CN1016874B - Wine turbidity removing method - Google Patents
Wine turbidity removing methodInfo
- Publication number
- CN1016874B CN1016874B CN 89100310 CN89100310A CN1016874B CN 1016874 B CN1016874 B CN 1016874B CN 89100310 CN89100310 CN 89100310 CN 89100310 A CN89100310 A CN 89100310A CN 1016874 B CN1016874 B CN 1016874B
- Authority
- CN
- China
- Prior art keywords
- wine
- polygorskite
- adsorbent
- contactor
- clarification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 20
- 235000014101 wine Nutrition 0.000 title abstract description 48
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 4
- 239000011521 glass Substances 0.000 claims abstract description 4
- 239000004033 plastic Substances 0.000 claims abstract description 3
- 229920003023 plastic Polymers 0.000 claims abstract description 3
- 239000002594 sorbent Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 239000004411 aluminium Substances 0.000 claims description 3
- 230000008929 regeneration Effects 0.000 claims description 3
- 238000011069 regeneration method Methods 0.000 claims description 3
- 230000008595 infiltration Effects 0.000 claims description 2
- 238000001764 infiltration Methods 0.000 claims description 2
- 239000007769 metal material Substances 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- 238000005352 clarification Methods 0.000 abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 4
- 229910052625 palygorskite Inorganic materials 0.000 abstract description 3
- 235000019990 fruit wine Nutrition 0.000 abstract description 2
- 239000003463 adsorbent Substances 0.000 abstract 3
- 239000000919 ceramic Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- 239000000796 flavoring agent Substances 0.000 description 6
- 235000019634 flavors Nutrition 0.000 description 6
- 235000013372 meat Nutrition 0.000 description 5
- 238000007710 freezing Methods 0.000 description 4
- 230000008014 freezing Effects 0.000 description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 241000227425 Pieris rapae crucivora Species 0.000 description 2
- 244000061456 Solanum tuberosum Species 0.000 description 2
- 235000002595 Solanum tuberosum Nutrition 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- XIRNKXNNONJFQO-UHFFFAOYSA-N ethyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC XIRNKXNNONJFQO-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 235000009973 maize Nutrition 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- 235000019991 rice wine Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- LVGKNOAMLMIIKO-UHFFFAOYSA-N Elaidinsaeure-aethylester Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC LVGKNOAMLMIIKO-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- FMMOOAYVCKXGMF-MURFETPASA-N ethyl linoleate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCC FMMOOAYVCKXGMF-MURFETPASA-N 0.000 description 1
- 229940031016 ethyl linoleate Drugs 0.000 description 1
- LVGKNOAMLMIIKO-QXMHVHEDSA-N ethyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC LVGKNOAMLMIIKO-QXMHVHEDSA-N 0.000 description 1
- 229940093471 ethyl oleate Drugs 0.000 description 1
- 229940067592 ethyl palmitate Drugs 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- -1 fatty acid esters Chemical class 0.000 description 1
- 244000144992 flock Species 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- FMMOOAYVCKXGMF-UHFFFAOYSA-N linoleic acid ethyl ester Natural products CCCCCC=CCC=CCCCCCCCC(=O)OCC FMMOOAYVCKXGMF-UHFFFAOYSA-N 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
Images
Landscapes
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
A method for removing turbidity of wine relates to a clarification method in wine brewing processing, and aims to provide an adsorbent and a clarification method which have the advantages of wide application range, no influence on wine taste, short treatment time, good effect, low cost and simple device. The invention uses the palygorskite after treatment as the adsorbent, and the palygorskite is filled in a container made of glass, plastic, ceramic or aluminum material, and the wine is clarified after passing through the container. The adsorbent can be regenerated after saturation, and the clarified wine is not turbid after being placed for several months to one year or cooled to below-10 ℃. It is suitable for production of various kinds of fragrant white spirit, low alcohol wine, fruit wine, yellow wine, etc.
Description
The present invention relates to brewageing, processing of drinks in the biological chemistry, specifically, relate to the defecation method of drinks.
As everyone knows, inebriant, comprise liquor, yellow rice wine and fruit juice wine, its brewage, in processing and the transporting procedures, turbid phenomenon can appear in some cases, for example in the still-process of wine, can floating oil droplet on the wine tail and muddiness occurs, and for example white flocks also can appear in high wine in low temperature environment; Make low alcohol with high wine for another example, reduce and also turbid phenomenon can occur when wine is spent adding entry, according to the study, cause that drinks produces the material of turbid phenomenon, be some high boiling fatty acid esters, mainly contain under ethyl palmitate, ethyl oleate and ethyl linoleate, the solubility with temperature of these ester classes in alcohol low and reduce.At low temperatures or wine degree when reducing,, be suspended in the wine, cause muddiness because these ester solubleness declines are separated out.Drinks produces the muddy aesthetic quality that can influence wine greatly, causes human consumer's apprehensions psychology.
Existing purifying method for wine mainly contains two kinds: a kind of is to adopt to go turbid sorbent material suction to go the ester class that can suspend out in the wine; Another kind is to adopt freezing method earlier these ester classes to be separated out elimination.Present existing cleaning agent has active carbon powder, starch, Mierocrystalline cellulose, ion exchange resin, wilkinite, agar, fat meat etc., these go turbid sorbent material to exist a series of shortcoming in various degree: 1. adsorption time is long, the shortest (as gac) needs 8-48 hour, the longest (as fat meat) needs the 3-6 month, 2. except that gac, existing most sorbent material all has the scope of best clarification wine degree, can not be adapted to various wine degree; 3. sorbent material such as agar, fat meat clarifying effect is not really desirable; 4. the adsorption filtration device of using these sorbent materials is more complicated all.5. the unit cost of clarifying process is than higher, by 87 years price-level costs minimum (as wilkinite, handle wine per ton and need 0.4-2 unit, (as gac, the fat meat) that cost is the highest is handled wine per ton and is needed 5-6 unit.6. the sorbent material that has (as starch, fat meat, gac) can bring certain influence to the mouthfeel of wine, even can change the original local flavor of wine.Though the freezing local flavor that goes turbid method can not change wine, the power drain height can increase facility investment and processing cost.
The object of the present invention is to provide a kind of have clarification wine degree scope wide, the local flavor of wine is had no effect, the treatment time is short, clarifying effect good, and is with low cost, adsorption unit is simple, maneuverable sorbent material and adsorption method thereof.
In order to realize this purpose, the contriver is by research, and (have another name called Palygorskite, structure is (Mg to select a kind of aluminium magensium silicate clay mineral-polygorskite for use
5) (Si
8) O
20(OH)
2(OH
2)
44H
2O, (Mg
4) (Si
6) O
15(OH)
2(OH
2)
24H
2O, MgO(Si
12O
30) (OH)
48H
2O) as sorbent material, drinks is removed muddy thing by the contactor of loading polygorskite.
Adopting the polygorskite that comes from the mine is massive ore, should not directly be used as sorbent material, need with after the clear water infiltration, adopt artificial or after mechanical workout tears up, drying and getting again, these sorbent materials are contained in the contactor made from non-metallic material such as glass, plastics, pottery or aluminium, again the wine of muddiness are like that directly passed through this contactor as the routine operation, then can obtain transparent wine product.Absorption proceeds to certain hour, sorbent material reach saturated after, it will be reused after taking out oven dry regeneration.
Method of the present invention is applicable to any wine degree scope; Local flavor to wine has no effect; Adsorption time is extremely short, and as long as drinks realizes going turbid, clarification immediately by contactor; Clarifying effect is fabulous, through clarification, go the wine after turbid to place 1 year, no matter is in room temperature or below-10 ℃, all can keep transparent; The filtration clarifying plant is simple; Handle the required processing cost of wine per ton and be lower than wilkinite; It is easy that the taking off of sorbent material inhaled regeneration, can use repeatedly.The present invention is applicable to the various aromatic white spirits of clarification, low alcohol white spirit, fruit wine, yellow rice wine etc.
Accompanying drawing is the schematic flow sheet of the inventive method, and 1 for supplying vinasse, and 2 is the wine pump, and 3 is header tank, and 4 is adsorption column, and 5 is the polygorskite sorbent material, and 6 is the pure mellow wine groove.
Embodiment 1: dress polygorskite sorbent material in the adsorption column made from Glass tubing is used to clarify Jinhua, Guizhou Province liquor.Wine is contained in in the vinasse, squeezes into header tank with the wine pump, utilizes potential difference to flow into adsorption column automatically, and the wine after absorption, clarification is filled into bottle.The assay of wine is before the clarification: water white transparency, micro-foreign matter is arranged, and have the common white spirit local flavor, 47.9 ° of wine degree, total acid 0.78g/l, total ester 1.57g/l, solid substance 0.08g/l, methyl alcohol does not detect, potato spirit 0.20g/100ml, plumbous, manganese does not all detect.The assay of clarification back wine is: water white transparency, have the common white spirit local flavor, and 47.9 ° of wine degree, total acid 0.78g/l: total ester 1.57g/l, solid substance 0.09g/l, methyl alcohol do not detect, potato spirit 0.20g/100ml, plumbous, manganese does not all detect.The index that meets the GB2757-81 standard.
Embodiment 2: adsorption method with embodiment 1, be used to clarify the maize liquor of Pan county, Guizhou Province official Liu brewery, this wine is 47 °, the muddiness that is white in color under the normal temperature leaves standstill after 8 hours and still to be white opacity, is refrigerated to that muddiness increases the weight of below-10 ℃; After the clarification of polygorskite adsorption column, left standstill 15 months or freezing arriving below-10 ℃, this wine is transparent.
Embodiment 3: adsorption method is with embodiment 1, be used to clarify the low alcohol that brewery is closed at county town, Xingyi, Guizhou Province, this wine system becomes 38 ° with 50 ° of maize liquor thin ups, is white opacity under the room temperature, leave standstill after 8 hours and still to be white opacity, be refrigerated to that muddiness increases the weight of below-10 ℃; After the clarification of polygorskite adsorption column, to place after nine months or freezing arriving below-10 ℃, this wine is all transparent.
Claims (3)
1, a kind of liquor of making sorbent material with polygorskite removes purifying method, it is characterized in that used polygorskite needs earlier with adopting artificial behind the water infiltration or machinery tears up, and again through oven dry and get, then drinks is removed muddy thing by the contactor that is filled with polygorskite.
2, in accordance with the method for claim 1, wherein used contactor can be cylindrical container, tower other shapes of containers made from non-metallic material such as glass, plastics, pottery or aluminium.
3, in accordance with the method for claim 1, it is characterized in that polygorskite absorption in the contactor reach saturated after, must reuse by oven dry regeneration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89100310 CN1016874B (en) | 1989-01-14 | 1989-01-14 | Wine turbidity removing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89100310 CN1016874B (en) | 1989-01-14 | 1989-01-14 | Wine turbidity removing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1044124A CN1044124A (en) | 1990-07-25 |
| CN1016874B true CN1016874B (en) | 1992-06-03 |
Family
ID=4853799
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 89100310 Expired CN1016874B (en) | 1989-01-14 | 1989-01-14 | Wine turbidity removing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1016874B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100341877C (en) * | 2005-12-08 | 2007-10-10 | 侯金荣 | Method for extracting artemisinin |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1049007C (en) * | 1995-06-16 | 2000-02-02 | 刘淑华 | Method for solving precipitation of fruit wine |
| CN1333063C (en) * | 2005-12-07 | 2007-08-22 | 梁音 | Method for purifying spirit liquor by nano-porcelain small balls |
| CN101787339B (en) * | 2010-03-18 | 2012-07-18 | 淮阴工学院 | Attapulgite clay-based purifying and aging agent used for wine and preparation method thereof |
-
1989
- 1989-01-14 CN CN 89100310 patent/CN1016874B/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100341877C (en) * | 2005-12-08 | 2007-10-10 | 侯金荣 | Method for extracting artemisinin |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1044124A (en) | 1990-07-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C13 | Decision | ||
| GR02 | Examined patent application | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |