CN101643680B - Lubricating preparation for micro enamelled wire below 0.10mm - Google Patents
Lubricating preparation for micro enamelled wire below 0.10mm Download PDFInfo
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- CN101643680B CN101643680B CN 200910157511 CN200910157511A CN101643680B CN 101643680 B CN101643680 B CN 101643680B CN 200910157511 CN200910157511 CN 200910157511 CN 200910157511 A CN200910157511 A CN 200910157511A CN 101643680 B CN101643680 B CN 101643680B
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- enamelled wire
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Abstract
The invention relates to a lubricating preparation for a micro enamelled wire below 0.10mm, consisting of the following materials by weight percentage: 70-80% of 200# solvent naphtha, 15-20% of n-hexane, 3-5% of 7# white mineral oil, and 1-2% of 46# refrigerator oil and the invention comprises the following steps: weighing the materials above according to the weight percentage, adding the materials into an insulated stirred reaction kettle having a steam jacket to increase the temperature to 40+/-5 DEG C by steam followed by stirring the materials at the temperature for 0.5h until the light yellow and transparent liquid is generated. The lubricating preparation for the micro enamelled wire below 0.10mm has the following beneficial effects: 1) no occurence of material separating out and adhering on the jewel needle hole of a winding machine to prevent the hole from being blocked, thus improving the production efficiency of customers; 2) no residual educt and transferred material on the enamelled wire after the enamelled wire is wound into a coil (relay) so that the service life of the coil is prolonged; and 3) low volatility with the gas volatility completely complying with the standard requirement of 'Lowgas enamelled wire' produced by the surface lubricating preparation.
Description
Technical field
The present invention relates to the lubricant formulations on the following fine enameled wire of a kind of 0.10mm of being used for.
Background technology
Enameled wire need to use surface lubricant in process of production, makes it when the production take-up, can be neat closely be arranged on the bobbin; But use the market at present, is main raw with solid-state and semi-solid paraffin mostly; The client wants in the use, is prone to following problem: 1), when coiling, solid-state and semi-solid paraffin, very easily separate out and the jewel pin hole attached to winding machine on, went up the jewel pin hole of line when stopping up coiling; Particularly very easily cause the phenomenon that occurs breaking during the coiling fine enameled wire; Need regularly be folded down cleaning, have a strong impact on production efficiency; 2), turn to coil after, it remains in the solid-state and semi-solid paraffin on enameled wire surface; When coil (particularly rly./micromotor) energising work, can separate out because of reason for heat, and shift on the contact attached to coil (rly./micromotor), increase the contact contact resistance, not even conducting; Cause coil (rly./micromotor) can not normal power-up to lose efficacy, thereby make coil (rly./micromotor) cisco unity malfunction and scrap; 3), at present, some high-end customers have proposed enameled wire after turning to coil, and the gaseous volatilization amount in its coil must be extremely low; " the Lowgas enameled wire " of said low volatilization gas just; The enamelled wire surface lubricant that uses on the market at present mostly can not satisfy this requirement.
Summary of the invention
The purpose of this invention is to provide the lubricant formulations preparation technology on the following fine enameled wire of a kind of 0.1mm of being used for; Use this enamelled wire surface lubricant; Can guarantee that enameled wire is in production take-up process; The needs of tight marshalling, can reach real raw material does not again have wax, the purpose of low gaseous volatilization.
Lubricant formulations on the following fine enameled wire of the 0.1mm of being used for of the present invention is processed by following raw materials by weight percent: 200# solvent oil 70-80%, normal hexane 15-20%, 7# white mineral oil 3-5%, 46# refrigerator oil 1-2%.
Preferably, the lubricant formulations on the following fine enameled wire of the 0.1mm of being used for of the present invention is processed by following raw materials by weight percent: 200# solvent oil 75%, normal hexane 20%, 7# white mineral oil 4%, 46# refrigerator oil 1%.
Preferably, the lubricant formulations on the following fine enameled wire of the said 0.1mm of being used for is processed by following raw materials by weight percent: 200# solvent oil 80%, normal hexane 15%, 7# white mineral oil 3%, 46# refrigerator oil 2%.
Lubricant formulations preparation technology on the following fine enameled wire of the 0.1mm of being used for according to the invention comprises following content:
Take by weighing each material in the above-mentioned prescription by weight ratio, add in the stirred autoclave of band vapour jacket insulation, be warming up to 40 ℃ ± 5 ℃ with steam after, under this temperature, stirred 0.5 hour, be faint yellow, transparent liquid until being generated as.
Beneficial effect of the present invention is: 1) the present invention is not owing to use the material of any solid-state or semi-solid paraffin; Can not occur that material is separated out and attached to the phenomenon of stopping up pin hole on the jewel pin hole of winding machine, thereby improve client's production efficiency; From before per tour stop line 1 hour and once clean, change into and need not stop line, enhance productivity more than 14%, improved production efficiency greatly.2) turn to coil after, the precipitate and the transfer of material of the noresidue of enameled wire surface; At coil (particularly rly.), can not shift on the contact attached to coil (rly.), and the phenomenon that causes coil (rly.) can not switch on and lose efficacy and scrap, thereby the work-ing life of extension coil (rly.); Be increased to 12-15 ten thousand times 100,000 times from average work-ing life.3) volatility is low, and with the enameled wire that this surface lubricant is produced, the gaseous volatilization amount meets " Lowgas enameled wire " standard-required fully, and the production technology of having filled up domestic like product Application Areas is blank.
Embodiment
Embodiment 1:
Lubricant formulations on the following fine enameled wire of the described 0.1mm of being used for of the embodiment of the invention is processed by following raw material:
200# solvent oil 75 grams, normal hexane 20 grams, 7# white mineral oil 4 grams, 46# refrigerator oil 1 gram.The preparation technology of the lubricant formulations on the following fine enameled wire of the 0.1mm of being used for of the present invention comprises following content:
Take by weighing each material in the above-mentioned prescription by weight ratio, add in the stirred autoclave of band vapour jacket insulation, be warming up to 35 ℃ with steam after, under this temperature, stirred 0.5 hour, be faint yellow, transparent liquid until being generated as.
Embodiment 2:
Lubricant formulations on the following fine enameled wire of the described 0.1mm of being used for of the embodiment of the invention is processed by following raw material:
200# solvent oil 80 grams, normal hexane 15 grams, 7# white mineral oil 3 grams, 46# refrigerator oil 2 grams.
The preparation technology of the lubricant formulations on the following fine enameled wire of the described 0.1mm of being used for of present embodiment comprises following content:
Take by weighing each material in the above-mentioned prescription by weight ratio, add in the stirred autoclave of band vapour jacket insulation, be warming up to 45 ℃ with steam after, under this temperature, stirred 0.5 hour, be faint yellow, transparent liquid until being generated as.
Embodiment 3:
Lubricant formulations on the following fine enameled wire of the described 0.1mm of being used for of the embodiment of the invention is processed by following raw material:
200# solvent oil 76 grams, normal hexane 20 grams, 7# white mineral oil 3 grams, 46# refrigerator oil 1 gram.
The preparation technology of the lubricant formulations on the following fine enameled wire of the described 0.1mm of being used for of present embodiment comprises following content:
Take by weighing each material in the above-mentioned prescription by weight ratio, add in the stirred autoclave of band vapour jacket insulation, be warming up to 45 ℃ with steam after, under this temperature, stirred 0.5 hour, be faint yellow, transparent liquid until being generated as.
Below be the data of measuring the residual quantity of unwanted volatile in the enameled wire with GC with Headspace-MS method:
GC with Headspace-MS method is measured volatile matter in the enameled wire: be applicable to the quantitative analysis of residual minim volatile matter in the various enameled wires; Method detects and is limited to 10-8 (ω); Linearity range is 2.5 * 10-8～5 * 10-6 (ω), and the mark-on average recovery rate surpasses 95%.
Testing method: headspace injection method, 150 ℃ of temperature, time 45min.
| Sequence number | The volatile matter title | Content (mg/Kg) |
| 1 | Toluene | ND |
| 2 | Ethylbenzene | ND |
| 3 | P-Xylol | ND |
| 4 | M-xylene | ND |
| 5 | O-Xylol | ND |
| 6 | Vinylbenzene | ND |
| 7 | Ortho Cresol | ND |
| 8 | Phenol | 0.13 |
| 9 | 2, the 5-xylenol | ND |
| 10 | P-cresol | 0.05 |
| 11 | M-cresol | 0.04 |
| 12 | 3, the 5-xylenol | 0.03 |
The lubricant formulations preparation technology who is used on the following fine enameled wire of 0.1mm of the present invention is not owing to use the material of any solid-state or semi-solid paraffin; Can not occur that material is separated out and attached to the phenomenon of stopping up pin hole on the jewel pin hole of winding machine, thereby improve client's production efficiency; From before per tour stop line 1 hour and once clean, change into and need not stop line, enhance productivity more than 14%, enhance productivity greatly.After turning to coil, in the precipitate and the transfer of material of enameled wire surface noresidue; At coil (particularly rly.), can not shift on the contact attached to coil (rly.), avoided owing to cause coil (rly.) not switch on losing efficacy scrapping the generation of phenomenon, thus the work-ing life of extension coil (rly.); Be increased to 12-15 ten thousand times 100,000 times from average work-ing life; Volatility is low, and with the enameled wire that this surface lubricant is produced, the gaseous volatilization amount meets " Lowgas enameled wire " standard-required fully, and the production technology of having filled up domestic like product Application Areas is blank.
| 13 | 3, the 4-xylenol | ND |
| 14 | P-ethyl phenol | ND |
| 15 | 2, the 3-xylenol | ND |
| 16 | 2, the 6-xylenol | ND |
| 17 | Phlorol | ND |
| 18 | The catenanes compound | ND |
Claims (3)
1. a lubricant formulations that is used on the following fine enameled wire of 0.1mm is characterized in that: processed by following raw materials by weight percent: 200# solvent oil 70-80%, normal hexane 15-20%, 7# white mineral oil 3-5%, 46# refrigerator oil 1-2%.
2. the lubricant formulations that is used on the following fine enameled wire of 0.1mm according to claim 1 is characterized in that preparation technology may further comprise the steps:
Take by weighing each material in the said prescription of an amount of claim 1 by weight ratio, in the stirred autoclave of adding band vapour jacket insulation, with steam intensification back, stirring, until generating faint yellow, transparent liquid.
3. the lubricant formulations that is used on the following fine enameled wire of 0.1mm according to claim 2 is characterized in that: be warming up to 40 ℃ ± 5 ℃ with steam, and under this temperature, stirred 0.5 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910157511 CN101643680B (en) | 2009-07-10 | 2009-07-10 | Lubricating preparation for micro enamelled wire below 0.10mm |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910157511 CN101643680B (en) | 2009-07-10 | 2009-07-10 | Lubricating preparation for micro enamelled wire below 0.10mm |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101643680A CN101643680A (en) | 2010-02-10 |
| CN101643680B true CN101643680B (en) | 2012-12-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200910157511 Active CN101643680B (en) | 2009-07-10 | 2009-07-10 | Lubricating preparation for micro enamelled wire below 0.10mm |
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| Country | Link |
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| CN (1) | CN101643680B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102181318B (en) * | 2011-03-28 | 2013-06-05 | 天津市鑫龙田线材厂 | Lacquered wire lubricating oil |
| CN103996466A (en) * | 2014-06-05 | 2014-08-20 | 珠海市一致电工有限公司 | Enamel covering method of fine enamel covered wires |
| CN105567395A (en) * | 2015-12-30 | 2016-05-11 | 先登控股集团股份有限公司 | Enameled wire surface treatment agent and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6166466A (en) * | 1995-06-28 | 2000-12-26 | Nisshinbo Industries, Inc. | Insulating material for enameled wire of motor of refrigeration compressor |
| CN1760351A (en) * | 2005-10-31 | 2006-04-19 | 余卓新 | Anticorrosive emulsified oil in use for drawing ultramicro-fine brass wires, and manufacturing method |
| CN201038004Y (en) * | 2007-01-11 | 2008-03-19 | 戚建萍 | Environment-friendly refrigerant composite enameled wire |
-
2009
- 2009-07-10 CN CN 200910157511 patent/CN101643680B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6166466A (en) * | 1995-06-28 | 2000-12-26 | Nisshinbo Industries, Inc. | Insulating material for enameled wire of motor of refrigeration compressor |
| CN1760351A (en) * | 2005-10-31 | 2006-04-19 | 余卓新 | Anticorrosive emulsified oil in use for drawing ultramicro-fine brass wires, and manufacturing method |
| CN201038004Y (en) * | 2007-01-11 | 2008-03-19 | 戚建萍 | Environment-friendly refrigerant composite enameled wire |
Non-Patent Citations (1)
| Title |
|---|
| 郑启荣.漆包线的表面润滑.《电线电缆》.1992,(第6期),14-16. * |
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| CN101643680A (en) | 2010-02-10 |
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Owner name: GUANGDONG RONGSHENG SUPERMICRO-WIRE CO., LTD. Free format text: FORMER OWNER: ZHEJIANG JIAXING RONSEN FINE WIRE CO., LTD. Effective date: 20120628 |
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Free format text: CORRECT: ADDRESS; FROM: 314003 JIAXING, ZHEJIANG PROVINCE TO: 519040 ZHUHAI, GUANGDONG PROVINCE |
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Effective date of registration: 20120628 Address after: 519040 Guangdong province Zhuhai City Sanzao town Jinwan District Sanzao Science and Technology Industrial Park Applicant after: Guangdong Rongsheng Supermicro-Wire Co., Ltd. Address before: 314003 No. 638, Tong Tong Road, Jiaxing economic and Technological Development Zone, Zhejiang, China Applicant before: Zhejiang Jiaxing Ronsen Fine wire Co., Ltd. |
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Effective date of registration: 20160805 Address after: Jinwan District Sanzao Town Airport West 519040 in Guangdong province Zhuhai City 681 Building No. 4 101 Patentee after: Zhuhai Rong Yu superfine wire Co., Ltd. Address before: 519040 Guangdong province Zhuhai City Sanzao town Jinwan District Sanzao Science and Technology Industrial Park Patentee before: Guangdong Rongsheng Supermicro-Wire Co., Ltd. |