CN101584439A - Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule - Google Patents
Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule Download PDFInfo
- Publication number
- CN101584439A CN101584439A CNA2009100121715A CN200910012171A CN101584439A CN 101584439 A CN101584439 A CN 101584439A CN A2009100121715 A CNA2009100121715 A CN A2009100121715A CN 200910012171 A CN200910012171 A CN 200910012171A CN 101584439 A CN101584439 A CN 101584439A
- Authority
- CN
- China
- Prior art keywords
- raspberry
- freeze
- dried powder
- capsule
- fruit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000011034 Rubus glaucus Nutrition 0.000 title claims abstract description 36
- 235000009122 Rubus idaeus Nutrition 0.000 title claims abstract description 36
- 240000007651 Rubus glaucus Species 0.000 title claims abstract description 31
- 239000002775 capsule Substances 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000009777 vacuum freeze-drying Methods 0.000 title claims abstract description 8
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 18
- 238000004821 distillation Methods 0.000 claims abstract description 9
- 238000010298 pulverizing process Methods 0.000 claims abstract description 9
- 230000005540 biological transmission Effects 0.000 claims description 7
- 238000004108 freeze drying Methods 0.000 claims description 7
- 238000012856 packing Methods 0.000 abstract description 7
- 238000005516 engineering process Methods 0.000 abstract description 6
- 235000015203 fruit juice Nutrition 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 235000013402 health food Nutrition 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 description 6
- 244000235659 Rubus idaeus Species 0.000 description 5
- 102000019197 Superoxide Dismutase Human genes 0.000 description 5
- 108010012715 Superoxide dismutase Proteins 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- 235000011430 Malus pumila Nutrition 0.000 description 3
- 235000015103 Malus silvestris Nutrition 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 2
- 241000220222 Rosaceae Species 0.000 description 2
- 241001092459 Rubus Species 0.000 description 2
- 229930003268 Vitamin C Natural products 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 235000019154 vitamin C Nutrition 0.000 description 2
- 239000011718 vitamin C Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241000220225 Malus Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 230000003579 anti-obesity Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 235000019990 fruit wine Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000015094 jam Nutrition 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- VWMVAQHMFFZQGD-UHFFFAOYSA-N p-Hydroxybenzyl acetone Natural products CC(=O)CC1=CC=C(O)C=C1 VWMVAQHMFFZQGD-UHFFFAOYSA-N 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- NJGBTKGETPDVIK-UHFFFAOYSA-N raspberry ketone Chemical compound CC(=O)CCC1=CC=C(O)C=C1 NJGBTKGETPDVIK-UHFFFAOYSA-N 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Storage Of Fruits Or Vegetables (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a kind of technology of utilizing vacuum freeze-drying method to produce raspberry active freeze-dried powder and capsule, it is characterized in that it selects fruit of raspberry for use is basic material.Through technologies such as cleaning, pre-freeze, distillation, parsing-desiccation, pulverizing, packing, capsule finished products, obtain the raspberry active freeze-dried powder, can be used as health foods such as preparation capsule, fruit juice.This product has the low characteristics of production cost, and plays the double effects of exploiting natural resources and keeping heat-sensitive active functional substances.
Description
Technical field
The present invention relates to a kind of method of utilizing vacuum freeze-drying method to produce raspberry active freeze-dried powder and capsule, belong to field of food industry.
Background technology
Raspberry (Rubus L.) belongs to the rose family (Rosaceae), and rubus is the important economic shrub of small fruit type, have the result early, advantages such as income is fast, taste of fruit is good, nutritive value height, be described as emerging third generation fruit tree.
Raspberry is planted promptly certain output in back 1 year, entered the best fruiting period on the 3rd year, and 20～25 years economic lifves, per mu yield can reach 1000～2000 kilograms.Raspberry has unique perfume and natural colouring matter, the content about 10% of sugar.Similar to apple, pears, citrus three big fruit, acid content 0.62～2.17%, amino acid content is higher than apple, glucose.Vitamin C is 5 times of apple.Be rich in vitamin E and selenium, its anti-ageing material superoxide dismutase (SOD) and cancer-resisting substance (tanning acid) content is higher than existing any cultivation and wild fruit at 1.6～2.1mg/100g.Its root, stem, leaf also all have medicinal efficacy, integrate food and health care.At aspects such as food, medicine, cosmetics, health cares purposes is widely arranged, have exploitation and be worth.
Raspberry both can be eaten raw, also can be processed into products such as freeze-dried powder, fruit juice, jam, fruit wine.Plant the raspberry ketone that contains in the skin, have antiobesity action, extremely the women welcomes.
Raspberry also is the quality raw materials that extract natural colouring matter.Fresh fruit because of the different anthocyanidin contents of kind between 30～50mg/100g.
The basic autoclave sterilization mode that adopts solves the spoilage problem that microbial contamination causes in the fresh-keeping technology of guaranteeing the quality of traditional fruit juice.Studies show that the vitamin C loss is more than 20% under hot and humid condition.Vitamin A is preserved loss 35～42% in 3 months under hot and humid condition.Anti-ageing material superoxide dismutase (SOD) is under 70 ℃ of high temperature, and the SOD activity linearly descends, with a toll of about 75%.Secondly illumination, oxidation reaction all can influence these active agent stability.
Summary of the invention
The objective of the invention is to it is characterized in that the present invention relates to a kind of technology of utilizing vacuum freeze-drying method to produce raspberry active freeze-dried powder and capsule it selects fruit of raspberry for use is basic material.Through technologies such as cleaning, pre-freeze, distillation, parsing-desiccation, pulverizing, packing, capsule finished products, obtain the raspberry active freeze-dried powder, can be used as health foods such as preparation capsule, fruit juice.Factor affecting such as that process can be avoided is hot and humid, illumination, oxidation, this product also has the low characteristics of production cost, and plays the double effects of exploiting natural resources and preserving whole heat-sensitive active functional substances.
The objective of the invention is to realize through the following steps:
Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder, may further comprise the steps:
1) fruit of raspberry is cleaned, drains standby;
2) fruit of raspberry after will draining is-26～-30 ℃ of following pre-freezes, and vacuum is 50～100Pa, keeps constant temperature 1～1.5 hour;
3) with the raspberry lyophilization that obtains, between-32～-35 ℃, in order to the carrying out of the transmission and the distillation of heat;
4) the fruit of raspberry resolution temperature that obtains is controlled between 50～55 ℃, 4～8 hours 20～60Pa time, is the raspberry active freeze-dried powder through pulverizing.
The raspberry active freeze-dried powder that makes according to the method described above incapsulated be raspberry active freeze-dried powder capsule finished product.
The specific embodiment
The following examples just are used to illustrate the present invention, are not construed as limiting the invention.
Embodiment 1
With fruit of raspberry pretreatment of raw material (cleaning, drain standby) → pre-freeze (-28 ℃ of pre-freezes, vacuum is that 50Pa kept constant temperature 1.3 hours) → lyophilization (at-33 ℃, in order to the carrying out of the transmission and the distillation of heat.Also claim primary drying) → parsing-desiccation (, 6 hours 30Pa time, also claiming redrying) → pulverizing → metering packing → capsule (0.8g/ is only) → storage at 50 ℃.
Embodiment 2
With fruit of raspberry pretreatment of raw material → pre-freeze (-27 ℃ of pre-freezes, vacuum is that 70Pa kept constant temperature 1.2 hours) → lyophilization (at-34 ℃, in order to the carrying out of the transmission and the distillation of heat.Also claim primary drying) → parsing-desiccation (, 5.5 hours 45Pa time, also claiming redrying) → pulverizing → metering packing → capsule (1.2g/ is only) → storage at 52 ℃.
Embodiment 3
With fruit of raspberry pretreatment of raw material → pre-freeze (-29 ℃ of pre-freezes, vacuum is that 80Pa kept constant temperature 1 hour) → lyophilization (between-32 ℃, in order to the carrying out of the transmission and the distillation of heat.Also claim primary drying) → parsing-desiccation (, 6 hours 55Pa time, also claiming redrying) → pulverizing → metering packing → capsule (1.5g/ is only) → storage below 54 ℃.
Embodiment 4
With fruit of raspberry pretreatment of raw material → pre-freeze (-30 ℃ of pre-freezes, vacuum is that 100Pa kept constant temperature 1.5 hours) → lyophilization (between-35 ℃, in order to the carrying out of the transmission and the distillation of heat.Also claim primary drying) → parsing-desiccation (, 8 hours 20Pa time, also claiming redrying) → pulverizing → metering packing → capsule (1.5g/ is only) → storage below 55 ℃.
Embodiment 5
With fruit of raspberry pretreatment of raw material → pre-freeze (-26 ℃ of pre-freezes, vacuum is 90Pa, keep constant temperature 1.5 hours) → lyophilization (between-35 ℃, in order to the carrying out of the transmission and the distillation of heat., also claim primary drying) → parsing-desiccation (, 8 hours 60Pa time, also claiming redrying) → pulverizing → metering packing → capsule (1.5g/ is only) → storage below 55 ℃.
Claims (2)
1, utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder, may further comprise the steps:
1) fruit of raspberry is cleaned, drains standby;
2) fruit of raspberry after will draining is-26～-30 ℃ of following pre-freezes, and vacuum is 50～100Pa, keeps constant temperature 1～1.5 hour;
3) with the raspberry lyophilization that obtains, between-32～-35 ℃, in order to the carrying out of the transmission and the distillation of heat;
4) the fruit of raspberry resolution temperature that obtains is controlled between 50～55 ℃, 4～8 hours 20～60Pa time, is the raspberry active freeze-dried powder through pulverizing.
2, utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder capsule, will incapsulate according to the described raspberry active freeze-dried powder of claim 1 and be raspberry active freeze-dried powder capsule finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2009100121715A CN101584439A (en) | 2009-06-22 | 2009-06-22 | Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2009100121715A CN101584439A (en) | 2009-06-22 | 2009-06-22 | Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101584439A true CN101584439A (en) | 2009-11-25 |
Family
ID=41369031
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2009100121715A Pending CN101584439A (en) | 2009-06-22 | 2009-06-22 | Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101584439A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101849654A (en) * | 2010-05-14 | 2010-10-06 | 江苏省农业科学院 | Preparation method of strawberry active freeze-drying flour |
| CN101849655A (en) * | 2010-05-14 | 2010-10-06 | 江苏省农业科学院 | Preparation method of blackberry active freeze-dried whole powder |
| CN102630787A (en) * | 2012-04-16 | 2012-08-15 | 张明玉 | Composite raspberry fruit tea and processing method thereof |
| CN102687861A (en) * | 2011-03-24 | 2012-09-26 | 辽宁今日农业有限公司 | Raspberry seed oil soft capsule and preparation method thereof |
| CN103284143A (en) * | 2012-03-31 | 2013-09-11 | 蔡晓鹏 | Rubus chingii decoction piece and preparation method thereof |
| CN103750328A (en) * | 2014-01-25 | 2014-04-30 | 山东黑尚莓生物技术发展股份有限公司 | Freeze-dried compound berry superfine powder and production method thereof |
| CN103875798A (en) * | 2014-04-14 | 2014-06-25 | 丹东君澳食品有限公司 | Freeze drying processing method of raspberries |
| CN104146223A (en) * | 2014-05-30 | 2014-11-19 | 呼玛县天地山野产品有限责任公司 | Preparation method of raspberry lyophilized powder |
| CN105796678A (en) * | 2016-03-23 | 2016-07-27 | 辽宁大学 | Application of raspberry freeze-dried powder or extract thereof to preparation of medicine for treating acute/chronic inflammatory bowel diseases |
| CN109674929A (en) * | 2017-10-18 | 2019-04-26 | 辽宁哈维尼克斯保健食品制造有限公司 | A kind of black raspberry fruit freeze-dried powder composite oral liquid prescription and preparation method thereof |
-
2009
- 2009-06-22 CN CNA2009100121715A patent/CN101584439A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101849654A (en) * | 2010-05-14 | 2010-10-06 | 江苏省农业科学院 | Preparation method of strawberry active freeze-drying flour |
| CN101849655A (en) * | 2010-05-14 | 2010-10-06 | 江苏省农业科学院 | Preparation method of blackberry active freeze-dried whole powder |
| CN102687861A (en) * | 2011-03-24 | 2012-09-26 | 辽宁今日农业有限公司 | Raspberry seed oil soft capsule and preparation method thereof |
| CN103284143A (en) * | 2012-03-31 | 2013-09-11 | 蔡晓鹏 | Rubus chingii decoction piece and preparation method thereof |
| CN103284143B (en) * | 2012-03-31 | 2014-10-08 | 蔡晓鹏 | Rubus chingii decoction piece and preparation method thereof |
| CN102630787A (en) * | 2012-04-16 | 2012-08-15 | 张明玉 | Composite raspberry fruit tea and processing method thereof |
| CN103750328A (en) * | 2014-01-25 | 2014-04-30 | 山东黑尚莓生物技术发展股份有限公司 | Freeze-dried compound berry superfine powder and production method thereof |
| CN103750328B (en) * | 2014-01-25 | 2015-08-19 | 山东黑尚莓生物技术发展股份有限公司 | A kind of freeze drying compound berry Ultramicro-powder and production method thereof |
| CN103875798A (en) * | 2014-04-14 | 2014-06-25 | 丹东君澳食品有限公司 | Freeze drying processing method of raspberries |
| CN104146223A (en) * | 2014-05-30 | 2014-11-19 | 呼玛县天地山野产品有限责任公司 | Preparation method of raspberry lyophilized powder |
| CN105796678A (en) * | 2016-03-23 | 2016-07-27 | 辽宁大学 | Application of raspberry freeze-dried powder or extract thereof to preparation of medicine for treating acute/chronic inflammatory bowel diseases |
| CN109674929A (en) * | 2017-10-18 | 2019-04-26 | 辽宁哈维尼克斯保健食品制造有限公司 | A kind of black raspberry fruit freeze-dried powder composite oral liquid prescription and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101584439A (en) | Utilize vacuum freeze-drying method to produce the method for raspberry active freeze-dried powder and capsule | |
| US8691220B2 (en) | Powdery malted rice extract composition | |
| KR20160058389A (en) | Method of Manufacturing Volumizing Antocyanine Probiotics Metabolite and Pharmetics, cosmetics and Juice and food complex | |
| CN105146538A (en) | Preparation method of enzyme powder | |
| CN108065155A (en) | Hawthorn tartaric acid beverage and preparation method thereof | |
| CN101579092A (en) | Method for producing active seabuckthorn freeze-drying powder and capsule thereof by using vacuum freeze-drying method | |
| US20090191294A1 (en) | Grape cane product, and method of making | |
| KR20160045520A (en) | Fermantation of Aronia's Extract | |
| KR101348311B1 (en) | Fermented extract of garlic and manufacturing process of the same | |
| CN106234862A (en) | A kind of functional drinks preparation method rich in selenium and strontium | |
| CN107535934A (en) | A kind of Blueberry frozen and preparation method thereof | |
| KR101348313B1 (en) | Fermented extract of guava and manufacturing process of the same | |
| KR102094084B1 (en) | Aged and complex-fermented mountain-cultivated ginseng having increased ginsenosides of human body absorption type and omega-6 fatty acid, and preparation method thereof | |
| CN109497516A (en) | A kind of preparation method of comprehensive fruit grain vegetable ferment | |
| CN109567086A (en) | A kind of quick freezing mango puree and preparation method thereof | |
| KR101037572B1 (en) | Powder manufacturing process using rind and pip of rubus coreanus | |
| KR20090078013A (en) | Blood glucose dropping mulberry leaf tea cultured with phellinus linteus mycelium | |
| RU2591128C1 (en) | Method for production of dietary marmalade from feijoa | |
| CN101849655A (en) | Preparation method of blackberry active freeze-dried whole powder | |
| CN107509838A (en) | A kind of preparation method of fermented black rice tea | |
| CN106418498A (en) | Method for preparing enzyme by using lemons and galangal as main materials | |
| RU2407407C2 (en) | Composition of ingredients for vitamin drink | |
| JP2021515549A (en) | Natural fermentation composition of pollen using ice tongue water and its production method | |
| CN109730216A (en) | Stems of dragon fruits gel stoste extracting method | |
| KR20190073912A (en) | Anti-oxidant and anti-inflammatory composition comprising a pear processing byproducts, and manufacturing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |
Open date: 20091125 |