CN202744527U - Solid-state distillation circular extraction device - Google Patents
Solid-state distillation circular extraction device Download PDFInfo
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- CN202744527U CN202744527U CN2012204477779U CN201220447777U CN202744527U CN 202744527 U CN202744527 U CN 202744527U CN 2012204477779 U CN2012204477779 U CN 2012204477779U CN 201220447777 U CN201220447777 U CN 201220447777U CN 202744527 U CN202744527 U CN 202744527U
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Abstract
The utility model discloses a solid-state distillation circular extraction device which is favorable for improving the aroma component extraction efficiency in the distillation process of distilled grains. The device comprises a distilling barrel and a bottom pot arranged at the bottom of the distilling barrel; the top of the distilling barrel is connected with a cooler through a wine steam pipe; a wine steam pipe control valve is arranged on the wine steam pipe; the bottom pot is connected with a steam input pipe; a steam input pipe control valve is arranged on the steam input pipe; and the device also comprises a circulating device for extracting steam out of the distilling barrel and feeding the steam into the bottom pot. The circulating device comprises a circulating air inlet pipe connected with the wine steam pipe and arranged between the wine steam pipe control valve and the distilling barrel; the circulating air inlet pipe is provided with a circulating air inlet pipe control valve; the circulating device also comprises a circulating air outlet pipe connected with the steam input pipe and arranged between the steam input pipe control valve and the bottom pot; a circulating air outlet pipe control valve is arranged on the circulating air outlet pipe; and a circulating air pump is connected between the circulating air inlet pipe and the circulating air outlet pipe.
Description
Technical field
The utility model relates to the solid state distillation circulation extracting apparatus that use in a kind of Brewing equipment field.
Background technology
Solid state distillation is the important way that liquor is produced.In liquor solid state distillation process, the solid-state poor unstrained spirits that ferments is filled in the rice steamer bucket equably, water vapor occurs in the end of rice steamer bottom of the barrel pot, from bottom to top go here and there steaming, from poor unstrained spirits, extract alcohol component and flavour ingredient, form at last wine steam, and be delivered to water cooler and be condensed into wine liquid.Water vapor penetrating in the process from bottom to top, alcohol component and flavour ingredient in the grain unstrained spirits progress in the water vapor, and from bottom to top be concentrated gradually, concentrated being conducive to of alcohol component extracts flavour ingredient in the poor unstrained spirits, because most of flavour ingredient belongs to the compositions such as the ester class, acids, alcohols of pure dissolubility, also therefore flavour ingredient is from bottom to top constantly concentrated, and extraction effect is better, and concentrated alcohol component and flavour ingredient together are output and are cooled to wine liquid at last.
Yet, in liquor solid state distillation process, because solid-state poor unstrained spirits self structure heterogeneity and the filling of poor unstrained spirits are difficult to fully uniformly problem, alcohol component and flavour ingredient extraction and incomplete in the poor unstrained spirits in the rice steamer bucket, also residual in the poor unstrained spirits after the extraction have part alcohol component and a flavour ingredient, and the alcohol concentration of component is not high after the poor unstrained spirits of rice steamer bottom of the barrel penetrates owing to water vapor, more flavour ingredient does not extract in it, thereby cause poor unstrained spirits extraction efficiency not high, " high yield is not had a good harvest ", and the serious waste that causes resource.
Therefore, improving in the poor unstrained spirits still-process alcohol concentration of component in the steam, is the important factor that improves flavour ingredient extraction efficiency in the poor unstrained spirits.
The utility model content
The technical problem that the utility model solves provides a kind of solid state distillation circulation extracting apparatus that is conducive to improve flavour ingredient extraction efficiency in the poor unstrained spirits still-process.
The technical scheme that its technical problem that solves the utility model adopts is: the solid state distillation circulation extracting apparatus, the end pot that comprises the rice steamer bucket and be arranged on the rice steamer bottom of the barrel, rice steamer bucket top links to each other with water cooler by the wine vapour pipe, be provided with wine vapour pipe control valve on the wine vapour pipe, be connected with steam input pipe on the end pot, be provided with the steam input pipe control valve on the steam input pipe, also comprise for the circulation device of in the rice steamer bucket, steam being extracted out and sending in the end pot.
Further be: described circulation device comprises the circulation inlet pipe between wine vapour pipe control valve and the rice steamer bucket of being arranged on that links to each other with the wine vapour pipe, be provided with circulation inlet pipe control valve on the circulation inlet pipe, circulation device also comprises the tracheae that recycles between steam input pipe control valve and the end pot of being arranged on that links to each other with steam input pipe, recycle to be provided with on the tracheae and recycle the tracheae control valve, circulation inlet pipe and recycle and be connected with the circulation air pump between the tracheae.
The beneficial effects of the utility model are: steam at rice steamer bucket internal recycle string with the steam that contains the alcohol in high concentration component that extracts, the extraction efficiency of alcohol component and flavour ingredient in the Effective Raise grain unstrained spirits, especially improve the extraction efficiency of flavour ingredient in the poor unstrained spirits, increased the flavour ingredient content in the wine.
Description of drawings
Fig. 1 is the schematic diagram of solid state distillation circulation extracting apparatus of the present utility model;
Be labeled as among the figure: rice steamer bucket 1, end pot 2, wine vapour pipe control valve 3, circulation inlet pipe 4, circulation air pump 5 recycles tracheae 6, steam input pipe 7, wine vapour pipe 8, water cooler 9, circulation inlet pipe control valve 10 recycles tracheae control valve 11, steam input pipe control valve 12.
Embodiment
Below in conjunction with the drawings and specific embodiments the utility model is further specified.
As shown in Figure 1, solid state distillation circulation extracting apparatus of the present utility model, the end pot 2 that comprises rice steamer bucket 1 and be arranged on the rice steamer bottom of the barrel, rice steamer bucket top links to each other with water cooler 9 by wine vapour pipe 8, be provided with wine vapour pipe control valve 3 on the wine vapour pipe 8, be connected with steam input pipe 7 on the end pot 2, be provided with steam input pipe control valve 12 on the steam input pipe 7, also comprise for from the interior circulation device of steam being extracted out and being sent in the end pot 2 of rice steamer bucket 1.During use, can be with the steam in the rice steamer bucket 1 constantly at rice steamer bucket 1 internal recycle by circulation device, along with improving constantly of ethanol content in the steam, the flavour ingredient in the poor unstrained spirits is effectively extracted.
The embodiment of above-mentioned circulation device has multiple, for example can a return line be installed at the rice steamer bucket, and return line links to each other with end pot, and an off-gas pump is installed on the flow tube.So just the steam in the rice steamer bucket can be regained end pot again, then again poor unstrained spirits be distilled.But said structure need to be transformed rice steamer bucket and end pot, and cost is higher, is not easy to arrange.In order to overcome above-mentioned deficiency, preferred implementation is: as shown in Figure 1, described circulation device comprises the circulation inlet pipe 4 between wine vapour pipe control valve 3 and the rice steamer bucket 1 of being arranged on that links to each other with wine vapour pipe 8, be provided with circulation inlet pipe control valve 10 on the circulation inlet pipe 4, circulation device comprises that also being arranged on of linking to each other with steam input pipe 7 recycles tracheae 6 between steam input pipe control valve 12 and the end pot 2, recycle to be provided with on the tracheae 6 and recycle tracheae control valve 11, circulation inlet pipe 4 and recycle and be connected with circulation air pump 5 between the tracheae 6.
In the liquor solid still-process, insert in rice steamer bucket 1 process at the solid-state poor unstrained spirits that will ferment, open simultaneously steam input pipe control valve 12 and wine vapour pipe control valve 3, in end pot 2, be filled with water vapor, water vapor from bottom to top penetrates to rice steamer bucket 1 interior poor unstrained spirits, constantly extract during this time alcohol component and aroma constituent in the poor unstrained spirits, and during to the upper part grain unstrained spirits of rice steamer bucket 1 in the water vapor alcohol component obtained constantly concentratedly, had higher concentration.And the alcohol component that the flavour ingredient in the poor unstrained spirits also constantly concentrates extracts, the common wine steam that contains higher concentration alcohol that forms of alcohol component and flavour ingredient and water vapor.When treating that wine steam is emerged in a large number from rice steamer bucket 1 is interior, steam off input tube control valve 12 and wine vapour pipe control valve 3, and open circulation inlet pipe control valve 10 and recycle tracheae control valve 11, circulation air pump 5 started simultaneously, rice steamer bucket 1 interior wine steam is extracted out, and be directed in the end pot 2.The wine steam that contains higher ethanol concn from bottom to top extracts alcohol component and flavour ingredient residual in the poor unstrained spirits again, again being recycled air pump 5 to rice steamer bucket 1 top transfers in the end pot 2, so circulation is extracted, and residual flavour ingredient in the poor unstrained spirits is fully extracted.Behind the certain hour to be recycled, such as 20min, close circulation inlet pipe control valve 10 and recycle tracheae control valve 11, open steam input pipe control valve 12 and wine vapour pipe control valve 3, out steam from bottom to top has extraction the wine steam of a large amount of alcohol components and flavour ingredient to release to end pot 2 from steam input pipe 7, be delivered to water cooler 9 by wine vapour pipe 8 at last, be condensed into liquid wine liquid, finish the extraction to alcohol and flavour ingredient in the poor unstrained spirits.
Embodiment
Experimental program 1: adopt this use New Solid distillation circulation extracting apparatus, operate according to the method described above, circulation extraction time is 20min, at last extraction is had the wine steam of a large amount of alcohol components and flavour ingredient to release, and be delivered to water cooler, be cooled to liquid wine liquid.
Experimental program 2: distill by prior art, adopt rice steamer bucket and the end pot of same capability, take the identical poor unstrained spirits that ferments of same Jiao Chi as extracting object, poor unstrained spirits is inserted in the rice steamer bucket equably, open simultaneously steam input pipe control valve 12, steam from bottom to top extracts alcohol component and the flavour ingredient in the poor unstrained spirits, when treating that steam is collected in rice steamer bucket top, directly be delivered in the water cooler, be cooled to liquid wine liquid.
Calculate the output of above-mentioned experimental program 1 and experimental program 2 obtained wine therebies, and with conventional gas chromatographic analysis flavour ingredient in the wine is detected.The result is as follows:
The output situation of table 1 wine
| Produce wine weight and (amount to into the weight of 60 degree alcohol, Kg) | |
| Experimental program 1 | 63.55 |
| Experimental program 2 | 55.37 |
Flavour ingredient content unit: g/L in table 2 wine
| Ethyl hexanoate | Ethyl acetate | Ethyl lactate | Ethyl butyrate | Acetic acid | Caproic acid | Butyric acid | |
| Experimental program 1 | 2.54 | 1.35 | 1.32 | 0.36 | 0.39 | 0.28 | 0.16 |
| Experimental program 2 | 1.87 | 1.01 | 1.11 | 0.16 | 0.27 | 0.19 | 0.09 |
As can be seen from Table 1, the weight of obtained wine thereby is 63.55Kg in the experimental program 1, and is higher by 14.78% than experimental program 2, and the circulation extracting method is adopted in explanation thus, is conducive to alcohol component remaining in the poor unstrained spirits is extracted, and avoids the waste of alcohol component.
As can be seen from Table 2, flavour ingredient is significantly higher than experimental program 2 in the experimental program 1, wherein the main body composition ethyl hexanoate in the wine body and ethyl acetate are respectively 1.36 and 1.34 times of experimental program 2, the circulation extracting process in the experimental program 1 is adopted in explanation thus, by the concentrated wine steam that the alcohol component is arranged, be conducive to improve the extraction efficiency of flavour ingredient in the poor unstrained spirits, improve flavour ingredient content in the wine body.
Claims (2)
1. solid state distillation circulation extracting apparatus, the end pot (2) that comprises rice steamer bucket (1) and be arranged on the rice steamer bottom of the barrel, rice steamer bucket top links to each other with water cooler (9) by wine vapour pipe (8), be provided with wine vapour pipe control valve (3) on the wine vapour pipe (8), be connected with steam input pipe (7) on the end pot (2), be provided with steam input pipe control valve (12) on the steam input pipe (7), it is characterized in that: also comprise for the circulation device of steam being extracted out and sending in the rice steamer bucket (1) in the end pot (2).
2. solid state distillation circulation extracting apparatus as claimed in claim 1, it is characterized in that: described circulation device comprises the circulation inlet pipe (4) between wine vapour pipe control valve (3) and the rice steamer bucket (1) of being arranged on that links to each other with wine vapour pipe (8), be provided with circulation inlet pipe control valve (10) on the circulation inlet pipe (4), circulation device comprises that also being arranged on of linking to each other with steam input pipe (7) recycles tracheae (6) between steam input pipe control valve (12) and the end pot (2), recycle to be provided with on the tracheae (6) and recycle tracheae control valve (11), circulation inlet pipe (4) and recycle and be connected with circulation air pump (5) between the tracheae (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012204477779U CN202744527U (en) | 2012-09-04 | 2012-09-04 | Solid-state distillation circular extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012204477779U CN202744527U (en) | 2012-09-04 | 2012-09-04 | Solid-state distillation circular extraction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202744527U true CN202744527U (en) | 2013-02-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2012204477779U Expired - Lifetime CN202744527U (en) | 2012-09-04 | 2012-09-04 | Solid-state distillation circular extraction device |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104195023A (en) * | 2014-09-09 | 2014-12-10 | 孙祯芳 | Combined type solid-state distillation device |
| CN107937229A (en) * | 2018-01-15 | 2018-04-20 | 沈墅 | A kind of high-purity white wine deep layer extracting system |
| CN108060049A (en) * | 2018-01-15 | 2018-05-22 | 沈墅 | A kind of circulating alcoholic extract system |
-
2012
- 2012-09-04 CN CN2012204477779U patent/CN202744527U/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104195023A (en) * | 2014-09-09 | 2014-12-10 | 孙祯芳 | Combined type solid-state distillation device |
| CN104195023B (en) * | 2014-09-09 | 2015-12-16 | 孙祯芳 | Combined type solid-state water distilling apparatus |
| CN107937229A (en) * | 2018-01-15 | 2018-04-20 | 沈墅 | A kind of high-purity white wine deep layer extracting system |
| CN108060049A (en) * | 2018-01-15 | 2018-05-22 | 沈墅 | A kind of circulating alcoholic extract system |
| CN108060049B (en) * | 2018-01-15 | 2021-01-26 | 上海帝浆生物科技有限公司 | Circulating alcohol extraction system |
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130220 |