CN101565762A - Production process for starch sugar - Google Patents

Production process for starch sugar Download PDF

Info

Publication number
CN101565762A
CN101565762A CNA2009101168583A CN200910116858A CN101565762A CN 101565762 A CN101565762 A CN 101565762A CN A2009101168583 A CNA2009101168583 A CN A2009101168583A CN 200910116858 A CN200910116858 A CN 200910116858A CN 101565762 A CN101565762 A CN 101565762A
Authority
CN
China
Prior art keywords
liquefier
starch
slag
sugar
jar
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CNA2009101168583A
Other languages
Chinese (zh)
Other versions
CN101565762B (en
Inventor
刘刚
李玉强
邓中兵
谢虎
王银生
彭绍春
贺存鲜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Mount Holyoke food source Biological Technology Co., Ltd.
Original Assignee
ANHUI UNITED WELL TECHNOLOGY Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI UNITED WELL TECHNOLOGY Ltd filed Critical ANHUI UNITED WELL TECHNOLOGY Ltd
Priority to CN2009101168583A priority Critical patent/CN101565762B/en
Publication of CN101565762A publication Critical patent/CN101565762A/en
Application granted granted Critical
Publication of CN101565762B publication Critical patent/CN101565762B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

The invention discloses a starch sugar production process, which comprises steps of rice pulverizing, liquifying, deslagging, saccharifying, decoloring, ion exchanging, concentrating, packing or the like. According to the invention, a high temperature high pressure spraying method is applied to a regulated starch milk charged with high temperature resistant a-amylase, so that a hollow cylindrical thin-film is formed by the starch milk under high temperature high pressure condition in the ejector, Van der Waals force between starch molecule is broken, which is beneficial for biochemical action of high temperature resistant a-amylase, the a-1,4 glycosidic bond of starch chain is rapidly cut. The problem of starch milk thorough hydrolysis is solved; temperature of liquefier is lowered to the physico-chemical temperature through two times of flash evaporation, concentration of sugar liquor is enhanced from 33% to 37%, and a large amount of steam is saved for the concentration step; by the improvement of the one-time deslagging and the one-time slag washing, not only 10% of sugar content is recovered from the sugar slag for enhancement of yield, but also protein content in the sugar slag is enhanced for earning increasing; by adopting counter current carbon discharging decoloring process, not only process requirement is ensured, but also the carbon cost is saved.

Description

A kind of production process for starch sugar
Technical field
The invention belongs to a kind of food production process, specifically is a kind of production method of Dian Fentang.
Background technology
China's rice processing industry, a large amount of the cracking rice of annual generation, these parts of cracking rice are as feed, partly as Nulomoline, as with these raw material processing and utilizations, can be enterprises engaged in processing agricultural products increases a considerable income, is processed into the carbohydrate product simultaneously, can satisfy the demands of consumers again.
With regard to present domestic Dian Fentang manufacturing enterprise, its technological line has acid system, enzyme process, acid-enzyme hydrolysis method, double-enzyme method, five kinds of methods of solid phase isomery enzyme process.No matter be to take which kind of technology, its core content all is the hydrolytic process of starch.There are three kinds of principal reactions in the starch hydrolytic process: the one, be hydrolyzed to glucose; The 2nd, be combined into compounding sugars such as isomaltose again after being hydrolyzed into glucose; The 3rd, breakdown of glucose generates 5-hydrocarbon methyl alditol and coloring matter.In concrete production technique, the degree of amylolytic speed, hydrolysis, liquefaction, saccharification, purification, crystallization, starch material, catalytic efficiency and processing unit performance etc. all can influence the quality of starch liquid sugar.Starch kind difference, its molecular structure are also different, also have different influences, the length of liquefying time directly to have influence on the performance and the production cycle of production capacity to liquefaction.
Summary of the invention
The purpose of this invention is to provide a kind of production process for starch sugar, break domestic comparatively traditional production method at present, add necessary sophisticated equipment in process of production, appropriate change processing parameter in technical process has advantages such as technology controlling and process is stable, comprehensive consumption is few, quality product is high, production cost is low, environmental protection pressure is little.
Technical scheme of the present invention is as follows:
A kind of production process for starch sugar is characterized in that carrying out successively following steps:
(1) soaks, grinds rice: after raw material is cracked rice and soak certain hour in water, remove impurity, grind into starch milk, adding clear water or slag washing water adjustment concentration is 33%, regulating the starch milk pH value by edible soda ash simultaneously is 5.9-6.0, to guarantee to liquefy effect stability and produce that postorder is working properly to be carried out;
(2) once liquefaction: the starch milk after the allotment of mill rice is pressed the heavy amount of 6-8U/ grammeter and is added efficient high-temperature resistant a-amylase, stir, after eight to ten minutes, with steam starch milk being heated to 108-110 ℃ liquefies and is ejected into the pressurize jar, the pressurize pressure tank is controlled to be 0.2-0.4MPa, temperature control is 108-110 ℃ in jar, material stops after 5-7 minute in the pressurize jar, enter flash system and cool to 95-97 ℃, then, enter the laminar flow jar again, temperature is 95-97 ℃ in the laminar flow jar, the residence time is 80-110 minute, finishes once liquefaction;
(3) secondary liquefaction: after once liquefaction is finished, in the liquefier also residual have do not have the starch of complete hydrolysis macrobead molecule on a small quantity, also need in liquefier, to add once more the heavy efficient high-temperature resistant a-amylase of 3-4U/ grammeter this moment, with the steam heating liquefier to temperature 120-130 ℃, liquefier is once more by the pressurize jar then, the pressurize pressure tank is controlled to be 0.3-0.5MPa, temperature control is 120-130 ℃ in jar, liquefier stops after 5-7 minute in the pressurize jar, enter flash system and cool to 90-95 ℃, the starch macrobead has also obtained thorough hydrolysis like this, and final starch milk is converted into and contains dextrin, maltose, the liquefier of trisaccharide and a small amount of glucose;
(4) take off slag: liquefier is handled by filter press, sugared slag is separated with liquid glucose; The pH value of filtrate is adjusted to 4.5-4.8, the filtrate temperature is reduced to 58-60 ℃ by cooling system; Sugared slag is added water stir, pass through the washery slag filtering system then, can thoroughly reclaim the sugar in the sugared slag on the one hand, to improve yield; Carry the protein content in the high pulp on the other hand;
(5) saccharification: the liquefier through taking off the slag operation enters the saccharification operation, the sugared concentration of liquefier has reached 35-37%, amount according to 2-4U/g liquefier butt is added fungal amylase, fungal amylase is under pH value 4.5-4.8, temperature 55-60 ℃ condition, through 8-16 hour saccharification react, produce malt syrup that contains 50%-60% and the glucose syrup that contains 3%-5%;
(6) decolouring:, remove the organic impurity in the liquid glucose by twice adsorption bleaching;
(7) ion-exchange: liquid glucose passes through weak base anion-exchange resin and storng-acid cation exchange resin successively, carries out purifying;
(8) concentrate: vacuum concentration is to the syrup solid substance, and concentration is about 75%;
(9) finished product packing.
Described decolouring adopts fresh gac as sorbent material.
The present invention adopts twice high pressure spraying to adding the diastatic starch milk of a-, and under the high temperature more than 100 ℃, a-amylase plays biochemical action, the a-1 of incision starch chain, 4 glycosidic links.After pH value is transferred to OK range, the enzyme that adds total consumption 2/3, a spray temperature is raised to rapidly and generates the aqueous solution that mixes the back carbohydrate after 110 ℃, adds the enzyme of 1/3 amount again, after two spray temperature rose to 125 ℃ rapidly, the carbohydrate molecule in the hydrating solution had obtained thorough decomposition.At bleaching workshop section, secondary decolourization adds fresh gac, brings into play the powerful decolorizing ability of new charcoal and removes the small amount of impurities in the destainer one time, and once decolouring adds secondary decolourization exhausted gac and adsorbs impurity a large amount of in the sugar, thereby saves the charcoal amount of using.In ion-exchange workshop section, when the ion exchange resin exchange capacity descends, utilize hydrochloric acid and caustic soda that Zeo-karb and anionite-exchange resin are regenerated, the production cycle shortens relatively greatly, has reduced production cost.
By this process modification, solved the difficult problem that starch milk is difficult to thorough hydrolysis; When liquefier being dropped to the physics and chemistry temperature, also sugar concentration is brought up to 37% from 33%, also saved a large amount of steam for enrichment process by twice flash distillation; By once taking off the improvement of a washery slag technology of slag, not only can reclaim in the sugared slag 10% sugar, improved yield, can also carry the protein content in the high pulp, additional income; Adopt adverse current to walk twice decoloring method of charcoal, can guarantee technic index, can economize on charcoal cost etc. again.
Production technique of the present invention reaches following six technical indicators and characteristics:
1, twice enzyme-added, twice injection, twice flash distillation liquefaction not only with the thorough hydrolysis of starch, can also bring up to 37% to liquefier concentration;
2, once take off slag, a washery slag, not only can improve yield, can also improve the protein content of byproduct;
3, adverse current is walked charcoal, twice decolouring, and ton sugar is reduced to 3.5kg with the charcoal amount by original 5kg;
4, recycling-guard ion exchange process can be realized the automatic preparation of acid-base solution, and the production cycle was reduced to 48 hours by original 72 hours;
5, quadruple effect falling liquid film vacuum concentration, steam consumption, water loss are low;
6, suitable adjusting process route and processing condition can be produced different Dian Fentang (Liquid Glucose, liquid dextrin, beer syrup, oligomeric isomaltose), for example add saccharifying enzyme and can produce glucose syrup in the saccharification operation; In the saccharification operation, add the β composite alpha-amylase and can produce beer syrup; Can produce fructose etc. after the preface of handing over, adding one group of isomery post.
Embodiment
A kind of production process for starch sugar is characterized in that carrying out successively following steps:
(1) soaks, grinds rice: after raw material is cracked rice and soak certain hour in water, remove impurity, grind into starch milk, adding clear water or slag washing water adjustment concentration is 33%, regulating the starch milk pH value by edible soda ash simultaneously is 5.9-6.0, to guarantee to liquefy effect stability and produce that postorder is working properly to be carried out;
(2) once liquefaction: the starch milk after the allotment of mill rice is pressed the heavy amount of 6-8U/ grammeter and is added efficient high-temperature resistant a-amylase, stir, after eight to ten minutes, with steam starch milk being heated to 108-110 ℃ liquefies and is ejected into the pressurize jar, the pressurize pressure tank is controlled to be 0.2-0.4MPa, temperature control is 108-110 ℃ in jar, material stops after 5-7 minute in the pressurize jar, enter flash system and cool to 95-97 ℃, then, enter the laminar flow jar again, temperature is 95-97 ℃ in the laminar flow jar, the residence time is 80-110 minute, finishes once liquefaction;
(3) secondary liquefaction: after once liquefaction is finished, in the liquefier also residual have do not have the starch of complete hydrolysis macrobead molecule on a small quantity, also need in liquefier, to add once more the heavy efficient high-temperature resistant a-amylase of 3-4U/ grammeter this moment, with the steam heating liquefier to temperature 120-130 ℃, liquefier is once more by the pressurize jar then, the pressurize pressure tank is controlled to be 0.3-0.5MPa, temperature control is 120-130 ℃ in jar, liquefier stops after 5-7 minute in the pressurize jar, enter flash system and cool to 90-95 ℃, the starch macrobead has also obtained thorough hydrolysis like this, and final starch milk is converted into and contains dextrin, maltose, the liquefier of trisaccharide and a small amount of glucose;
(4) take off slag: liquefier is handled by filter press, sugared slag is separated with liquid glucose; The pH value of filtrate is adjusted to 4.5-4.8, the filtrate temperature is reduced to 58-60 ℃ by cooling system; Sugared slag is added water stir, pass through the washery slag filtering system then, can thoroughly reclaim the sugar in the sugared slag on the one hand, to improve yield; Carry the protein content in the high pulp on the other hand;
(5) saccharification: the liquefier through taking off the slag operation enters the saccharification operation, the sugared concentration of liquefier has reached 35-37%, amount according to 2-4U/g liquefier butt is added fungal amylase, fungal amylase is under pH value 4.5-4.8, temperature 55-60 ℃ condition, through 8-16 hour saccharification react, produce malt syrup that contains 50%-60% and the glucose syrup that contains 3%-5%;
(6) decolouring:, remove the organic impurity in the liquid glucose by twice adsorption bleaching;
(7) ion-exchange: liquid glucose passes through weak base anion-exchange resin and storng-acid cation exchange resin successively, carries out purifying; Utilize the adsorption of resin, remove water-soluble inorganic impurity.Zwitterion and the H+ on the anion-cation exchange resin, OH-in the liquid glucose exchange, and H+, OH-in the last and liquid glucose are combined into water, and inorganic impurity generates corresponding water and is removed.
(8) concentrate: vacuum concentration is to the syrup solid substance, and concentration is about 75%;
Finished product packing.

Claims (2)

1, a kind of production process for starch sugar is characterized in that carrying out successively following steps:
(1) soaks, grinds rice: after raw material is cracked rice and soak certain hour in water, remove impurity, grind into starch milk, adding clear water or slag washing water adjustment concentration is 33%, regulating the starch milk pH value by edible soda ash simultaneously is 5.9-6.0, to guarantee to liquefy effect stability and produce that postorder is working properly to be carried out;
(2) once liquefaction: the starch milk after the allotment of mill rice is pressed the heavy amount of 6-8U/ grammeter and is added efficient high-temperature resistant a-amylase, stir, after eight to ten minutes, with steam starch milk being heated to 108-110 ℃ liquefies and is ejected into the pressurize jar, the pressurize pressure tank is controlled to be 0.2-0.4MPa, temperature control is 108-110 ℃ in jar, material stops after 5-7 minute in the pressurize jar, enter flash system and cool to 95-97 ℃, then, enter the laminar flow jar again, temperature is 95-97 ℃ in the laminar flow jar, the residence time is 80-110 minute, finishes once liquefaction;
(3) secondary liquefaction: after once liquefaction is finished, in the liquefier also residual have do not have the starch of complete hydrolysis macrobead molecule on a small quantity, also need in liquefier, to add once more the heavy efficient high-temperature resistant a-amylase of 3-4U/ grammeter this moment, with the steam heating liquefier to temperature 120-130 ℃, liquefier is once more by the pressurize jar then, the pressurize pressure tank is controlled to be 0.3-0.5MPa, temperature control is 120-130 ℃ in jar, liquefier stops after 5-7 minute in the pressurize jar, enter flash system and cool to 90-95 ℃, the starch macrobead has also obtained thorough hydrolysis like this, and final starch milk is converted into and contains dextrin, maltose, the liquefier of trisaccharide and a small amount of glucose;
(4) take off slag: liquefier is handled by filter press, sugared slag is separated with liquid glucose; The pH value of filtrate is adjusted to 4.5-4.8, the filtrate temperature is reduced to 58-60 ℃ by cooling system; Sugared slag is added water stir, pass through the washery slag filtering system then, can thoroughly reclaim the sugar in the sugared slag on the one hand, to improve yield; Carry the protein content in the high pulp on the other hand;
(5) saccharification: the liquefier through taking off the slag operation enters the saccharification operation, the sugared concentration of liquefier has reached 35-37%, amount according to 2-4U/g liquefier butt is added fungal amylase, fungal amylase is under pH value 4.5-4.8, temperature 55-60 ℃ condition, through 8-16 hour saccharification react, produce malt syrup that contains 50%-60% and the glucose syrup that contains 3%-5%;
(6) decolouring:, remove the organic impurity in the liquid glucose by twice adsorption bleaching;
(7) ion-exchange: liquid glucose passes through weak base anion-exchange resin and storng-acid cation exchange resin successively, carries out purifying;
(8) concentrate: vacuum concentration is to the syrup solid substance, and concentration is about 75%;
(9) finished product packing.
2, production process for starch sugar according to claim 1 is characterized in that described decolouring adopts fresh gac as sorbent material.
CN2009101168583A 2009-05-25 2009-05-25 Production process for starch sugar Expired - Fee Related CN101565762B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009101168583A CN101565762B (en) 2009-05-25 2009-05-25 Production process for starch sugar

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009101168583A CN101565762B (en) 2009-05-25 2009-05-25 Production process for starch sugar

Publications (2)

Publication Number Publication Date
CN101565762A true CN101565762A (en) 2009-10-28
CN101565762B CN101565762B (en) 2011-09-28

Family

ID=41282123

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009101168583A Expired - Fee Related CN101565762B (en) 2009-05-25 2009-05-25 Production process for starch sugar

Country Status (1)

Country Link
CN (1) CN101565762B (en)

Cited By (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101886145A (en) * 2010-06-30 2010-11-17 潍坊盛泰药业有限公司 High-yield glucose production method
CN102321686A (en) * 2011-09-14 2012-01-18 中粮生物化学(安徽)股份有限公司 Processing method and application of starch raw material
CN102373254A (en) * 2010-08-12 2012-03-14 中粮生物化学(安徽)股份有限公司 Enzymolysis method of starchy material and preparation method of citric acid
CN102373239A (en) * 2010-08-12 2012-03-14 中粮生物化学(安徽)股份有限公司 Preparation method for ethanol
CN101748220B (en) * 2010-01-08 2012-06-20 西王集团有限公司 Glucose production process for reducing steam consumption
CN102743897A (en) * 2012-07-23 2012-10-24 中粮生物化学(安徽)股份有限公司 Refining method of starch sugar liquor
CN102912043A (en) * 2012-10-24 2013-02-06 安徽汇佳生物科技有限公司 Method for producing purified fructose
CN103031388A (en) * 2012-12-21 2013-04-10 菱花集团有限公司 Recycling method of liquefied waste heat during starch sugar production process
CN103060402A (en) * 2013-01-07 2013-04-24 安徽友勇生物科技有限公司 Production method of starch syrup
CN103283914A (en) * 2013-05-31 2013-09-11 安徽友勇生物科技有限公司 Preparation method of health care starch sugar
CN103695502A (en) * 2013-12-13 2014-04-02 广西丰浩糖业集团有限公司 Method for preparing sugar from yam starch
CN103898243A (en) * 2012-12-31 2014-07-02 保龄宝生物股份有限公司 Exhaust steam comprehensive utilization device in high fructose corn syrup production process
CN104862428A (en) * 2015-05-12 2015-08-26 华南理工大学 Separating device and method for enzymatic starch sugar sugar-free grains enrichment
CN105969915A (en) * 2016-06-29 2016-09-28 河北健民淀粉糖业有限公司 Glucose production technology
CN106191159A (en) * 2016-07-15 2016-12-07 双桥(湖北)有限公司 The production technology of starch syrup prepared by a kind of rice
CN106512772A (en) * 2016-11-30 2017-03-22 无锡甜丰食品有限公司 Spray atomizing and mixing method for syrup production
CN106755613A (en) * 2016-12-16 2017-05-31 广州双桥股份有限公司 A kind of purification process of starch sugar
CN107130007A (en) * 2017-06-23 2017-09-05 安徽万德生物科技有限公司 A kind of starch syrup production technology
CN107223773A (en) * 2017-06-23 2017-10-03 安徽万德生物科技有限公司 A kind of feed rice protein powder craft
CN107287262A (en) * 2017-07-25 2017-10-24 安徽万德生物科技有限公司 A kind of preparation technology of starch syrup
CN108085349A (en) * 2017-11-07 2018-05-29 双桥(厦门)有限公司 A kind of production method of corn starch sugar
CN108754036A (en) * 2018-05-26 2018-11-06 双桥(厦门)有限公司 Starch syrup purifies method for concentration
CN108967648A (en) * 2018-08-23 2018-12-11 湖南汇升生物科技有限公司 A kind of processing and treating method of the exceeded rice of cadmium
CN109439807A (en) * 2018-12-18 2019-03-08 浙江华康药业股份有限公司 A kind of xylose production process
CN110551779A (en) * 2019-09-11 2019-12-10 安徽焕发生物科技有限公司 F42 fructose processing technology
CN111218493A (en) * 2019-12-04 2020-06-02 双桥(厦门)有限公司 Production process of syrup suitable for sports functional beverage
CN111893147A (en) * 2020-07-13 2020-11-06 南通佳之味食品有限公司 Preparation method of glucose syrup with low DE value
CN114292966A (en) * 2021-12-23 2022-04-08 巴彦淖尔华恒生物科技有限公司 Separation method and application of flocculation protein in starch sugar solution

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109136302B (en) * 2018-08-23 2021-11-16 湖南汇升生物科技有限公司 Production method for controlling standard exceeding of furfural in starch sugar production

Cited By (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101748220B (en) * 2010-01-08 2012-06-20 西王集团有限公司 Glucose production process for reducing steam consumption
CN101886145A (en) * 2010-06-30 2010-11-17 潍坊盛泰药业有限公司 High-yield glucose production method
CN102373254B (en) * 2010-08-12 2013-09-25 中粮生物化学(安徽)股份有限公司 Enzymolysis method of starchy material and preparation method of citric acid
CN102373254A (en) * 2010-08-12 2012-03-14 中粮生物化学(安徽)股份有限公司 Enzymolysis method of starchy material and preparation method of citric acid
CN102373239A (en) * 2010-08-12 2012-03-14 中粮生物化学(安徽)股份有限公司 Preparation method for ethanol
CN102321686A (en) * 2011-09-14 2012-01-18 中粮生物化学(安徽)股份有限公司 Processing method and application of starch raw material
CN102743897A (en) * 2012-07-23 2012-10-24 中粮生物化学(安徽)股份有限公司 Refining method of starch sugar liquor
CN102743897B (en) * 2012-07-23 2015-06-10 中粮生物化学(安徽)股份有限公司 Refining method of starch sugar liquor
CN102912043A (en) * 2012-10-24 2013-02-06 安徽汇佳生物科技有限公司 Method for producing purified fructose
CN102912043B (en) * 2012-10-24 2014-01-15 安徽汇佳生物科技有限公司 Method for producing purified fructose
CN103031388A (en) * 2012-12-21 2013-04-10 菱花集团有限公司 Recycling method of liquefied waste heat during starch sugar production process
CN103898243A (en) * 2012-12-31 2014-07-02 保龄宝生物股份有限公司 Exhaust steam comprehensive utilization device in high fructose corn syrup production process
CN103060402A (en) * 2013-01-07 2013-04-24 安徽友勇生物科技有限公司 Production method of starch syrup
CN103283914A (en) * 2013-05-31 2013-09-11 安徽友勇生物科技有限公司 Preparation method of health care starch sugar
CN103695502B (en) * 2013-12-13 2016-06-29 广西丰浩糖业集团有限公司 A kind of Rhizoma Dioscoreae starch method for manufacturing sugar
CN103695502A (en) * 2013-12-13 2014-04-02 广西丰浩糖业集团有限公司 Method for preparing sugar from yam starch
CN104862428A (en) * 2015-05-12 2015-08-26 华南理工大学 Separating device and method for enzymatic starch sugar sugar-free grains enrichment
CN105969915A (en) * 2016-06-29 2016-09-28 河北健民淀粉糖业有限公司 Glucose production technology
CN106191159B (en) * 2016-07-15 2019-08-06 双桥(湖北)有限公司 A kind of rice prepares the production technology of starch syrup
CN106191159A (en) * 2016-07-15 2016-12-07 双桥(湖北)有限公司 The production technology of starch syrup prepared by a kind of rice
CN106512772A (en) * 2016-11-30 2017-03-22 无锡甜丰食品有限公司 Spray atomizing and mixing method for syrup production
CN106755613A (en) * 2016-12-16 2017-05-31 广州双桥股份有限公司 A kind of purification process of starch sugar
CN107130007A (en) * 2017-06-23 2017-09-05 安徽万德生物科技有限公司 A kind of starch syrup production technology
CN107223773A (en) * 2017-06-23 2017-10-03 安徽万德生物科技有限公司 A kind of feed rice protein powder craft
CN107287262A (en) * 2017-07-25 2017-10-24 安徽万德生物科技有限公司 A kind of preparation technology of starch syrup
CN108085349A (en) * 2017-11-07 2018-05-29 双桥(厦门)有限公司 A kind of production method of corn starch sugar
CN108754036A (en) * 2018-05-26 2018-11-06 双桥(厦门)有限公司 Starch syrup purifies method for concentration
CN108967648A (en) * 2018-08-23 2018-12-11 湖南汇升生物科技有限公司 A kind of processing and treating method of the exceeded rice of cadmium
CN109439807A (en) * 2018-12-18 2019-03-08 浙江华康药业股份有限公司 A kind of xylose production process
CN110551779A (en) * 2019-09-11 2019-12-10 安徽焕发生物科技有限公司 F42 fructose processing technology
CN111218493A (en) * 2019-12-04 2020-06-02 双桥(厦门)有限公司 Production process of syrup suitable for sports functional beverage
CN111893147A (en) * 2020-07-13 2020-11-06 南通佳之味食品有限公司 Preparation method of glucose syrup with low DE value
CN114292966A (en) * 2021-12-23 2022-04-08 巴彦淖尔华恒生物科技有限公司 Separation method and application of flocculation protein in starch sugar solution

Also Published As

Publication number Publication date
CN101565762B (en) 2011-09-28

Similar Documents

Publication Publication Date Title
CN101565762B (en) Production process for starch sugar
CN103060402A (en) Production method of starch syrup
CN102912043B (en) Method for producing purified fructose
EP1737550B1 (en) Recovery of inorganic salt during processing of lignocellulosic feedstocks
CN102337316B (en) Process for producing starch sugar
CN109503676B (en) Method for preparing xylitol and mixed syrup from xylose mother liquor
CN100422347C (en) Crystalline glucose producing process based on whole membrane method
JP2008506370A (en) Method for obtaining a sugar product stream from cellulosic biomass
CN107130007A (en) A kind of starch syrup production technology
CN105821095A (en) Optimization method for crystallization of glucose
CN101724669A (en) Method for producing moderately inverted syrup by synergistic saccharification with multiple enzymes
JP7454103B2 (en) System and method for simultaneous production of erythritol and liquid sorbitol using corn starch
CN101628922B (en) Oligosaccharide ferulic acid ester preparation method
CN101125892A (en) Method for producing aminoglucose hydrochloride
CN101831477A (en) Method for preparing rice into glucose for injection
CN213475846U (en) Xylitol mother liquor utilizes system
CN102102116B (en) Method for preparing high-purity crystalline dextrose from maize peel acid hydrolysis residues
CN102382911A (en) Method for preparing crystalline xylose by using bagasse pith as raw material
CN105482933B (en) A kind of preparation method of high-attenuation degree beer syrup
CN108774273B (en) Trehalose crystallization process
CN100534996C (en) Preparation of dulcose crystal
CN108822305B (en) Method for extracting gutta-percha from eucommia bark based on imidazole ionic liquid pretreatment
CN101979640B (en) Method for producing xylooligosaccharide by using sugarcane leaves
CN107840782A (en) The production method and device of sorbierite
CN113135965A (en) System and method for producing crystalline xylose by using xylose mother liquor

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Wang Yinsheng

Inventor after: Liu Tao

Inventor after: Zhu Geng

Inventor before: Liu Gang

Inventor before: Li Yuqiang

Inventor before: Deng Zhongbing

Inventor before: Xie Hu

Inventor before: Wang Yinsheng

Inventor before: Peng Shaochun

Inventor before: He Cunxian

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20170728

Address after: 237200 Lu'an Mount Holyoke Economic Development Zone, Anhui

Patentee after: Anhui Mount Holyoke food source Biological Technology Co., Ltd.

Address before: 237200 Mount Holyoke Economic Development Zone, Anhui Province

Patentee before: Anhui United Well Technology Limited

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110928

Termination date: 20180525