CN101683182A - Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product - Google Patents
Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product Download PDFInfo
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- CN101683182A CN101683182A CN200810197141A CN200810197141A CN101683182A CN 101683182 A CN101683182 A CN 101683182A CN 200810197141 A CN200810197141 A CN 200810197141A CN 200810197141 A CN200810197141 A CN 200810197141A CN 101683182 A CN101683182 A CN 101683182A
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- CN
- China
- Prior art keywords
- radix isatidis
- cordate houttuynia
- extract
- compound extract
- feed liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000284 extract Substances 0.000 title claims abstract description 74
- 235000013717 Houttuynia Nutrition 0.000 title claims abstract description 63
- 239000010231 banlangen Substances 0.000 title claims abstract description 61
- 150000001875 compounds Chemical class 0.000 title claims abstract description 41
- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 25
- 239000000654 additive Substances 0.000 title claims abstract description 18
- 230000000996 additive effect Effects 0.000 title claims abstract description 18
- 240000000691 Houttuynia cordata Species 0.000 title abstract 3
- 241000132004 Symphyotrichum cordifolium Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 27
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 27
- 239000007788 liquid Substances 0.000 claims abstract description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000006227 byproduct Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 239000011347 resin Substances 0.000 claims abstract description 9
- 229920005989 resin Polymers 0.000 claims abstract description 9
- 239000003205 fragrance Substances 0.000 claims abstract description 8
- 230000001105 regulatory effect Effects 0.000 claims abstract description 7
- 239000003513 alkali Substances 0.000 claims abstract description 4
- 241000758769 Houttuynia Species 0.000 claims description 60
- 235000019504 cigarettes Nutrition 0.000 claims description 30
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 7
- 239000003480 eluent Substances 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 5
- 239000003546 flue gas Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 238000002955 isolation Methods 0.000 claims description 2
- 239000002798 polar solvent Substances 0.000 claims description 2
- 239000000779 smoke Substances 0.000 abstract description 4
- 238000000605 extraction Methods 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 abstract 4
- 241000758794 Asarum Species 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000334160 Isatis Species 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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Abstract
The invention relates to a heartleaf houttuynia herb and radix isatidis compound extract and application thereof as an additive of a tobacco product. A preparation method comprises the following steps: first adding alkali into an extracting agent, regulating the pH value of the extracting agent to 8.5-10.5, ensuring the weight ratio of the heartleaf houttuynia herb to the radix isatidis to be 10-20:1 and the weight ratio of the extracting agent to the extracting materials to be 5-10:1, carrying out extraction for 1-5h at 50-90 DEG C, concentrating feed liquid until the volume of the feed liquid is 1/6 of the original volume after separating out the feed liquid, using AB-8 macroporous resins to separate concentrated liquid, collecting eluant with ethanol concentration of 40-60% and concentrating the eluant into an extract, using 5-10 times of extracting agent to re-dissolve the extract, filtering and separating by-products again and concentrating the feed liquid into an extract again, thus obtaining the extract of the invention. The extract can be added into the cut tobaccos as the additive of the tobacco product, can effectively increase fragrance when the tobacco product is smoked, has rich fragrance, improves firm feel of smoke and can endow the tobacco product with unique note.
Description
Technical field
The present invention relates to the application of a kind of natural plant extracts in tobacco product, specifically a kind of cordate houttuynia and radix isatidis compound extract and as the purposes of additive of tobacco product.
Background technology
" Chinese style cigarette " core competitiveness is to form the selling point style, embodies personalization and differentiation, adapts to sucking of Chinese consumers in general and is accustomed to and consumer need.Chinese style cigarette essence and flavoring agent is Chinese style cigarette product " soul ", is the secret place that " Chinese style cigarette " style characteristic forms.Flavoring and casing scientifically in cigarette, the important means of the personalized style of outstanding cigarette product just.Simultaneously, in order to improve the security of smoking, lowering harm and decreasing coking becomes an important component part of " Chinese style cigarette ".When reducing coke tar in cigarette, promote and raising flue gas concentration and fragrance, also only by means of the flavoring and casing technology.Along with going deep into of Chinese style cigarette lowering harm and decreasing coking work, reinforced its importance that demonstrates further of tobacco flavoring.Extracting essence and flavoring agent from the natural herbal plant, succession Chinese herbal medicine in thousand is used for cigarette, allow healthy theory along with the refined perfume (or spice) of cigarette, move towards the consumer together, is one of basic research of development " Chinese style cigarette ".
Cordate houttuynia has the fragrance style of self uniqueness, and contains abundant flavonoids in the cordate houttuynia, has the prospect as essence spice for cigarette.And Radix Isatidis has the effect of removing peroxy radical, can be used for the work of cigarette harm reduction.But the achievement in research that sees report at present has only both to be used in Chinese medicine and the correlated product, and not seeing has the bibliographical information that is used to cigarette additive.And in our research process, discovery is simple to have bigger negative effect by resulting independent houttuynia extract of conventional extraction process or isatis root extract, can't satisfy the instructions for use as cigarette additive.
Summary of the invention
Purpose of the present invention is exactly the defective at prior art, provides a kind of cordate houttuynia and radix isatidis compound extract and as the purposes of additive of tobacco product.
Technical scheme of the present invention is achieved in that it is to adopt cordate houttuynia and Radix Isatidis for extracting raw material, with the polar solvent is extractant, carry out abstraction reaction, adopting the macroporous resin column isolation technics will extract byproduct separates, again feed liquid is concentrated into the medicinal extract shape, use extractant Hui Rong, isolated by filtration once more, the gained feed liquid is extract of the present invention.
Wherein said extractant is 30～80% ethanol water, and wherein the weight ratio of cordate houttuynia and Radix Isatidis is 10～20: 1.
Extracting method of the present invention is to adopt cordate houttuynia and Radix Isatidis for extracting raw material, specifically may further comprise the steps: earlier alkali is joined in the extractant, regulating extractant pH value is 8.5～10.5, extractant is 5～10: 1 with the weight ratio of extracting raw material, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, returns molten medicinal extract with 5～10 times of extractants, once more the isolated by filtration byproduct, feed liquid is concentrated into the medicinal extract shape once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.
Wherein the weight ratio of cordate houttuynia and Radix Isatidis is 10～20: 1, and described extractant is 30～80% ethanol water.
The present invention is the purposes of additive of tobacco product, it is that cordate houttuynia and radix isatidis compound extract are added in the pipe tobacco of cigarette, the cordate houttuynia and the radix isatidis compound extract that are added in the pipe tobacco account for 0.01%～0.05% of pipe tobacco weight, flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas.The cordate houttuynia and the radix isatidis compound extract that wherein are added in the pipe tobacco preferably account for 0.02%～0.04% of pipe tobacco weight.
The present invention is during as the purposes of additive of tobacco product, preferably cordate houttuynia and radix isatidis compound extract are dissolved in 95% the ethanol, the alcohol solvent that is dissolved with cordate houttuynia and radix isatidis compound extract rolled at the pipe tobacco of production of cigarettes be sprayed in the process on the pipe tobacco, subsequently evaporating solvent.
Extracting method of the present invention technical scheme preferably is that described alkali is NaOH, calcium hydroxide, ammoniacal liquor or sodium carbonate;
A series of experimental study results that smoke panel test of patent applicant show, the cordate houttuynia of adding and radix isatidis compound extract flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas; And cordate houttuynia and radix isatidis compound extract can also be given the aromatic and the note of tobacco product uniqueness.And when improving the tobacco product mouthfeel, can avoid introducing negative effects such as assorted gas, increase excitant.
The present invention has opened up a new application for cordate houttuynia and radix isatidis compound extract, has increased new effect of cordate houttuynia and Radix Isatidis and effect.Cordate houttuynia and radix isatidis compound extract are as additive of tobacco product, and effect is obvious, and " Chinese style cigarette " goods of developing characteristic style are had good application prospects.
Description of drawings
Fig. 1 is a process schematic representation of the present invention.
The specific embodiment
The present invention is described further below by embodiment.
The extraction of embodiment 1 cordate houttuynia and Radix Isatidis
The weight ratio of cordate houttuynia and Radix Isatidis is 10: 1, earlier NaOH is joined in 75% ethanol water, regulating ethanol water pH value is 9.5, the weight ratio of ethanol water and cordate houttuynia and Radix Isatidis is 6: 1, extracted 3 hours at 90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, and density is 1.1, with 8 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.This extract can be used for additive of tobacco product.
Embodiment 2
Cordate houttuynia and Radix Isatidis weight ratio are 15: 1, earlier ammoniacal liquor is joined in 75% ethanol water, regulating ethanol water pH value is 8.5, ethanol water and cordate houttuynia and Radix Isatidis weight ratio are 8: 1, extracted 4 hours at 50 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, and density is 1.3, with 8 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.This extract can be used for additive of tobacco product.
Embodiment 3
Cordate houttuynia and Radix Isatidis weight ratio are 18: 1, earlier calcium hydroxide is joined in 75% ethanol water, regulating ethanol water pH value is 10.0, ethanol water and cordate houttuynia and Radix Isatidis weight ratio are 10: 1, extracted 2 hours at 60 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, and density is 1.2, with 5 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.This extract can be used for additive of tobacco product.
Embodiment 4
Cordate houttuynia and Radix Isatidis weight ratio are 20: 1, earlier sodium carbonate is joined in 75% ethanol water, regulating ethanol water pH value is 9.0, ethanol water with cordate houttuynia and Radix Isatidis weight ratio be 9: 1, extracted 5 hours at 80 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, and density is 1.2, with 6 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.This extract can be used for additive of tobacco product.
Embodiment 5 adds the extract that is obtained in the pipe tobacco of cigarette
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.Be added into cordate houttuynia and radix isatidis compound extract in the pipe tobacco, account for 0.03% of pipe tobacco weight.Concrete grammar is earlier cordate houttuynia and radix isatidis compound extract to be dissolved in the ethanol, and the Diluted Alcohol that is dissolved with cordate houttuynia and radix isatidis compound extract evenly is sprayed on the pipe tobacco, and ethanol evaporation is fallen subsequently.Pipe tobacco rolls into test sample cigarette through cigarette machine.
Effect experiment in embodiment 6 cigarette smokes
Be taken at two parts of the good finished cut tobacco of 22 ℃ ± 1 ℃ of temperature and 60% ± 2% time balance of relative humidity (RH) 40 grams, take by weighing cordate houttuynia and radix isatidis compound extract by 0.04% of its quality, after the dilution of 95% ethanol, be sprayed on the pipe tobacco equably with the larynx jet pipe, perfuming and not the aromatic tobacco sample be placed in the climatic chamber of 22 ℃ ± 1 ℃ of temperature and RH60% ± 2% balance 48 hours, with fill out the cigarette device respectively with perfuming and not the pipe tobacco of perfuming make cigarette and prop up, 22 ℃ ± 1 ℃ and RH60% ± 2% time balance 48 hours, please cigarette sensory evaluating smoking group smoke panel test again.
The personnel that smoke panel test are consistent to think the cordate houttuynia that adds and radix isatidis compound extract flavouring effectively when tobacco product aspirate, and fragrance is abundant, the solid sense of increase flue gas; And cordate houttuynia and radix isatidis compound extract can also be given the aromatic and the note of cigarette uniqueness.
Claims (10)
1, a kind of cordate houttuynia and radix isatidis compound extract, it is to adopt cordate houttuynia and Radix Isatidis for extracting raw material, with the polar solvent is extractant, carry out abstraction reaction, adopt the macroporous resin column isolation technics will extract byproduct and separate, again feed liquid is concentrated into the medicinal extract shape, use extractant Hui Rong, isolated by filtration once more, the gained feed liquid is extract of the present invention.
2, cordate houttuynia according to claim 1 and radix isatidis compound extract, wherein said extractant are 30～80% ethanol water.
3, cordate houttuynia according to claim 1 and radix isatidis compound extract, wherein the weight ratio of cordate houttuynia and Radix Isatidis is 10～20: 1.
4, cordate houttuynia according to claim 1 and radix isatidis compound extract, wherein extractant is 5～10: 1 with the weight ratio of extracting raw material
5, the extracting method of a kind of cordate houttuynia and radix isatidis compound extract, it adopts cordate houttuynia and Radix Isatidis for extracting raw material, specifically may further comprise the steps: earlier alkali is joined in the extractant, regulating extractant pH value is 8.5～10.5, extractant is 5～10: 1 with the weight ratio of extracting raw material, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, feed liquid is concentrated into 1/6 of original volume, with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting concentration of alcohol 40-60% is concentrated into the medicinal extract shape, return molten medicinal extract with 5～10 times of extractants, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains cordate houttuynia of the present invention and radix isatidis compound extract.
6, the extracting method of cordate houttuynia according to claim 5 and radix isatidis compound extract, wherein the weight ratio of cordate houttuynia and Radix Isatidis is 10～20: 1.
7, the extracting method of cordate houttuynia according to claim 5 and radix isatidis compound extract, wherein said extractant are 30～80% ethanol water.
8, a kind of cordate houttuynia and radix isatidis compound extract are as the purposes of additive of tobacco product, it is that cordate houttuynia and radix isatidis compound extract are added in the pipe tobacco of cigarette, the cordate houttuynia and the radix isatidis compound extract that are added in the pipe tobacco account for 0.01%～0.05% of pipe tobacco weight, flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas.
9, cordate houttuynia according to claim 8 and radix isatidis compound extract are as the purposes of additive of tobacco product, and the cordate houttuynia and the radix isatidis compound extract that wherein are added in the pipe tobacco account for 0.02%～0.04% of pipe tobacco weight.
10, cordate houttuynia according to claim 8 and radix isatidis compound extract are as the purposes of additive of tobacco product, wherein cordate houttuynia and radix isatidis compound extract are dissolved in 95% the ethanol, the alcohol solvent that is dissolved with cordate houttuynia and radix isatidis compound extract is rolled in the process at the pipe tobacco of production of cigarettes are sprayed on the pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101971411A CN101683182B (en) | 2008-09-27 | 2008-09-27 | Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101971411A CN101683182B (en) | 2008-09-27 | 2008-09-27 | Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101683182A true CN101683182A (en) | 2010-03-31 |
| CN101683182B CN101683182B (en) | 2012-07-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2008101971411A Expired - Fee Related CN101683182B (en) | 2008-09-27 | 2008-09-27 | Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415611A (en) * | 2011-07-24 | 2012-04-18 | 红云红河烟草(集团)有限责任公司 | Tobacco charging method for promoting using effect of tobacco spice |
| CN102754904A (en) * | 2011-04-25 | 2012-10-31 | 湖北中烟工业有限责任公司 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
| CN107129867A (en) * | 2017-04-27 | 2017-09-05 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl Radix Isatidis essence and its application in cigarette |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1548104A (en) * | 2003-05-24 | 2004-11-24 | 毛友昌 | Compound cordate bouttuynia bolus and its prepn |
| CN101040950B (en) * | 2007-04-29 | 2012-02-22 | 江西天施康中药股份有限公司 | Method of preparing compound Houttuynia cordata dropping pills |
-
2008
- 2008-09-27 CN CN2008101971411A patent/CN101683182B/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102754904A (en) * | 2011-04-25 | 2012-10-31 | 湖北中烟工业有限责任公司 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
| CN102754904B (en) * | 2011-04-25 | 2014-10-29 | 湖北中烟工业有限责任公司 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
| CN102415611A (en) * | 2011-07-24 | 2012-04-18 | 红云红河烟草(集团)有限责任公司 | Tobacco charging method for promoting using effect of tobacco spice |
| CN102415611B (en) * | 2011-07-24 | 2013-04-03 | 红云红河烟草(集团)有限责任公司 | Tobacco charging method for promoting using effect of tobacco spice |
| CN107129867A (en) * | 2017-04-27 | 2017-09-05 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl Radix Isatidis essence and its application in cigarette |
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| Publication number | Publication date |
|---|---|
| CN101683182B (en) | 2012-07-04 |
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