CN101548940A - Method for preparing beauty mask containing active compound of pilose antler and traditional Chinese medicine composition - Google Patents
Method for preparing beauty mask containing active compound of pilose antler and traditional Chinese medicine composition Download PDFInfo
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- CN101548940A CN101548940A CNA200910072004XA CN200910072004A CN101548940A CN 101548940 A CN101548940 A CN 101548940A CN A200910072004X A CNA200910072004X A CN A200910072004XA CN 200910072004 A CN200910072004 A CN 200910072004A CN 101548940 A CN101548940 A CN 101548940A
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- active compound
- pilose antler
- chinese medicine
- medicine composition
- beauty mask
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Abstract
A method for preparing beauty mask containing active compound of pilose antler and traditional Chinese medicine composition relates to a method for extracting active compound of pilose antler and a method for preparing beauty mask. The invention settles the problems of low extraction rate, low activity and tedious production process when a prior traditional method is used for extracting active compound of pilose antler. The method for preparing beauty mask containing active compound of pilose antler comprises the following steps: selecting fresh two-branched antler of cervus elaphus, selecting a one-third part at the front end, crushing the pilose antler of cervus elaphus with liquid nitrogen through a mixing-bead milling method, extracting through highfield, separating the raffinate with a low-temperature ultracentrifuge, eliminating the lipid matter, condensing with a vacuum blade type film, mixing the concentrated solution of active compound of pilose antler, Auricularia Auricular polysaccharide, ginseing extract, angelia extract and Bletilla striata extract, milling with a colloid mill and homogenizing for preparing the beauty mask containing the active compound of pilose antler. The beauty mask containing active compound of pilose antler and traditional Chinese medicine composition, which is prepared according to the invention, has no side effect for human body, has the functions of beautifying and face nursing, and can be applied for the fields of beautifying, cosmetic manufacturing, etc.
Description
Technical field
The present invention relates to a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask.
Background technology
Active compound of pilose antler such as polysaccharide, polypeptide, polyamines, insulin-like active factors isoreactivity composition, its major function is to promote cell differentiation, propagation and survival, stimulate the synthetic and cell proliferation of RNA, DNA, particularly in mitosis important meaning such as cell cycle cycle C0-G1 and G1-Gs stages.Muscle power, energy, endurance, appearance to the people reach to the huge improvement of the whole generation of life.The growth promoter and the metabolism of scalable endocrine, enhancing human body immunity, promotion body have defying age, looks improving and the skin nourishing, protect the liver kidney and the sexual function improvement effect of supporting.
Active compound of pilose antler can be widely used in food, medicine, health product, Cosmetic Manufacture at present, is the worldwide anti-aging product of fashionable America and Europe, Japan and Korea S., and its market prospect is boundless.Though it is at present a lot of to the research of active compound of pilose antler, but the extracting method of active compound of pilose antler is mainly based on supercritical ultrasonics technology and reflux extraction method, with producing a large amount of free radicals in the supercritical ultrasonics technology extraction active compound of pilose antler process, destroy the active compound of pilose antler physiologically active, and the reflux extraction method is a kind of high temperature abstraction technique, can make active compound of pilose antler lose physiological function equally, and the extraction ratio of two kinds of methods have only the bright sample Cornu Cervi Pantotrichum of 3.0～5.0 μ g/g.This invention proposition highfield extraction active compound of pilose antler reaches the preparation method with the Chinese medicine composition beauty mask, has well kept activity, has good cosmetic result, can be applicable to fields such as beauty treatment, cosmetics.
Summary of the invention
Low in order to solve the active compound of pilose antler extraction ratio, the problem that activity is not high and utilization rate is low, the invention provides a kind of highfield legal system be equipped with active compound of pilose antler method and with the preparation method of Chinese medicine composition beauty mask, can effectively improve the extraction ratio and the product activity of active compound of pilose antler.Among the present invention, a kind of step of the preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask is as follows: one, the extraction of active compound of pilose antler: carry out the screening of cervus elaphus linnaeus earlier, choose the fresh two thick stick young pilose antlers of Cervus elaphus linnaeus, choose tip 1/3rd places, with liquid nitrogen and agitation beads polishing cervus elaphus linnaeus is ground into powder, be that to add Pilose Antler and concentration respectively be 60% ethanol for the ratio of 1g: 5mL～1g: 10mL with the solid-liquid ratio, with highfield extraction 25～35 minutes, obtain containing the active compound of pilose antler extract, use refrigerated centrifuge with the centrifugal 7～10min of the speed of 3500～4000r/rnin at last, get the upper strata extracting solution, the ratio that with the solid-liquid ratio is 1g: 5mL～1g: 10mL again is that 60% ethanol joins and proceeds highfield extraction and centrifugalize in the lower sediment with concentration, extract 3 times continuously, remove lower sediment, merge the upper strata extracting solution; Two, concentrate: the active compound of pilose antler extracting solution is adopted vacuum scraper-type thin film concentration, and concentrated condition is 35～45 ℃ of temperature, and vacuum is 0.1～0.15mbar, obtains the active compound of pilose antler concentrated solution; Three, preparation: Cornu Cervi Pantotrichum concentrated solution and Auricularia polycose, Chinese medicine extract are prepared in following ratio, Cornu Cervi Pantotrichum concentrate: Auricularia polycose: Pseudobulbus Bletillae (Rhizoma Bletillae) extract: Radix Ginseng extract: Radix Angelicae Dahuricae extract: distilled water=1: 30: 15: in blend tank stir 30 minute, contain Cornu Cervi Pantotrichum, Chinese medicine composition at 15: 15: 45..Four, colloidal grinding:, must contain active compound of pilose antler and Chinese medicine composition beauty mask with compositions colloid mill circular grinding 3 times.
Among the present invention, in the preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask, adopt the ultralow temperature agitation beads to grind highfield economic benefits and social benefits extraction active compound of pilose antler technology, handle cooperation agitation beads Ginding process with nitrogen ultra low temperature cervus elaphus linnaeus is carried out micronizing, then by the highfield auxiliary extraction, make active compound of pilose antler be able to abundant release, make the extraction ratio of active compound of pilose antler can reach 70～80%, than the extraction ratio of ultrasonic extraction or solvent refluxing extraction method high respectively 40～60% and 70～90%.Its specific activity extraction method ultrasonic extraction or solvent refluxing extraction method height 50～80%, improved active compound of pilose antler cosmetic activity and added economic value greatly by Cornu Cervi Pantotrichum extract and Chinese medicine composition.Technology of the present invention is simple, extraction ratio height, suitable promotion and application.The active compound of pilose antler of the present invention's preparation is active high, is applied to fields such as beauty treatment, cosmetics manufacturing.
The specific embodiment
The specific embodiment one: in this specific embodiment, a kind of step of the preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask is as follows: one, the extraction of active compound of pilose antler: carry out the screening of cervus elaphus linnaeus earlier, choose the fresh two thick stick young pilose antlers of Cervus elaphus linnaeus, choose tip 1/3rd places, with liquid nitrogen and agitation beads polishing cervus elaphus linnaeus is ground into powder, be that to add Pilose Antler and concentration respectively be 60% ethanol for the ratio of 1g: 5mL～1g: 10mL with the solid-liquid ratio, with highfield extraction 25～35 minutes, obtain containing the active compound of pilose antler extract, use refrigerated centrifuge with the centrifugal 7～10min of the speed of 3500～4000r/min at last, get the upper strata extracting solution, the ratio that with the solid-liquid ratio is 1g: 5mL～1g: 10mL again is that 60% ethanol joins and proceeds highfield extraction and centrifugalize in the lower sediment with concentration, extract 3 times continuously, remove lower sediment, merge the upper strata extracting solution; Two, concentrate: the active compound of pilose antler extracting solution is adopted vacuum scraper-type thin film concentration, and concentrated condition is 35～45 ℃ of temperature, and vacuum is 0.1～0.15mbar, obtains the active compound of pilose antler concentrated solution; Three, preparation: Cornu Cervi Pantotrichum concentrated solution and Auricularia polycose, Chinese medicine extract are prepared in following ratio, Cornu Cervi Pantotrichum concentrate: Auricularia polycose: Pseudobulbus Bletillae (Rhizoma Bletillae) extract: Radix Ginseng extract: Radix Angelicae Dahuricae extract: distilled water=1: 30: 15: in blend tank stir 30 minute, contain Cornu Cervi Pantotrichum, Chinese medicine composition at 15: 15: 45..Four, colloidal grinding:, must contain active compound of pilose antler and Chinese medicine composition beauty mask with compositions colloid mill circular grinding 3 times.
The specific embodiment two: what this specific embodiment and the specific embodiment one were different is: cervus elaphus linnaeus is broken in the step 1 is ground into 40 order powder with liquid nitrogen and agitation beads polishing with cervus elaphus linnaeus, stirring revolution is that per minute 40～50 changes, and the grinding bead useful load is for grinding 30～40% of storehouse.Other is identical with the specific embodiment one.
The specific embodiment three: what this specific embodiment and the specific embodiment one were different is: highfield intensity is 50～100 kilovolts every square centimeter in the step 1, high voltage electric field strokes per minute 400～500 times, pulse frequency 200～300Hz.Other is identical with the specific embodiment one.
The specific embodiment four: what this specific embodiment and the specific embodiment one were different is: in the step 2 in the concentrated solution solid content be 50%～80%.Other is identical with the specific embodiment one.
The specific embodiment five: what this specific embodiment and the specific embodiment one were different is: Pseudobulbus Bletillae (Rhizoma Bletillae) extract concentrations is 5g/mL (containing Pseudobulbus Bletillae (Rhizoma Bletillae) crude drug 5 grams in every milliliter) in the step 3, and Radix Ginseng extract concentration is 7g/mL, and Radix Angelicae Dahuricae extract concentration is 7g/mL.
The extraction ratio of active compound of pilose antler is 70～80% in this specific embodiment, and gained contains active compound of pilose antler and Chinese medicine composition beauty mask activity is high, cosmetic result is good.
Claims (5)
1, a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask, the preparation method step that it is characterized in that containing active compound of pilose antler and Chinese medicine composition beauty mask is as follows: one, the extraction of active compound of pilose antler: carry out the screening of cervus elaphus linnaeus earlier, choose the fresh two thick stick young pilose antlers of Cervus elaphus linnaeus, choose tip 1/3rd places, with liquid nitrogen and agitation beads polishing cervus elaphus linnaeus is ground into powder, be that to add Pilose Antler and concentration respectively be 60% ethanol for the ratio of 1g: 5mL～1g: 10mL with the solid-liquid ratio, with highfield extraction 25～35 minutes, obtain containing the active compound of pilose antler extract, use refrigerated centrifuge with the centrifugal 7～10min of the speed of 3500～4000r/min at last, get the upper strata extracting solution, the ratio that with the solid-liquid ratio is 1g: 5mL～1g: 10mL again is that 60% ethanol joins and proceeds highfield extraction and centrifugalize in the lower sediment with concentration, extract 3 times continuously, remove lower sediment, merge the upper strata extracting solution; Two, concentrate: the active compound of pilose antler extracting solution is adopted vacuum scraper-type thin film concentration, and concentrated condition is 35～45 ℃ of temperature, and vacuum is 0.1～0.15mbar, obtains the active compound of pilose antler concentrated solution; Three, preparation: Cornu Cervi Pantotrichum concentrated solution and Auricularia polycose, Chinese medicine extract are prepared in following ratio, Cornu Cervi Pantotrichum concentrate: Auricularia polycose: Pseudobulbus Bletillae (Rhizoma Bletillae) extract: Radix Ginseng extract: Radix Angelicae Dahuricae extract: distilled water=1: 30: 15: in blend tank stir 30 minute, contain Cornu Cervi Pantotrichum, Chinese medicine composition at 15: 15: 45..Four, colloidal grinding:, must contain active compound of pilose antler and Chinese medicine composition beauty mask with compositions colloid mill circular grinding 3 times.
2, a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask according to claim 1, it is characterized in that the Cornu Cervi Pantotrichum fragmentation is ground into 40 order powder with liquid nitrogen and agitation beads polishing with cervus elaphus linnaeus in the step 1, stirring revolution is that per minute 40～50 changes, and the grinding bead useful load is for grinding 30～40% of storehouse.
3, a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask according to claim 1, it is characterized in that highfield intensity is 50～100 kilovolts every square centimeter in the step 1, high voltage electric field strokes per minute 400～500 times, pulse frequency 200～300Hz.
4, a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask according to claim 1 is characterized in that in the step 2 that solid content is 50%～80% in the concentrated solution.
5, a kind of preparation method that contains active compound of pilose antler and Chinese medicine composition beauty mask according to claim 1 is characterized in that Pseudobulbus Bletillae (Rhizoma Bletillae) extract concentrations is 5g/mL (containing Pseudobulbus Bletillae (Rhizoma Bletillae) crude drug 5 grams in every milliliter) in the step 3, Radix Ginseng extract concentration is 7g/mL, and Radix Angelicae Dahuricae extract concentration is 7g/mL.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA200910072004XA CN101548940A (en) | 2009-05-12 | 2009-05-12 | Method for preparing beauty mask containing active compound of pilose antler and traditional Chinese medicine composition |
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| CNA200910072004XA CN101548940A (en) | 2009-05-12 | 2009-05-12 | Method for preparing beauty mask containing active compound of pilose antler and traditional Chinese medicine composition |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101822698A (en) * | 2010-05-21 | 2010-09-08 | 王振宇 | Method for preparing black fungus and pantotrichum hypoglycemic composition |
| CN103110534A (en) * | 2013-01-29 | 2013-05-22 | 海南巨鹿堂保健美容品有限公司 | Combined essence of composite velvet antler polypeptide lyophilized powder and nano-scale buffering microemulsion for skin beauty and health care and preparation method of combined essence |
| CN106420564A (en) * | 2016-10-31 | 2017-02-22 | 江苏煌上田投资有限公司 | Cornu cervi pantotrichum external restoration composition |
-
2009
- 2009-05-12 CN CNA200910072004XA patent/CN101548940A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101822698A (en) * | 2010-05-21 | 2010-09-08 | 王振宇 | Method for preparing black fungus and pantotrichum hypoglycemic composition |
| CN103110534A (en) * | 2013-01-29 | 2013-05-22 | 海南巨鹿堂保健美容品有限公司 | Combined essence of composite velvet antler polypeptide lyophilized powder and nano-scale buffering microemulsion for skin beauty and health care and preparation method of combined essence |
| CN103110534B (en) * | 2013-01-29 | 2014-10-22 | 海南巨鹿堂保健美容品有限公司 | Combined essence of composite velvet antler polypeptide lyophilized powder and nano-scale buffering microemulsion for skin beauty and health care and preparation method of combined essence |
| CN106420564A (en) * | 2016-10-31 | 2017-02-22 | 江苏煌上田投资有限公司 | Cornu cervi pantotrichum external restoration composition |
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Application publication date: 20091007 |