271760A (en) * | 2000-03-20 | 2000-11-01 | 汤立敬 | Energy-saving additive of heavy oil and its preparing process |
| CN1513958A (en) * | 2002-12-02 | 2004-07-21 | 陶世清 | Environment protection fuel coal energy increasing liquid |
-
2009
- 2009-12-31 CN CN200910114694A patent/CN101747978A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197106A (en) * | 1998-03-06 | 1998-10-28 | 呼世滨 | Fuel oil additive and its prodn. method |
| CN1271760A (en) * | 2000-03-20 | 2000-11-01 | 汤立敬 | Energy-saving additive of heavy oil and its preparing process |
| CN1513958A (en) * | 2002-12-02 | 2004-07-21 | 陶世清 | Environment protection fuel coal energy increasing liquid |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102757836A (en) * | 2012-06-28 | 2012-10-31 | 李庆才 | Coal combustion improver |
| CN105038899A (en) * | 2015-05-16 | 2015-11-11 | 张金海 | Fuel coal composite catalyst and use method of same |
| CN108722492A (en) * | 2017-04-21 | 2018-11-02 | 中国石油化工股份有限公司 | One kind being suitable for smokeless catalytic coal gasifaction catalyst and preparation method thereof |
| CN109207231A (en) * | 2018-11-12 | 2019-01-15 | 山东东阿润生粘合剂有限公司 | A kind of coal-saving comburant improving efficiency of fire coal |
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Application publication date: 20100623 |