CN101659902A - Method and equipment for grease deodorization - Google Patents

Method and equipment for grease deodorization Download PDF

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Publication number
CN101659902A
CN101659902A CN200910063659A CN200910063659A CN101659902A CN 101659902 A CN101659902 A CN 101659902A CN 200910063659 A CN200910063659 A CN 200910063659A CN 200910063659 A CN200910063659 A CN 200910063659A CN 101659902 A CN101659902 A CN 101659902A
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China
Prior art keywords
grease
deodorization
tank
deodorizing tank
steam
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CN200910063659A
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Chinese (zh)
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CN101659902B (en
Inventor
唐孝鹏
汪志明
李翔宇
周强
耿安锋
张敏
肖子豪
肖敏
杨金涛
马凡提
尚耘
向丽
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Limited By Share Ltd Biotechnology (wuhan) Co Ltd
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Cargill Alking Bioengineering Wuhan Co Ltd
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Abstract

The invention relates to a method and equipment for grease deodorization. The equipment is provided with a deodorization tank which is connected with a vacuum pump to pump the deodorization tank to bein a vacuum state; the temperature in the deodorization tank is maintained at 200+/-20 DEG C; an atomizing spray gun is arranged in the deodorization tank; the input end of the atomizing spray gun isrespectively connected with a steam channel and a grease channel; in the grease channel, the temperature of the grease reaches 200+/-20 DEG C; the grease is pressed to a spray nozzle through the grease channel, and the grease and the steam are mixed to be sprayed and atomized in the deodorization tank, wherein the atomized grease and the steam fly to the lower part of the deodorization tank underthe action of the atomized pressure, volatilized components and steam in the grease are pumped by the vacuum pump, and qualified grease falls at the bottom of the deodorization tank, flows into an oil storage tank and enters the next process. The grease has good deodorization effect and high processing efficiency, can effectively reduce the form of trans-fatty acid and achieve good quality of refined grease; a better refining effect can be achieved by secondary deodorization; and the method and the equipment have simple structure and low manufacturing cost and are convenient to popularize andapply.

Description

A kind of grease deodorization method and apparatus
Technical field
The present invention relates to a kind of method and apparatus of grease deodorization, be directed to the deodorization of food oils especially, belong to grease processing technology field.
Background technology
Greasy refining will just can make quality, color and luster, the smoke point of oil reach the requirement of using and eating through alkali refining, decolouring, deodorization.At present for greasy deodorizing technology, main method is after grease is heated to certain temperature, under high vacuum, feed steam, volatile substances gas in the grease is put forward, reach deodorization and refining greasy purpose, therefore the equipment of corresponding use is based on also that this technology designs, its subject matter is that equipment is long to the grease warm-up time, and temperature is more than 250 degree, easy output trans fatty acid, thus influence greasy food safety.The functional grease of existing market mass selling contains unsaturated fatty acids more, but adopts traditional grease deodorization method, will cause the generation of trans fatty acid, and reduces the grease production yield.
Up-to-date oil refining process is the technology that adopts molecular distillation, can effectively reduce the temperature and time of refining and deodorizing, guarantee greasy quality, but the cost of this technology equipment used is more expensive, causes the increase of grease tooling cost.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of grease deodorization method and apparatus at the deficiency of above-mentioned prior art existence, it not only can effectively improve the effect of grease deodorization, reduce the formation of trans fatty acid, and technology is simple and effective, device structure is simple, cost is low, and is easy to utilize.
The technical scheme of the inventive method is:
The configuration deodorizing tank, deodorizing tank links to each other with vacuum pump and makes the deodorizing tank state that is evacuated, make by the heating, temperature keeping device that temperature remains on 200 ± 20 ℃ in the deodorizing tank, the atomizing spray is set in the deodorizing tank robs, the input terminus of atomizing lance joins with vapour passage and grease channel respectively, and the pressurization of heating of the grease for the treatment of deodorization processing in grease channel makes the grease temperature reach 200 ± 20 ℃, by grease channel grease is pressed onto the nozzle place, is ejected in the deodorizing tank with vapor mixing and atomizes; Fly in the grease of atomizing and the steam bottom to deodorizing tank under the effect of atomizing pressure, because vacuum and temperature action, volatile component and steam in the grease are extracted out by vacuum pump, and qualified grease falls at the bottom of the deodorizing tank, flow into storage tank, and enter next step technology from vent pipe.
Press such scheme, the volatile component part in the described grease is brought into the capture tank condensation by steam and is reclaimed, and part volatile component and steam are extracted out by vacuum pump.
Press such scheme, the vacuum tightness of described deodorizing tank vacuum state is equal to or less than 1KPa.
Press such scheme, the pressure of steam is 0.2~0.5MPa in the described vapour passage; Grease pressure in the described grease channel is 0.2~0.5MPa.
Press such scheme, the grease of deodorization can be entered next deodorization procedures, carry out the secondary deodorization, temperature and grease temperature are 150 ± 10 ℃ in the deodorizing tank of deodorization for the second time, the vacuum tightness of deodorizing tank vacuum state is equal to or less than 500Pa, and the pressure of steam is 0.1~0.2MPa.The secondary deodorization can further improve greasy refining purity.
The technical scheme of present device is:
Comprise deodorizing tank, storage tank and vacuum pump, it is characterized in that: described deodorizing tank top is connected with vacuum pump by pipeline, the below of deodorizing tank communicates with storage tank, outside deodorizing tank, be installed on the heating, temperature keeping device, being installed on the atomizing spray in the deodorizing tank robs, the input terminus that the atomizing spray is robbed connects steam-pipe and oil pump pipeline respectively, and is connected in series oil heater in the oil pump pipeline.
Press such scheme, the capture tank of connecting band condenser in deodorizing tank and pipeline that vacuum pump links to each other.
Press such scheme, described oil heater makes the temperature of polished fat rise to 200 ± 20 ℃.
Press such scheme, described atomizing lance comprises vapour passage, grease channel and is arranged on the nozzle that the termination is robbed in the atomizing spray; Vapour passage is connected with described steam-pipe, and grease channel is connected with described oil pump pipeline.
Press such scheme, described deodorizing tank is connected by valve with storage tank.
Working process of the present invention is: under vacuum and high temperature action, the grease of ejection is atomized fully, by grease atomizing being made in the grease volatile substances fully separate and being brought into the capture tank condensation by steam in a vacuum with grease, and qualified grease falls the deodorizing tank underflow and goes into storage tank, reaches the effect of grease deodorization.
Beneficial effect of the present invention is: 1, grease deodorization is effective, the working (machining) efficiency height, and can effectively reduce the formation of trans fatty acid, the quality of oil and fat refining is good; 2, complete processing is simply effective, is easy to operate and control, and can reach better refining effect by the secondary deodorization; 3, structure is provided with rationally simply, and the device fabrication cost is low, and is easy to utilize.
Description of drawings
Fig. 1 is the structure iron of an embodiment of present device.
Fig. 2 robs the partial enlarged drawing of nozzle for atomizing spray among Fig. 1.
Fig. 3 is the structure iron of another embodiment of present device.
Embodiment
Further specify embodiments of the invention below in conjunction with accompanying drawing.
An embodiment of present device comprises a deodorizing tank 5 as shown in Figure 1, 2, and deodorizing tank is set with heating and heat-insulating device 4 outward, and the lower bottom part of deodorizing tank is connected with storage tank 2 by star-like valve 3, and the bottom of storage tank connects vent pipe 1; The top, top of deodorizing tank 5 links by pipeline and capture tank 8, is installed on condenser in the capture tank, and capture tank 8 opposite sides are provided with vacuum pump interface 9 and are connected with vacuum pump.Be installed on the atomizing spray and rob 6 in deodorizing tank, described atomizing lance comprises vapour passage 14, grease channel 15 and is arranged on the nozzle 13 that the termination is robbed in the atomizing spray; Vapour passage is connected with steam-pipe 7, and grease channel is connected with oil pump pipeline 10, and the oil pump pipeline is connected with oil pump 12 via oil heater 11, and oil heater is used for the heating to polished fat, makes the grease temperature reach 200 ℃.
The present embodiment working process is: by vacuum pump with the deodorizing tank state that is evacuated, and deodorizing tank is heated to default temperature with the heating, temperature keeping device, after the vacuum tightness in the deodorizing tank and temperature reach processing requirement, vapour passage from atomizing lance feeds steam, and squeeze into the grease that needs deodorization by oil pump, in oil heater, grease is heated to predetermined temperature, grease is pressed onto the nozzle place, be ejected in the deodorizing tank with vapor mixing and atomize by grease channel; Fly in the grease of atomizing and the steam bottom to deodorizing tank under the effect of atomizing pressure, because vacuum and temperature action, volatile component in the grease is brought into the capture tank condensation by steam and is reclaimed, part volatile component and steam are extracted out by vacuum pump, and qualified grease can fall at the bottom of the deodorizing tank, flow into storage tank by star-like valve, and enter next step technology from vent pipe.
Another embodiment of present device as shown in Figure 3, it is a secondary deodorization equipment, it is to set up a cover deodorization equipment on the basis of a last embodiment again, comprise the secondary deodorizing tank 22 that has heating, temperature keeping device 18, install grease spray thrower 23 in the secondary deodorizing tank, the grease spray thrower links to each other with the grease vent pipe 1 of a deodorization, or the removal storage tank directly is connected by the star-like valve 3 of vent pipe 1 with a deodorizing tank bottom, the top, top of secondary deodorizing tank links by pipeline and capture tank 19, be installed on condenser in the capture tank, the capture tank opposite side is provided with vacuum pump interface 20 and is connected with vacuum pump, in the top duct ingress of secondary deodorizing tank outlet damper 21 can be set; Be installed on steam distributor 17 below in the secondary deodorizing tank, steam distributor is connected with steam-pipe 24, is connected with secondary deodorization vent pipe 16 by valve 25 at the jar end of secondary deodorizing tank, promptly constitutes the secondary deodorization equipment.
The embodiment of processing method of the present invention is as follows:
Embodiment 1
Present embodiment uses a deodour method: by vacuum pump with deodorizing tank and the total system state that is evacuated, vacuum tightness is 500Pa, and deodorizing tank is heated to 210 ℃ by the deodorizing tank heating jacket, after system vacuum degree and temperature reach requirement, vapour passage from the atomizing lance feeds the steam of 0.4MPa pressure, stable system vacuum tightness and temperature 5min, being squeezed into by oil pump needs the grease of deodorization 2T, by oil heater grease is heated to 210 ℃, by grease channel grease is pressed onto the nozzle place, grease pressure in the grease channel is 0.4MPa, is ejected in the deodorizing tank with vapor mixing to atomize; Produce to finish, get from storage tank and produce the grease of finishing and carry out weighing, results finished product grease is 1.984T, and it is as follows that the finished product grease is detected acid value, peroxide value, dissolvent residual, trans fatty acid and color and luster result:
Acid value (mg KOH/g) Peroxide value (meq/kg) Dissolvent residual (mg/Kg) Trans fatty acid (%) Color and luster, the Lovibond color and luster Yield
??0.2 ??0.03 ??≤1 ??≤0.3 ??Y10?R0.9 ??99.2%
Embodiment 2
Adopt one time deodour method: by vacuum pump with deodorizing tank and the total system state that is evacuated, vacuum tightness is 500Pa, and deodorizing tank is heated to 190 ℃ by the deodorizing tank heating jacket, after system vacuum degree and temperature reach requirement, vapour passage from the atomizing lance feeds the steam of 0.4MPa pressure, stable system vacuum tightness and temperature 5min, being squeezed into by oil pump needs the grease of deodorization 2T, by oil heater grease is heated to 190 ℃, by grease channel grease is pressed onto the nozzle place, grease pressure in the grease channel is 0.4MPa, is ejected in the deodorizing tank with vapor mixing to atomize; Produce to finish, get from storage tank and produce the grease of finishing and carry out weighing, results finished product grease is 1.99T, and it is as follows that the finished product grease is detected acid value, peroxide value, dissolvent residual, trans fatty acid and color and luster result:
Acid value (mg KOH/g) Peroxide value (meq/kg) Dissolvent residual (mg/Kg) Trans fatty acid (%) Color and luster, the Lovibond color and luster Yield
??0.2 ??0.20 ??≤1 ??≤0.3 ??Y11?R0.9 ??99.5%
Embodiment 3
This processing method is used the secondary deodorization: by vacuum pump with deodorizing tank and the total system state that is evacuated, vacuum tightness is 500Pa, and deodorizing tank is heated to 190 ℃ by the deodorizing tank heating jacket, after system vacuum degree and temperature reach requirement, vapour passage from the atomizing lance feeds the steam of 0.5MPa pressure, stable system vacuum tightness and temperature 5min, being squeezed into by oil pump needs the grease of deodorization 2T, by oil heater grease is heated to 190 ℃, by grease channel grease is pressed onto the nozzle place, grease pressure in the grease channel is 0.5MPa, is ejected in the deodorizing tank with vapor mixing to atomize; Grease after the deodorization flows into the secondary deodorizing tank, the secondary deodorizing tank is by the heating of deodorizing tank heating jacket and be stabilized in 150 ℃, and vacuum tightness is 500Pa, and the grease that enters the secondary deodorizing tank is under 150 ℃ condition, feeding pressure from secondary deodorizing tank bottom is the steam of 0.1MPa, deodorization 30min.Produce to finish, get from the secondary deodorizing tank and produce the grease of finishing and carry out weighing, results finished product grease is 1.98T, and acid value, peroxide value, dissolvent residual, trans fatty acid and color and luster result are as follows.
Acid value (mg KOH/g) Peroxide value (meq/kg) Dissolvent residual (mg/Kg) Trans fatty acid (%) Color and luster, the Lovibond color and luster Yield
??0.2 ??0.03 ??≤1 ??≤0.3 ??Y11?R0.9 ??99%

Claims (9)

1, a kind of grease deodorization method, it is characterized in that disposing deodorizing tank, deodorizing tank links to each other with vacuum pump and makes the deodorizing tank state that is evacuated, make by the heating, temperature keeping device that temperature remains on 200 ± 20 ℃ in the deodorizing tank, the atomizing spray is set in the deodorizing tank robs, the input terminus of atomizing lance joins with vapour passage and grease channel respectively, the pressurization of heating of the grease of in grease channel, treating deodorization processing, make the grease temperature reach 200 ± 20 ℃, by grease channel grease is pressed onto the nozzle place, is ejected in the deodorizing tank with vapor mixing and atomizes; Fly in the grease of atomizing and the steam bottom to deodorizing tank under the effect of atomizing pressure, because vacuum and temperature action, volatile component and steam in the grease are extracted out by vacuum pump, and qualified grease falls at the bottom of the deodorizing tank, flow into storage tank, and enter next step technology from vent pipe.
2, by the described grease deodorization method of claim 1, it is characterized in that the volatile component part in the described grease is brought into capture tank condensation recovery by steam, part volatile component and steam are extracted out by vacuum pump.
3, by claim 1 or 2 described grease deodorization methods, it is characterized in that the vacuum tightness of described deodorizing tank vacuum state is equal to or less than 1KPa.
4, by claim 1 or 2 described grease deodorization methods, the pressure that it is characterized in that steam in the described vapour passage is 0.2~0.5MPa; Grease pressure in the described grease channel is 0.2~0.5MPa.
5, by claim 1 or 2 described grease deodorization methods, it is characterized in that the grease of deodorization enters next deodorization procedures, carry out the secondary deodorization, temperature and grease temperature are 150 ± 10 ℃ in the deodorizing tank of deodorization for the second time, the vacuum tightness of deodorizing tank vacuum state is equal to or less than 500Pa, and the pressure of steam is 0.1~0.2MPa.
6, a kind of grease deodorization equipment, comprise deodorizing tank, storage tank and vacuum pump, it is characterized in that: described deodorizing tank top is connected with vacuum pump by pipeline, the below of deodorizing tank communicates with storage tank, outside deodorizing tank, be installed on the heating, temperature keeping device, be installed on the atomizing spray in the deodorizing tank and rob, the input terminus that the atomizing spray is robbed connects steam-pipe and oil pump pipeline respectively, and is connected in series oil heater in the oil pump pipeline.
7,, it is characterized in that the capture tank of connecting band condenser in deodorizing tank and pipeline that vacuum pump links to each other by the described grease deodorization equipment of claim 6.
8,, it is characterized in that described atomizing lance comprises vapour passage, grease channel and is arranged on the nozzle that the termination is robbed in the atomizing spray by claim 6 or 7 described grease deodorization equipment; Vapour passage is connected with described steam-pipe, and grease channel is connected with described oil pump pipeline.
9, by claim 6 or 7 described grease deodorization equipment, it is characterized in that setting up again a cover deodorization equipment, comprise the secondary deodorizing tank that has the heating, temperature keeping device, install the grease spray thrower in the secondary deodorizing tank, the grease spray thrower links to each other with the grease vent pipe of a deodorization, or the removal storage tank directly is connected with a deodorizing tank bottom by vent pipe, the top, top of secondary deodorizing tank links by pipeline and capture tank, be installed on condenser in the capture tank, the capture tank opposite side is provided with the vacuum pump interface and is connected with vacuum pump, be installed on steam distributor below in the secondary deodorizing tank, steam distributor is connected with steam-pipe, the jar end at the secondary deodorizing tank is connected with secondary deodorization vent pipe by valve, promptly constitutes the secondary deodorization equipment.
CN2009100636590A 2009-08-19 2009-08-19 Method and equipment for grease deodorization Active CN101659902B (en)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101942358A (en) * 2010-09-03 2011-01-12 北京中农康元粮油技术发展有限公司 Freeze-condensing vacuum deodorizing method and equipment for fat and oil
CN101993779A (en) * 2010-11-12 2011-03-30 东北农业大学 Method for reducing trans fatty acid content in vegetable oil grease by two-stage type deodorization tower
CN102311874A (en) * 2011-08-17 2012-01-11 郑州远洋油脂工程技术有限公司 Technology of stripping-deodorizing during grease deodorization process, vacuum heat recovery heat exchanger used for process and equipment thereof
CN102770519A (en) * 2010-03-17 2012-11-07 花王株式会社 Production process for refined fats and oils
CN102782108A (en) * 2010-03-17 2012-11-14 花王株式会社 Method for producing refined oils and fats
CN103409236A (en) * 2013-09-03 2013-11-27 河南粮工科技有限公司 Combined type deacidification and deodorization tower suitable for deodorizing edible oil in oil industry
CN104629912A (en) * 2013-11-07 2015-05-20 日清奥利友集团株式会社 Preparation method of refined oil, method for reducing acetaldehyde amount in oil, method for reducing oil being smelly under exposure, and method for improving cold resistance of soybean oil
CN105296149A (en) * 2015-12-14 2016-02-03 广汉市迈德乐食品有限公司 Beef tallow decolorization system and grease continuous decolorization method
CN104277910B (en) * 2014-09-25 2016-09-07 江阴天田真空设备制造有限公司 Vaporising device for grease condensing, freezing deodorization
CN106433971A (en) * 2016-11-23 2017-02-22 天津炫盛科技开发有限公司 Pressure spray emu oil separator
CN108018120A (en) * 2016-11-02 2018-05-11 天津瑞海潮科技有限公司 A kind of deodorization equipment with return line
CN111234921A (en) * 2020-01-21 2020-06-05 山东西王食品有限公司 Oil refining process rich in natural antioxidant
CN112646658A (en) * 2020-12-23 2021-04-13 四川航佳生物科技有限公司 Beef tallow deslagging and drying system and production process

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102770519B (en) * 2010-03-17 2014-10-08 花王株式会社 Production process for refined fats and oils
US9006474B2 (en) 2010-03-17 2015-04-14 Kao Corporation Method for producing refined a fat or oil
CN102770519A (en) * 2010-03-17 2012-11-07 花王株式会社 Production process for refined fats and oils
CN102782108A (en) * 2010-03-17 2012-11-14 花王株式会社 Method for producing refined oils and fats
US8846963B2 (en) 2010-03-17 2014-09-30 Kao Corporation Production process for refined fat or oil
CN102782108B (en) * 2010-03-17 2015-03-18 花王株式会社 Method for producing refined oils and fats
CN101942358A (en) * 2010-09-03 2011-01-12 北京中农康元粮油技术发展有限公司 Freeze-condensing vacuum deodorizing method and equipment for fat and oil
CN101993779B (en) * 2010-11-12 2013-09-11 东北农业大学 Method for reducing trans fatty acid content in vegetable oil grease by two-stage type deodorization tower
CN101993779A (en) * 2010-11-12 2011-03-30 东北农业大学 Method for reducing trans fatty acid content in vegetable oil grease by two-stage type deodorization tower
CN102311874A (en) * 2011-08-17 2012-01-11 郑州远洋油脂工程技术有限公司 Technology of stripping-deodorizing during grease deodorization process, vacuum heat recovery heat exchanger used for process and equipment thereof
CN103409236A (en) * 2013-09-03 2013-11-27 河南粮工科技有限公司 Combined type deacidification and deodorization tower suitable for deodorizing edible oil in oil industry
CN104629912B (en) * 2013-11-07 2023-11-03 日清奥利友集团株式会社 Method for producing refined oil, method for reducing acetaldehyde content in oil, method for reducing exposure odor of oil, and method for improving cold resistance of soybean oil
CN104629912A (en) * 2013-11-07 2015-05-20 日清奥利友集团株式会社 Preparation method of refined oil, method for reducing acetaldehyde amount in oil, method for reducing oil being smelly under exposure, and method for improving cold resistance of soybean oil
CN104277910B (en) * 2014-09-25 2016-09-07 江阴天田真空设备制造有限公司 Vaporising device for grease condensing, freezing deodorization
CN105296149A (en) * 2015-12-14 2016-02-03 广汉市迈德乐食品有限公司 Beef tallow decolorization system and grease continuous decolorization method
CN108018120A (en) * 2016-11-02 2018-05-11 天津瑞海潮科技有限公司 A kind of deodorization equipment with return line
CN106433971A (en) * 2016-11-23 2017-02-22 天津炫盛科技开发有限公司 Pressure spray emu oil separator
CN111234921A (en) * 2020-01-21 2020-06-05 山东西王食品有限公司 Oil refining process rich in natural antioxidant
CN112646658A (en) * 2020-12-23 2021-04-13 四川航佳生物科技有限公司 Beef tallow deslagging and drying system and production process

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Patentee after: Limited by Share Ltd Biotechnology (Wuhan) Co., Ltd.

Address before: 430073 Hubei city of Wuhan province Wuchang Guanshan road two No. 1 International Business Center Building 5 floor A block Juxian

Patentee before: Chia lung Biological Engineering (Wuhan) Co., Ltd.