CN101711784A - Preparation method of serissa serissoide extractive - Google Patents
Preparation method of serissa serissoide extractive Download PDFInfo
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- CN101711784A CN101711784A CN200810200874A CN200810200874A CN101711784A CN 101711784 A CN101711784 A CN 101711784A CN 200810200874 A CN200810200874 A CN 200810200874A CN 200810200874 A CN200810200874 A CN 200810200874A CN 101711784 A CN101711784 A CN 101711784A
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Abstract
The invention discloses a preparation method of a serissa serissoide extractive. The preparation method comprises the following steps of: collecting, chopping and cleaning serissa serissoide; putting the raw materials in an alcohol extract tank; adding ethanol; boiling; refluxing the ethanol; filtering into filter liquid and filter residue after the first extraction; recycling ethanol in the filter liquid by a decompression concentrating tank; continuously concentrating dense liquid to obtain concentrated liquid; adding ethanol again to the filter residue; boiling; refluxing the ethanol; filtering to obtain first filter liquid and filter residue; adding water to the filter residue; boiling; filtering to respectively obtain second filter liquid and filter residue; discarding the filter residue; mixing and concentrating the concentrated liquid, the first filter liquid and the second filter liquid to obtain a serissa serissoide extract; filling the serissa serissoide extract in a container to refrigerate and store; and drying the extract to obtain extractive dry powder. The extractive is added to beverages or acts on a human body in other modes and improves the health level of people by utilizing the serissa serissoide efficacy of dispelling mild wind, relieving exterior syndrome, clearing heat, promoting diuresis, stimulating the circulation of the blood and relaxing the muscles and joints.
Description
Technical field
The present invention relates to a kind of preparation method of extract, particularly a kind of preparation method of Serissa foetida extract belongs to beverage raw material and makes the field.
Background technology
At present, in summer, people can drink many beverages, but these products can only satisfy the effect that heat clearing away, expelling summer-heat are refreshed oneself substantially, and can not play the function of health care to people.
Serissa foetida is called again: Caulis et folium pavettae hongkongensis, broken leaf Ilicis Purpureae, Radix Serissae, jasmine, know tender tea leaves
The evergreen undershrub of Serissa foetida, plant height three chis, branch is very thin, becomes the strain branch dense. and spend small and densely, the tree type is attractive in appearance beautiful, is suitable for potted plant or makes potted landscape.Leaf is minimum, and oval is green entirely, and the green milky kind of inlaying of leaf is also arranged. and floral white, infundibulate is scattered as snowflake when in full bloom summer at florescence, so name " Serissa foetida ". and originate in China, breed available pole and insert method, suitable spring and autumn plantation.
Serissa foetida is bloomed June, far sees as being in silver and white clothing, and is elegant lovely just as snowing June, and get Serissa foetida.
Its Nature of not only dressing up, and have dispelling wind to relieve the exterior syndrome, clearing away heat-damp and promoting diuresis, the effect of relaxing muscles and tendons and activating QI and blood in the collateral.Be used for flu, cough, toothache, acute tonsillitis, pharyngolaryngitis, acute and chronic hepatitis, enteritis, dysentery, infantile malnutrition, hypertension complicated headache, migraine, rheumatic arthralgia, leucorrhea; Stem ashing eye dripping is controlled mist.
The medical institutions that have are observed the bacteriostasis of Serissa foetida, detect the bacteriostasis of Serissa foetida with plate assay, and measure its minimum inhibitory concentration (MIC) and minimum bactericidal concentration (MBC). acute toxicity testing is measured maximum tolerated dose (MTD) with mice with oral administration. and the result: Serissa foetida is to bacillus subtilis, escherichia coli all have stronger inhibitory action, minimum inhibitory concentration is 1.25%, minimum bactericidal concentration is respectively 2.5%, 1.25%. the acute toxicity testing maximum tolerated dose that shows this material is greater than the 40g/kg. conclusion: Serissa foetida has tangible bacteriostasis, and it belongs to low toxicity or innocuous substance.
Therefore, develop as early as possible a kind of contain natural plants Serissa foetida not only can expelling summer-heat but also the healthy beverage that can keep healthy, be problem demanding prompt solution in the industry.
Summary of the invention
The objective of the invention is to, by a kind of preparation method of Serissa foetida extract is provided, to develop a kind of not only expelling summer-heat but also to have the beverage of health care.
The present invention adopts following technological means to realize:
A kind of preparation method of Serissa foetida extract,
Gather the Serissa foetida truncate, choose clean;
Above-mentioned raw materials is packed in the alcohol extraction jar, add 60%～95% ethanol of 3～6 times of amounts, boiled 1～3 hour, steam pressure is 0.4MPa～0.7MPa, alcohol reflux;
For the first time carry pure after-filtration, divide other filtrate to close filtering residue, filtrate is reclaimed ethanol by the concentrating under reduced pressure jar, stop to reclaim until ethanol＜60% that reclaims, dope continue to concentrate concentrated solution;
Filtering residue adds 60%～95% ethanol of 3～6 times of amounts for the second time, boils 1～3 hour, and steam pressure is 0.4MPa～0.7MPa, and alcohol reflux stops to reclaim until ethanol＜60% that reclaims, and filters win filtrate and filtering residue; Filtering residue adds 6～9 times of water gagings, boils 1～3 hour, and steam pressure is 1MPa～1.3MPa, filters, and obtains second filtrate and filtering residue respectively, discards filtering residue;
Concentrated solution, first filtrate, second filtrate mixed and be concentrated into D=0.8～1.5 promptly get Serissa foetida extractum; The extractum container of packing into, cold preservation is preserved down in 1 ℃～5 ℃;
The extractum spray dryer of packing into, inlet temperature is 180 ℃～195 ℃, leaving air temp is 70 ℃～90 ℃, promptly gets extract dry powder.
Aforesaid concentrated solution, first filtrate, second filtrate concentrated is respectively concentrating under reduced pressure or the interlayer concentration tank concentrates.
Aforesaid extract is: aqueous or capsule shape or ball shape or graininess or diffusing shape.
The present invention compared with prior art has following remarkable advantages and beneficial effect:
The preparation method of a kind of Serissa foetida extract of the present invention, by extracting the extract of the Serissa foetida that exists in the Nature, again extract is added in the beverage, perhaps adopt alternate manner to act on human body, utilize dispelling wind to relieve the exterior syndrome that Serissa foetida has, clearing away heat-damp and promoting diuresis, the effect of relaxing muscles and tendons and activating QI and blood in the collateral, changed only the lower the temperature present situation of expelling summer-heat of prior beverage, for the health that improves people has been made useful contribution.Simultaneously, extract can also be used as food additives, can also be as the additive of cosmetic skincare product, for people's health provides service more widely.
The specific embodiment
Below in conjunction with accompanying drawing specific embodiments of the invention are illustrated:
First embodiment:
A kind of preparation method of Serissa foetida extract,
Gather the Serissa foetida truncate, choose clean;
Above-mentioned raw materials is packed in the alcohol extraction jar, add 60% ethanol of 3 times of amounts, boiled 1 hour, steam pressure is 0.4MPa, alcohol reflux;
For the first time carry pure after-filtration, divide other filtrate to close filtering residue, filtrate is reclaimed ethanol by the concentrating under reduced pressure jar, stop to reclaim until ethanol＜60% that reclaims, dope continue to concentrate concentrated solution;
Filtering residue adds 60%～95% ethanol of 3 times of amounts for the second time, boils 1 hour, and steam pressure is 0.4MPa, and alcohol reflux stops to reclaim until ethanol＜60% that reclaims, and filters win filtrate and filtering residue;
Filtering residue adds 6 times of water gagings, boils 1 hour, and steam pressure is 1MPa, filters, and obtains second filtrate and filtering residue respectively, discards filtering residue;
Concentrated solution, first filtrate, second filtrate mixed and be concentrated into D=0.8 promptly get Serissa foetida extractum;
The extractum container of packing into, cold preservation is preserved down in 1 ℃;
The extractum spray dryer of packing into, inlet temperature is 180 ℃, leaving air temp is 70 ℃, promptly gets extract dry powder.
Second embodiment:
A kind of preparation method of Serissa foetida extract,
Gather the Serissa foetida truncate, choose clean;
Above-mentioned raw materials is packed in the alcohol extraction jar, add 70% ethanol of 5 times of amounts, boiled 1～3 hour, steam pressure is 0.75MPa, alcohol reflux;
For the first time carry pure after-filtration, divide other filtrate to close filtering residue, filtrate is reclaimed ethanol by the concentrating under reduced pressure jar, stop to reclaim until ethanol＜60% that reclaims, dope continue to concentrate concentrated solution;
Filtering residue adds 60%～95% ethanol of 5 times of amounts for the second time, boils 2 hours, and steam pressure is 0.5MPa, and alcohol reflux stops to reclaim until ethanol＜60% that reclaims, and filters win filtrate and filtering residue;
Filtering residue adds 7 times of water gagings, boils 2 hours, and steam pressure is 1.1MPa, filters, and obtains second filtrate and filtering residue respectively, discards filtering residue;
Concentrated solution, first filtrate, second filtrate mixed and be concentrated into D=1.2 promptly get Serissa foetida extractum; The extractum container of packing into, cold preservation is preserved down in 3 ℃; The extractum spray dryer of packing into, inlet temperature is 190 ℃, leaving air temp is 80 ℃, promptly gets extract dry powder
The 3rd embodiment:
A kind of preparation method of Serissa foetida extract,
Gather the Serissa foetida truncate, choose clean;
Above-mentioned raw materials is packed in the alcohol extraction jar, add 95% ethanol of 6 times of amounts, boiled 3 hours, steam pressure is 0.7MPa, alcohol reflux;
For the first time carry pure after-filtration, divide other filtrate to close filtering residue, filtrate is reclaimed ethanol by the concentrating under reduced pressure jar, stop to reclaim until ethanol＜60% that reclaims, dope continue to concentrate concentrated solution;
Filtering residue adds 95% ethanol of 6 times of amounts for the second time, boils 3 hours, and steam pressure is 0.7MPa, and alcohol reflux stops to reclaim until ethanol＜60% that reclaims, and filters win filtrate and filtering residue;
Filtering residue adds 9 times of water gagings, boils 3 hours, and steam pressure is 1.3MPa, filters, and obtains second filtrate and filtering residue respectively, discards filtering residue;
Concentrated solution, first filtrate, second filtrate mixed and be concentrated into D=1.5 promptly get Serissa foetida extractum; The extractum container of packing into, cold preservation is preserved down in 1 ℃～5 ℃;
The extractum spray dryer of packing into, inlet temperature is 195 ℃, leaving air temp is 90 ℃, promptly gets extract dry powder
The above mainly is that the extract with Serissa foetida is made as dry powder, again with the additive of dry powder as beverage, drinks for people.
But extract can also be made as other arbitrary shape, and can be, or as the additive of beauty and skin care product with it as food additives.
It should be noted that at last: above embodiment only in order to the explanation the present invention and and unrestricted technical scheme described in the invention; Therefore, although this description has been described in detail the present invention with reference to each above-mentioned embodiment,, those of ordinary skill in the art should be appreciated that still and can make amendment or be equal to replacement the present invention; And all do not break away from the technical scheme and the improvement thereof of the spirit and scope of invention, and it all should be encompassed in the middle of the claim scope of the present invention.
Claims (3)
1. the preparation method of a Serissa foetida extract is characterized in that:
Step 1; Gather the Serissa foetida truncate, choose clean;
Step 1.1; Above-mentioned raw materials is packed in the alcohol extraction jar, add 60%～95% ethanol of 3～6 times of amounts, boiled 1～3 hour, steam pressure is 0.4MPa～0.7MPa, alcohol reflux;
Step 1.2; For the first time carry pure after-filtration, divide other filtrate to close filtering residue, filtrate is reclaimed ethanol by the concentrating under reduced pressure jar, stop to reclaim until ethanol＜60% that reclaims, dope continue to concentrate concentrated solution;
Step 1.3; Filtering residue adds 60%～95% ethanol of 3～6 times of amounts for the second time, boils 1～3 hour, and steam pressure is 0.4MPa～0.7MPa, and alcohol reflux stops to reclaim until ethanol＜60% that reclaims, and filters win filtrate and filtering residue;
Step 1.4; Filtering residue adds 6～9 times of water gagings, boils 1～3 hour, and steam pressure is 1MPa～1.3MPa, filters, and obtains second filtrate and filtering residue respectively, discards filtering residue;
Step 1.5; Concentrated solution, first filtrate, second filtrate mixed and be concentrated into D=0.8～1.5 promptly get Serissa foetida extractum;
Step 1.6; The extractum container of packing into, cold preservation is preserved down in 1 ℃～5 ℃;
Step 1.7; The extractum spray dryer of packing into, inlet temperature is 180 ℃～195 ℃, leaving air temp is 70 ℃～90 ℃, promptly gets extract dry powder.
According to claim 1 described the preparation method of Serissa foetida extract, it is characterized in that: described concentrated solution, first filtrate, second filtrate concentrated is respectively concentrating under reduced pressure or the interlayer concentration tank concentrates.
3. according to the described preparation method that gets Serissa foetida extract of claim 1, it is characterized in that: described extract is: aqueous or capsule shape or ball shape or graininess or diffusing shape.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810200874A CN101711784A (en) | 2008-10-08 | 2008-10-08 | Preparation method of serissa serissoide extractive |
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| CN200810200874A CN101711784A (en) | 2008-10-08 | 2008-10-08 | Preparation method of serissa serissoide extractive |
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| CN101711784A true CN101711784A (en) | 2010-05-26 |
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| CN200810200874A Pending CN101711784A (en) | 2008-10-08 | 2008-10-08 | Preparation method of serissa serissoide extractive |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109619661A (en) * | 2019-01-11 | 2019-04-16 | 广西中烟工业有限责任公司 | A kind of preparation method of serissa extract and its application in cigarette |
| CN110447746A (en) * | 2019-09-11 | 2019-11-15 | 胡玉涛 | A kind of Poria cocos coffee beverage and its production method |
-
2008
- 2008-10-08 CN CN200810200874A patent/CN101711784A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109619661A (en) * | 2019-01-11 | 2019-04-16 | 广西中烟工业有限责任公司 | A kind of preparation method of serissa extract and its application in cigarette |
| CN110447746A (en) * | 2019-09-11 | 2019-11-15 | 胡玉涛 | A kind of Poria cocos coffee beverage and its production method |
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Open date: 20100526 |