CN101606750A - Radish seed extract and as the purposes of additive of tobacco product - Google Patents
Radish seed extract and as the purposes of additive of tobacco product Download PDFInfo
- Publication number
- CN101606750A CN101606750A CNA2008100480361A CN200810048036A CN101606750A CN 101606750 A CN101606750 A CN 101606750A CN A2008100480361 A CNA2008100480361 A CN A2008100480361A CN 200810048036 A CN200810048036 A CN 200810048036A CN 101606750 A CN101606750 A CN 101606750A
- Authority
- CN
- China
- Prior art keywords
- radish seed
- seed extract
- extract
- extractant
- feed liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000284 extract Substances 0.000 title claims abstract description 83
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 title claims abstract description 64
- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 23
- 239000000654 additive Substances 0.000 title claims abstract description 18
- 230000000996 additive effect Effects 0.000 title claims abstract description 18
- 244000088415 Raphanus sativus Species 0.000 title 1
- 241000220259 Raphanus Species 0.000 claims abstract description 63
- 239000007788 liquid Substances 0.000 claims abstract description 32
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 31
- 241000208125 Nicotiana Species 0.000 claims abstract description 27
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 27
- 238000000926 separation method Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000006227 byproduct Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 238000001556 precipitation Methods 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 7
- 230000001105 regulatory effect Effects 0.000 claims abstract description 7
- 150000007524 organic acids Chemical class 0.000 claims abstract description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 4
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 3
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 3
- 239000001630 malic acid Substances 0.000 claims description 3
- 235000011090 malic acid Nutrition 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- WLJVXDMOQOGPHL-PPJXEINESA-N 2-phenylacetic acid Chemical compound O[14C](=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-PPJXEINESA-N 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000000151 deposition Methods 0.000 claims description 2
- 239000002798 polar solvent Substances 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 4
- 125000003118 aryl group Chemical group 0.000 abstract description 4
- 239000003546 flue gas Substances 0.000 abstract description 4
- 239000007787 solid Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 6
- 238000000605 extraction Methods 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000000779 smoke Substances 0.000 description 3
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- WLJVXDMOQOGPHL-UHFFFAOYSA-N phenylacetic acid Chemical compound OC(=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229960003424 phenylacetic acid Drugs 0.000 description 1
- 239000003279 phenylacetic acid Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Images
Abstract
The present invention relates to a kind of radish seed extract and as the purposes of additive of tobacco product.It is earlier organic acid to be joined in the extractant, regulating extractant pH value is 4.5～6.5, extractant and radish seed volume ratio are 1～5, extract 1～5 hour at 50～90 ℃, isolate feed liquid after, the water and the precipitation separation that add 1～5 times of material liquid volume, feed liquid after the separation is concentrated into the medicinal extract shape, returns molten medicinal extract with 5～10 times of extractants, once more the isolated by filtration byproduct, feed liquid is concentrated into the medicinal extract shape once more, promptly obtains radish seed extract.Radish seed extract can be used as additive of tobacco product and adds in the pipe tobacco of cigarette, and the radish seed extract that is added in the pipe tobacco accounts for 0.01%～0.05% of pipe tobacco weight.The radish seed extract that adds flavouring effectively when tobacco product aspirate, and fragrance is abundant, the solid sense of increase flue gas; And radish seed extract can also be given the aromatic and the note of tobacco product uniqueness.
Description
Technical field
The present invention relates to the application of a kind of natural plant extracts in tobacco product, specifically a kind of radish seed extract and as the purposes of additive of tobacco product.
Background technology
" Chinese style cigarette " core competitiveness is to form the selling point style, embodies personalization and differentiation, adapts to sucking of Chinese wide consumer and is accustomed to and consumer need.The Chinese style essence spice for cigarette is Chinese style cigarette product " soul ", is the secret place that " Chinese style cigarette " style characteristic forms.Flavoring and casing scientifically in cigarette, the important means of the personalized style of outstanding cigarette product just.Simultaneously, in order to improve the security of smoking, lowering harm and decreasing coking becomes an important component part of " Chinese style cigarette ".When reducing coke tar in cigarette, promote and raising flue gas concentration and fragrance, also only by means of the flavoring and casing technology.Along with going deep into of Chinese style cigarette lowering harm and decreasing coking work, reinforced its importance that demonstrates further of tobacco flavoring.
Construct the Chinese style essence spice for cigarette and the new technology of independent intellectual property right, from the natural herbal plant, extract essence and flavoring agent, succession Chinese herbal medicine in thousand is used for cigarette, allow the refined perfume (or spice) of healthy theory along with cigarette, moving towards the consumer together, is one of basic research of development " Chinese style cigarette ".
Radish seed has the fragrance style of self uniqueness, and contains multiple aldehydes, ketone, ester type compound in the radish seed, has the prospect as essence spice for cigarette.But what see report at present has only radish seed and carries thing and be used to Chinese medicine, and extraction process is that simple water is carried or alcohol extraction process, does not see that radish seed extract is used to the bibliographical information of cigarette additive.And in our research process, find the simple resulting radish seed extract of extraction process, have bigger negative effect, can't satisfy instructions for use as cigarette additive by water extract-alcohol precipitation or alcohol extracting-water precipitating.
Summary of the invention
Purpose of the present invention is exactly the defective at prior art, provides a kind of radish seed extract and as the purposes of additive of tobacco product.
Radish seed extract of the present invention is to adopt radish seed for extracting raw material, is extractant with the polar solvent, carries out abstraction reaction, adopt the depositing in water technology will extract byproduct and separate, again feed liquid is concentrated into the medicinal extract shape, use extractant Hui Rong, isolated by filtration once more, the gained feed liquid is extract of the present invention.Wherein said extractant is 40～80% ethanol water.
Extracting method of the present invention may further comprise the steps: adopt radish seed for extracting raw material, earlier organic acid is joined in the extractant, regulating extractant pH value is 4.5～6.5, extractant and radish seed volume ratio are 1～5, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, the water and the precipitation separation that add 1～5 times of material liquid volume, feed liquid after the separation is concentrated into the medicinal extract shape, return molten medicinal extract with 5～10 times of extractants, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains radish seed extract of the present invention.
Extracting method of the present invention technical scheme preferably is that described organic acid is phenylacetic acid, citric acid, malic acid or citric acid; Described extractant is 40～80% ethanol water.
Radish seed extract of the present invention is as the purposes of additive of tobacco product, and it is that radish seed extract is added in the pipe tobacco of cigarette, and the radish seed extract that is added in the pipe tobacco accounts for 0.01%～0.05% of pipe tobacco weight, and preferred 0.02%～0.04%.
Technical scheme is that radish seed extract is dissolved in the solvent preferably, the solvent that is dissolved with radish seed extract is rolled at the pipe tobacco of production of cigarettes be sprayed in the process on the pipe tobacco, subsequently evaporating solvent; Described solvent is 95% ethanol.
A series of experimental study results that smoke panel test of patent applicant show, the radish seed extract of adding flavouring effectively when tobacco product aspirates, and fragrance is abundant, increases the solid sense of flue gas; And radish seed extract can also be given the aromatic and the note of tobacco product uniqueness.And when improving the tobacco product mouthfeel, can avoid introducing negative effects such as assorted gas, increase excitant.
The present invention has opened up a new application for radish seed extract, has increased new effect and the effect of radish seed.Radish seed extract is as additive of tobacco product, and effect is obvious, and " Chinese style cigarette " goods of developing characteristic style are had good application prospects.
Description of drawings
Fig. 1 is a process schematic representation of the present invention.
The specific embodiment
The present invention is described further below by embodiment.
The extraction of embodiment 1 radish seed
Earlier phenylacetic acid is joined in 75% ethanol water, regulating ethanol water pH value is 5.0, and ethanol water and radish seed volume ratio are 3, extracts 3 hours at 90 ℃, after isolating feed liquid, add the water and the precipitation separation of 2 times of material liquid volumes, the feed liquid after the separation is concentrated into the medicinal extract shape, and density is 1.1, with 8 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains radish seed extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 2
Earlier citric acid is joined in 75% ethanol water, regulating ethanol water pH value is 5.5, and ethanol water and radish seed volume ratio are 5, extracts 4 hours at 50 ℃, after isolating feed liquid, add the water and the precipitation separation of 2 times of material liquid volumes, the feed liquid after the separation is concentrated into the medicinal extract shape, and density is 1.3, with 8 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains radish seed extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 3
Earlier malic acid is joined in 75% ethanol water, regulating ethanol water pH value is 4.5, and ethanol water and radish seed volume ratio are 2, extracts 2 hours at 60 ℃, after isolating feed liquid, add the water and the precipitation separation of 2 times of material liquid volumes, the feed liquid after the separation is concentrated into the medicinal extract shape, and density is 1.2, with 5 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains radish seed extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 4
Earlier citric acid is joined in 75% ethanol water, regulating ethanol water pH value is 6.5, and ethanol water and radish seed volume ratio are 4, extracts 5 hours at 80 ℃, after isolating feed liquid, add the water and the precipitation separation of 2 times of material liquid volumes, the feed liquid after the separation is concentrated into the medicinal extract shape, and density is 1.2, with 6 times of extractant Hui Rong, the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains radish seed extract of the present invention.This extract can be used for additive of tobacco product.
Embodiment 5 adds the extract that is obtained in the pipe tobacco of cigarette
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.Be added into the radish seed extract in the pipe tobacco, account for 0.03% of pipe tobacco weight.Concrete grammar is earlier radish seed extract to be dissolved in the ethanol, and the Diluted Alcohol that is dissolved with radish seed extract evenly is sprayed on the pipe tobacco, and ethanol evaporation is fallen subsequently.Pipe tobacco rolls into test sample cigarette through cigarette machine.
Effect experiment in embodiment 6 cigarette smokes
Be taken at two parts of the good finished cut tobacco of 22 ℃ ± 1 ℃ of temperature and 60% ± 2% time balance of relative humidity (RH) 40 grams, take by weighing radish seed extract by 0.04% of its quality, after the dilution of 95% ethanol, be sprayed on the pipe tobacco equably with the larynx jet pipe, perfuming and not the aromatic tobacco sample be placed in the climatic chamber of 22 ℃ ± 1 ℃ of temperature and RH60% ± 2% balance 48 hours, with fill out the cigarette device respectively with perfuming and not the pipe tobacco of perfuming make cigarette and prop up, 22 ℃ ± 1 ℃ and RH60% ± 2% time balance 48 hours, please cigarette sensory evaluating smoking group smoke panel test again.
The personnel that smoke panel test are consistent to think the radish seed extract that adds flavouring effectively when tobacco product aspirate, and fragrance is abundant, the solid sense of increase flue gas; And radish seed extract can also be given the aromatic and the note of cigarette uniqueness.
Claims (9)
1, a kind of radish seed extract, it is to adopt radish seed for extracting raw material, with the polar solvent is extractant, carry out abstraction reaction, adopt the depositing in water technology will extract byproduct and separate, again feed liquid is concentrated into the medicinal extract shape, use extractant Hui Rong, isolated by filtration once more, the gained feed liquid is extract of the present invention.
2, radish seed extract according to claim 1, wherein said extractant are 40～80% ethanol water.
3, a kind of extracting method of radish seed extract, it may further comprise the steps: adopt radish seed for extracting raw material, earlier organic acid is joined in the extractant, regulating extractant pH value is 4.5～6.5, extractant and radish seed volume ratio are 1～5, extracted 1～5 hour at 50～90 ℃, after isolating feed liquid, the water and the precipitation separation that add 1～5 times of material liquid volume, feed liquid after the separation is concentrated into the medicinal extract shape, returns molten medicinal extract with 5～10 times of extractants, once more the isolated by filtration byproduct, feed liquid is concentrated into the medicinal extract shape once more, promptly obtains radish seed extract of the present invention.
4, the extracting method of radish seed extract according to claim 3, wherein said organic acid are phenylacetic acid, citric acid, malic acid or citric acid.
5, the extracting method of radish seed extract according to claim 3, wherein said extractant are 40～80% ethanol water.
6, radish seed extract is as the purposes of additive of tobacco product, and it is that radish seed extract is added in the pipe tobacco of cigarette, and the radish seed extract that is added in the pipe tobacco accounts for 0.01%～0.05% of pipe tobacco weight.
7, radish seed extract according to claim 6 is as the purposes of additive of tobacco product, and the radish seed extract that wherein is added in the pipe tobacco accounts for 0.02%～0.04% of pipe tobacco weight.
8, radish seed extract according to claim 6 wherein is dissolved in radish seed extract in the solvent as the purposes of additive of tobacco product, the solvent that is dissolved with radish seed extract is rolled in the process at the pipe tobacco of production of cigarettes be sprayed on the pipe tobacco.
9, radish seed extract according to claim 8 is as the purposes of additive of tobacco product, and wherein said solvent is 95% ethanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100480361A CN101606750B (en) | 2008-06-16 | 2008-06-16 | Radish seed extract and application thereof as tobacco product additive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100480361A CN101606750B (en) | 2008-06-16 | 2008-06-16 | Radish seed extract and application thereof as tobacco product additive |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101606750A true CN101606750A (en) | 2009-12-23 |
| CN101606750B CN101606750B (en) | 2012-02-08 |
Family
ID=41480791
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100480361A Expired - Fee Related CN101606750B (en) | 2008-06-16 | 2008-06-16 | Radish seed extract and application thereof as tobacco product additive |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101606750B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN104905398A (en) * | 2015-05-29 | 2015-09-16 | 湖北中烟工业有限责任公司 | Alfalfa leaf extract preparation method and use as tobacco product additive |
| CN106235397A (en) * | 2016-09-09 | 2016-12-21 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Artemisia dracunculus cigarette extract |
| CN108201166A (en) * | 2016-12-16 | 2018-06-26 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette extract and preparation method thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1241904C (en) * | 2004-05-11 | 2006-02-15 | 上海纳贝生物技术有限责任公司 | Method for preparing active ingredient of sinapine |
| KR100626398B1 (en) * | 2005-03-11 | 2006-09-20 | 박선호 | Mixtures of antioxidand supplement for current or former smokers and manufacturing method therof |
| CN101062081A (en) * | 2006-04-25 | 2007-10-31 | 长春英联生物技术有限公司 | Dispersing tablets for reducing dizzy feeling and pressure and the preparing method thereof |
| CN100518776C (en) * | 2007-05-11 | 2009-07-29 | 由能力 | Health protection tea for reducing blood pressure, and blood fat, and preparation method |
-
2008
- 2008-06-16 CN CN2008100480361A patent/CN101606750B/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103349355A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Black pepper and dark plum compound extract, preparation method thereof and application of compound extract taken as tobacco product additive |
| CN103349355B (en) * | 2013-06-28 | 2016-03-09 | 湖北中烟工业有限责任公司 | Black pepper dark plum composite extract and preparation method thereof and the purposes as additive of tobacco product |
| CN104905398A (en) * | 2015-05-29 | 2015-09-16 | 湖北中烟工业有限责任公司 | Alfalfa leaf extract preparation method and use as tobacco product additive |
| CN106235397A (en) * | 2016-09-09 | 2016-12-21 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of Artemisia dracunculus cigarette extract |
| CN108201166A (en) * | 2016-12-16 | 2018-06-26 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette extract and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101606750B (en) | 2012-02-08 |
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