CN101627773A - Wound protective agent for preventing apple tree canker - Google Patents
Wound protective agent for preventing apple tree canker Download PDFInfo
- Publication number
- CN101627773A CN101627773A CN200910166049A CN200910166049A CN101627773A CN 101627773 A CN101627773 A CN 101627773A CN 200910166049 A CN200910166049 A CN 200910166049A CN 200910166049 A CN200910166049 A CN 200910166049A CN 101627773 A CN101627773 A CN 101627773A
- Authority
- CN
- China
- Prior art keywords
- protective agent
- wound
- wound protective
- canker
- valsa canker
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000003223 protective agent Substances 0.000 title claims abstract description 21
- 235000011430 Malus pumila Nutrition 0.000 title abstract description 26
- 235000015103 Malus silvestris Nutrition 0.000 title abstract description 26
- 244000141359 Malus pumila Species 0.000 title abstract description 6
- 240000000233 Melia azedarach Species 0.000 claims abstract description 7
- 239000010231 banlangen Substances 0.000 claims abstract description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 6
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 6
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 6
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 5
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 5
- 230000000694 effects Effects 0.000 claims abstract description 4
- 241000196324 Embryophyta Species 0.000 claims abstract description 3
- 102000018997 Growth Hormone Human genes 0.000 claims abstract description 3
- 108010051696 Growth Hormone Proteins 0.000 claims abstract description 3
- 239000000122 growth hormone Substances 0.000 claims abstract description 3
- 229920001213 Polysorbate 20 Polymers 0.000 claims abstract 2
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 claims abstract 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 claims abstract 2
- 241001645362 Valsa Species 0.000 claims description 19
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 7
- 239000005631 2,4-Dichlorophenoxyacetic acid Substances 0.000 claims description 6
- HXKWSTRRCHTUEC-UHFFFAOYSA-N 2,4-Dichlorophenoxyaceticacid Chemical compound OC(=O)C(Cl)OC1=CC=C(Cl)C=C1 HXKWSTRRCHTUEC-UHFFFAOYSA-N 0.000 claims description 6
- 206010020649 Hyperkeratosis Diseases 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000002562 thickening agent Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000003381 stabilizer Substances 0.000 claims description 5
- 239000012452 mother liquor Substances 0.000 claims description 4
- 235000009529 zinc sulphate Nutrition 0.000 claims description 4
- 239000011686 zinc sulphate Substances 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 229920000136 polysorbate Polymers 0.000 claims description 2
- 239000003755 preservative agent Substances 0.000 claims description 2
- 230000002335 preservative effect Effects 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims 1
- 230000008595 infiltration Effects 0.000 claims 1
- 238000001764 infiltration Methods 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 230000002265 prevention Effects 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 abstract description 2
- 230000001737 promoting effect Effects 0.000 abstract 2
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 abstract 1
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 abstract 1
- 230000035876 healing Effects 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 abstract 1
- 229960001763 zinc sulfate Drugs 0.000 abstract 1
- 229910000368 zinc sulfate Inorganic materials 0.000 abstract 1
- 241000220225 Malus Species 0.000 description 19
- 206010052428 Wound Diseases 0.000 description 14
- 208000027418 Wounds and injury Diseases 0.000 description 14
- 238000002360 preparation method Methods 0.000 description 9
- GAMFEMAXLMWCRG-UHFFFAOYSA-N bis(dimethylcarbamothioylsulfanyl)arsanyl n,n-dimethylcarbamodithioate Chemical compound CN(C)C(=S)S[As](SC(=S)N(C)C)SC(=S)N(C)C GAMFEMAXLMWCRG-UHFFFAOYSA-N 0.000 description 5
- 230000003449 preventive effect Effects 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 1
- 241000581835 Monodora junodii Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- WMGSQTMJHBYJMQ-UHFFFAOYSA-N aluminum;magnesium;silicate Chemical compound [Mg+2].[Al+3].[O-][Si]([O-])([O-])[O-] WMGSQTMJHBYJMQ-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 1
- 230000000069 prophylactic effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Cultivation Of Plants (AREA)
Abstract
The invention relates to a wound protective agent for preventing apple tree canker, which is a prevention protective agent with functions of promoting wound to heal and sterilizing. The prevention protective agent is prepared by adopting the following main components: 5g/L of zinc sulfate, 150 g/L of chinaberry, 1.0 g/L of sodium benzoate, 3.5 g/L of radix isatidis, 1.5 g/L of sodium dodecyl sulfate, 0.1mg/L of 2, 4-dichlorphenoxyacetic acid and 0.5mg/L of naphthylacetic acid of plant cell healing growth hormone substances, and 10ml/L of tween-20. Field test results show that the wound protective agent has stable prevention effect of the apple tree canker and strong property of promoting the wound to heal, is superior to the conventional farm chemical, and is suitable to heal the wound of an apple tree and prevent the canker.
Description
Technical field:
The present invention relates to a kind of Wound protective agent that prevents apple valsa canker and preparation method thereof.
Technical background:
China's apple production accounts for 46% (2008) of Gross World Product, occupies the No. 1 in the world, and the development of apple and apple industry thereof is for huge contribution has been made in Shaanxi Province's economic growth and social progress.Yet the generation of apple valsa canker has become the key factor of restriction China's apple production and outlet, has caused serious output and economic loss.Apple valsa canker distributes extensively in China, harm is heavy, control is difficult, is referred to as apple tree " cancer ".Cause when sick light that bark rots, tree vigo(u)r is weak, fruit yield and quality descend, cause when serious that mobile jib, bough and whole tree are withered, even cause the garden of ruining.China has carried out big quantity research and control exploration since the seventies in 20th century.Wherein asomate is a preventive effect better chemical medicament, but easily causes environmental pollution long, the difficult decomposition of its lasting period, has been listed in the forbidding medication; The second class chemical agent is a tpn, and it easily decomposes, the lasting period short.
Up to now, apple valsa canker still can't be controlled effectively, and is still endangering widely, and the apple industry has been caused huge threat.This area still needs to continue to develop the medicament that can be used in apple valsa canker.Consider that apple valsa canker mainly invades from wound, the present invention is in line with the theory of preventing and treating of putting prevention first, and is intended to design a kind of compliance with environmental protection requirements, easily promotes wound to produce callus, can effectively kills pathogen, long Wound protective agent of lasting period simultaneously.
Summary of the invention:
The invention provides a kind of Wound protective agent that prevents apple valsa canker and preparation method thereof.This protectant is a kind of, noresidue nontoxic to people and animals, the significant environmental protection preparation of preventive effect.
The Wound protective agent of prevention apple valsa canker of the present invention; it mainly is prepared from by zinc sulphate 5g/L, chinaberry 150g/L, Sodium Benzoate 1.0g/L, Radix Isatidis 3.5g/L, dodecyl sodium sulfate 1.5g/L, 2,4 dichlorophenoxyacetic acid 0.1mg/L, methyl 0.5mg/L, polysorbas20 10ml/L.Wherein 2,4 dichlorophenoxyacetic acid and methyl belong to plant cell callus growth hormone material, can promote the generation of callus.
Selectable, above-mentioned preparation also comprises one or more in an amount of stabilizing agent, antifreezing agent and/or the thickener, stabilizing agent, antifreezing agent, preservative, thickener are the pesticide adjuvants of this area routine, the preferred aluminium-magnesium silicate of stabilizing agent wherein, the preferred propane diols of antifreezing agent, thickener preferably polyethylene alcohol, xanthans, CMC, thickener have the effect that prolongs the water conservation time, can prolong active ingredient release time.
The preparation process of the Wound protective agent of prevention apple valsa canker is: plucks and pulverizes after the 150g chinaberry is dried in the shade, be soaked in the ethanol of 100mL, place 4 ℃ to spend the night, and standby; Preparation 2,4 dichlorophenoxyacetic acid mother liquor (concentration is 0.5mg/mL) and methyl mother liquor (concentration is 1.0mg/mL) place-20 ℃, and be standby; Get Radix Isatidis and pulverized 80 mesh sieves, standby.In proportion zinc sulphate, Sodium Benzoate, Radix Isatidis, dodecyl sodium sulfate are added in the 600mL sterile distilled water successively, after the stirring and dissolving, add 4 ℃ of chinaberrys of spending the night and invade body fluid, stirring and evenly mixing adds 2 then in proportion successively, 4-dichlorphenoxyacetic acid, methyl, tween, selectable, one or more in adding stabilizing agent, antifreezing agent and/or the thickener stir, last water is settled to 1 liter, and the container of packing into gets final product.
Concrete case study on implementation:
Wound protective agent of the present invention is used for the field preventive effect investigation of apple valsa canker: 2007-2009 selects 8-13 green apple tree to carry out the rot prophylactic tria on Shaanxi Province's acrobatic skill, Yang Ling and other places; the apple tree kind is Fuji and loud, high-pitched sound, is contrast with 100 times of liquid of 40% asomate wetting powder and clear water.Result of the test is as shown in table 1; the result shows that 3 years field efficacies of Wound protective agent of the present invention reach 95.9%; control efficiency apparently higher than 100 times of liquid of 40% asomate wetting powder; and the wound that uses Wound protective agent of the present invention to handle; wound callus formation width is 2.1cm after 3 months, obviously is better than the 0.2cm of 100 times of liquid of 40% asomate wetting powder.
The Wound protective agent field preventive effect investigation of table 1 apple valsa canker
This shows:
1. preparation of the present invention can be used for the field prevention of apple valsa canker;
2. the effect of preparation prevention apple valsa canker of the present invention is better than asomate;
3. preparation of the present invention has the powerful ability that promotes wound healing.
Claims (6)
1. Wound protective agent that is used to prevent apple valsa canker; it is characterized in that it mainly is prepared from by zinc sulphate 5g/L, chinaberry 150g/L, Sodium Benzoate 1.0g/L, Radix Isatidis 3.5g/L, dodecyl sodium sulfate 1.5g/L, 2,4 dichlorophenoxyacetic acid 0.1mg/L, methyl 0.5mg/L, polysorbas20 10ml/L.
2. Wound protective agent according to claim 1 further comprises in stabilizing agent, antifreezing agent and/or the thickener one or more.
3. prepare the method for preventing the apple valsa canker Wound protective agent according to claim 1, comprise the steps: to pluck and pulverize after the 150g chinaberry is dried in the shade, be soaked in the ethanol of 100mL, place 4 ℃ to spend the night, standby; Compound concentration is the 2,4 dichlorophenoxyacetic acid mother liquor of 0.5mg/mL and the methyl mother liquor that concentration is 1.0mg/mL, places-20 ℃, and is standby; Get Radix Isatidis and pulverized 80 mesh sieves, standby; Successively zinc sulphate, Sodium Benzoate, Radix Isatidis, dodecyl sodium sulfate are joined in the 600mL sterile distilled water in proportion, after the stirring and dissolving, add 4 ℃ of chinaberry leaching liquors that spend the night, stirring and evenly mixing, add 2,4 dichlorophenoxyacetic acid, methyl, tween at last in proportion successively, stir, be settled to 1 liter with sterile distilled water, the container of packing into.
4. the Wound protective agent that is used to prevent apple valsa canker according to claim 1, Tween20 wherein possess infiltration, expand, stick the effect of synergy.
5. the Wound protective agent that is used to prevent apple valsa canker according to claim 1, wherein said Sodium Benzoate possesses preservative efficacy.
6. the Wound protective agent that is used to prevent apple valsa canker according to claim 1,2,4 dichlorophenoxyacetic acid 0.1mg/L wherein, methyl 0.5mg/L belong to plant cell callus growth hormone material, can promote the generation of callus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101660493A CN101627773B (en) | 2009-08-05 | 2009-08-05 | Wound protective agent for preventing apple tree canker |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101660493A CN101627773B (en) | 2009-08-05 | 2009-08-05 | Wound protective agent for preventing apple tree canker |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101627773A true CN101627773A (en) | 2010-01-20 |
| CN101627773B CN101627773B (en) | 2012-07-25 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009101660493A Expired - Fee Related CN101627773B (en) | 2009-08-05 | 2009-08-05 | Wound protective agent for preventing apple tree canker |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101627773B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104855421A (en) * | 2015-06-04 | 2015-08-26 | 福建省老区隆丰农业开发有限公司 | Preparation and using methods of gummosis suppresser for fruit trees |
| CN105777341A (en) * | 2016-03-03 | 2016-07-20 | 和县朱韩瓜果种植家庭农场 | Red pear fruit tree wound protecting spray agent and preparation method thereof |
| CN105851079A (en) * | 2016-05-09 | 2016-08-17 | 山西省农业科学院果树研究所 | Bactericide for controlling fruit tree rotten diseases and preparation method and application method of bactericide for controlling fruit tree rotten diseases |
| CN107162744A (en) * | 2017-06-08 | 2017-09-15 | 合肥龙滨化工科技有限公司 | It is a kind of to prevent medicine of apple tree canker and preparation method thereof |
| CN110115170A (en) * | 2019-03-20 | 2019-08-13 | 甘肃农业大学 | A method for the treatment of apple tree canker |
-
2009
- 2009-08-05 CN CN2009101660493A patent/CN101627773B/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104855421A (en) * | 2015-06-04 | 2015-08-26 | 福建省老区隆丰农业开发有限公司 | Preparation and using methods of gummosis suppresser for fruit trees |
| CN105777341A (en) * | 2016-03-03 | 2016-07-20 | 和县朱韩瓜果种植家庭农场 | Red pear fruit tree wound protecting spray agent and preparation method thereof |
| CN105851079A (en) * | 2016-05-09 | 2016-08-17 | 山西省农业科学院果树研究所 | Bactericide for controlling fruit tree rotten diseases and preparation method and application method of bactericide for controlling fruit tree rotten diseases |
| CN105851079B (en) * | 2016-05-09 | 2018-09-21 | 山西省农业科学院果树研究所 | A kind of fungicide and its preparation and application of prevention fruit tree putrefaction disease |
| CN107162744A (en) * | 2017-06-08 | 2017-09-15 | 合肥龙滨化工科技有限公司 | It is a kind of to prevent medicine of apple tree canker and preparation method thereof |
| CN110115170A (en) * | 2019-03-20 | 2019-08-13 | 甘肃农业大学 | A method for the treatment of apple tree canker |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101627773B (en) | 2012-07-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Free format text: FORMER OWNER: WANG BAOTONG ZHAO ZHENGYANG Effective date: 20121228 Owner name: NORTHWEST A + F UNIVERSITY Free format text: FORMER OWNER: HU XIAOPING Effective date: 20121228 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20121228 Address after: 712100 Shaanxi Province Tai Road No. 3 in Yangling demonstration zone Patentee after: Northwest A & F University Address before: 712100 School of plant protection, Northwest Agriculture and Forestry University, 22 West Agricultural Road, Yangling demonstration area, Shaanxi Patentee before: Hu Xiaoping Patentee before: Wang Baotong Patentee before: Zhao Zhengyang |
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| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120725 Termination date: 20130805 |