CN101514299B - Compound diesel - Google Patents
Compound diesel Download PDFInfo
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- CN101514299B CN101514299B CN 200910014639 CN200910014639A CN101514299B CN 101514299 B CN101514299 B CN 101514299B CN 200910014639 CN200910014639 CN 200910014639 CN 200910014639 A CN200910014639 A CN 200910014639A CN 101514299 B CN101514299 B CN 101514299B
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Abstract
The invention discloses a compound diesel, composed of the following raw materials: 15-20 parts of water, 8-12 parts of methanol, 30-35 parts of diesel, 9-12 parts of oleic acid, 21-28 parts of solvent oil, 4-7 parts of No.1 additives and 0.5-1.5 parts of No.2 additives by weight. The invention overcomes the defects that the prior emulsified diesel fuel has non-transparent milky color, and the prior methanol diesel and emulsified diesel can not be mixed with pure diesel and has insufficient dynamic property and terrible odor and has the advantages of good use effects, low cost, energy saving and environmental protection, etc.
Description
Technical field
The present invention relates to a kind of compound diesel.
Background technology
As everyone knows, diesel oil is one of most important Nonrenewable energy resources, because it is non-renewable, along with the development of society, the diesel oil resource sharply reduces, and seeks the substitute of diesel oil or prepares the effective measure that economical and practical diesel fuel complex additive is the alleviation problem.
There are multiple diesel fuel complex additive, compound diesel etc. in the prior art, but more or less all have following shortcoming: 1, can not mix with pure diesel oil use; 2, be short of power; 3, bad 4, the high expensive of smell.
Summary of the invention
For above-mentioned prior art, for solving the problem of diesel oil resource worsening shortages, consider from economy, result of use etc. are many-sided, the invention provides a kind of energy-conserving and environment-protective, stable practical compound diesel.
The present invention is achieved by the following technical solutions:
A kind of compound diesel is comprised of following raw material, and the parts by weight of each raw material are: water 15-20 part, methyl alcohol 8-12 part, diesel oil 30-35 part, oleic acid 9-12 part, solvent oil 21-28 part, an additive 4-7 part, No. two additive 0.5-1.5 parts.
Described solvent oil is No. 200 solvent oils.
A described additive is comprised of the raw material of following parts by weight: polyoxyethylene octylphenol ether 3.5-7 part, polyoxyethylene nonylphenol ether 2.6-4 part, hexahydroaniline 3-6 part, many thanomins 1.7-3 part, straight chain alcohol 20-27 part, branched-chain alcoho 30-38 part, sodium hydroxide 13-20 part, isooctyl ester nitrate 2-4 part, ferrocene 0.5-1 part, 1 part of 2,6 ditertiary butyl p cresol, 0.5 part of benzotriazole.
Described many thanomins are a kind of several combinations in thanomin, diethanolamine, the trolamine.
Described straight chain alcohol is a kind of or several combination in propyl carbinol, nonylcarbinol, the n-Octanol.
Described branched-chain alcoho is a kind of or several combination in isooctyl alcohol, Virahol, the primary isoamyl alcohol.
Described No. two additives are comprised of the raw material of following parts by weight: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
A kind of preparation method of compound diesel is characterized in that, step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, many thanomins, straight chain alcohol, branched-chain alcoho, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 30～60 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 10～30 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, solvent oil mix with an additive, stir 60～120 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Compound diesel of the present invention has following excellent properties:
1, true to nature: outward appearance is as diesel oil, and is limpid transparent, haze-free, and (complete the sort of oyster white without oil in water emulsion of the prior art), the user easily accepts.
2, refuse water: after the ratio of water in the compound diesel after the configuration is fixed (emulsification is fused), add again water and can not add, only can be sunken to the oil in water emulsion bottom.
3, stable: unchanged, not stratified, can satisfy user's needs fully.
4, dissolve each other: these characteristics are most important factors that can diesel oil emulsification be promoted on a large scale, if can not dissolve each other, popularization is impossible.Compound diesel of the present invention can mix with pure diesel oil arbitrarily, and does not affect result of use, never degenerates, and greatly is user-friendly to and production and sales etc.
5, practicality: energy-conservation more than 10～20%, tail gas clean-up rate 30%, cost is low, produces and need not special-purpose specific installation, and the golden eggs space is arranged.
Contain multiple catalytically active material in the compound diesel of the present invention, metal ion not has the usefulness of multiple excellence:
One, this oil product has stabilization;
Two, this oil product has the effect of not stratified, not degreasing, not emulsification;
Three, this oil product makes combustion flame obviously brighten, shorten, can realize abundant burning by optimizing the oil plant carbon-chain structure;
Four, this oil product is guaranteed the original normal compression of power without carbon deposit, reduces oil consumption;
Five, the condensation point of this oil product is low, and good fluidity can be realized abundant atomizing, makes burning more abundant;
Six, this oil product has the decomposition combustion aid function: compound diesel of the present invention contains certain hydroxide material, under the combustion high temperature condition, especially in the combustion chamber of power through high temperature and catalysis, can decompose hydrogen and oxygen, they are active atom and the free radicals that can participate in burning, can promote burning and make fuel discharge larger heat energy.
The present inventor is through concentrating on studies for many years, carries out various tests and batch production is on probation, invented this " water-in-oil " type environment-friendly energy-saving diesel fuel, and through evidence, it has following multiple effect:
1, cracking energization effect; Water is comprised of hydrogen-oxygen, can cracking go out the hydrogen participation burning higher 3.5 times than diesel oil energy under the high-temperature.
2, energy-conservation for oxygen effect: the oxygen of cracking is combustion-supporting for burning has increased the oxygen adding, makes its burning more abundant, and is more energy-conservation.
3, effect of micro-explosion: during water vapor, can break through oil film when producing the steam than self large 1700 times of volume, oil be atomized once again, thereby more fully burn.
4, water-gas effect: water vapour is converted to CO with the CO that fails to burn
2And a large amount of heat releases.
5, environmental protection effect: emulsifying combustion can reduce the fume emission degree more than 62%.
Compound diesel of the present invention can be all carries out operation in the higher Sealing Arrangement of level of automation and pipeline, do not have the discharging of " three wastes " such as waste gas, waste water, waste residues in the whole technical process, and is minimum to surrounding environment influence.
The used raw material sources of the present invention are extensive, and cost is low: diesel oil itself can be bought everywhere, and water can be gathered materials on the spot, methyl alcohol, the local procurement of chemical industry auxiliary material.Principle is easily purchased preparation, and price is clear and definite, and wherein the diesel oil wholesale price is clear, and water price is clear, and economic benefit is very clear.
The present invention has overcome the opaque milky defective of color of former diesel oil emulsification, overcome the defective that former methanol diesel-oil, diesel oil emulsification can not mix with pure diesel oil, methanol diesel-oil before having overcome, the shortcoming of diesel oil emulsification dynamic property deficiency have overcome methanol diesel-oil, the bad defective of diesel oil emulsification smell.The present invention has that result of use is good, the advantages such as cost is low, energy-conserving and environment-protective.
Embodiment
Embodiment 1: prepare a kind of compound diesel
Prescription is: 20 parts in water, 10 parts of methyl alcohol, 32 parts of diesel oil, 9 parts of oleic acid, 21 parts of 200# solvent oils, 7 parts of additives, 1 part of No. two additive.
Wherein, the prescription of an additive is: 7 parts of polyoxyethylene octylphenol ethers, 4 parts of polyoxyethylene nonylphenol ethers, 4 parts of hexahydroaniline, 3 parts of thanomins, 27 parts of n-Octanols, 38 parts of isooctyl alcohol, 13 parts in sodium hydroxide, 2 parts of isooctyl ester nitrates, 0.5 part of ferrocene, 2,1 part of 6-ditertbutylparacresol, 0.5 part of benzotriazole.
The prescription of No. two additives is: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
Step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, thanomin, n-Octanol, isooctyl alcohol, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 30 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 30 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, 200# solvent oil mix with an additive, stir 120 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Embodiment 2: prepare a kind of compound diesel
Prescription is: 20 parts in water, 10 parts of methyl alcohol, 32 parts of diesel oil, 9 parts of oleic acid, 21 parts of 200# solvent oils, 7 parts of additives, 1 part of No. two additive.
Wherein, the prescription of an additive is: 7 parts of polyoxyethylene octylphenol ethers, 4 parts of polyoxyethylene nonylphenol ethers, 4 parts of hexahydroaniline, 3 parts of thanomins, 27 parts of propyl carbinols, 38 parts of Virahols, 13 parts in sodium hydroxide, 2 parts of isooctyl ester nitrates, 0.5 part of ferrocene, 2,1 part of 6-ditertbutylparacresol, 0.5 part of benzotriazole.
The prescription of No. two additives is: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
Step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, thanomin, propyl carbinol, Virahol, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 60 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 10 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, 200# solvent oil mix with an additive, stir 60 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Embodiment 3: prepare a kind of compound diesel
Prescription is: 20 parts in water, 10 parts of methyl alcohol, 32 parts of diesel oil, 9 parts of oleic acid, 21 parts of 200# solvent oils, 7 parts of additives, 1 part of No. two additive.
Wherein, the prescription of an additive is: 7 parts of polyoxyethylene octylphenol ethers, 4 parts of polyoxyethylene nonylphenol ethers, 4 parts of hexahydroaniline, 3 parts of trolamines, 27 parts of positive certain herbaceous plants with big flowers alcohol, 38 parts of primary isoamyl alcohol, 13 parts in sodium hydroxide, 2 parts of isooctyl ester nitrates, 0.5 part of ferrocene, 2,1 part of 6-ditertbutylparacresol, 0.5 part of benzotriazole.
The prescription of No. two additives is: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
Step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, trolamine, positive certain herbaceous plants with big flowers alcohol, primary isoamyl alcohol, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 45 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 20 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, 200# solvent oil mix with an additive, stir 90 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Embodiment 4: prepare a kind of compound diesel
Prescription is: 15 parts in water, 12 parts of methyl alcohol, 30 parts of diesel oil, 12 parts of oleic acid, 28 parts of 200# solvent oils, 6 parts of additives, 0.5 part of No. two additive.
Wherein, the prescription of an additive is: 3.5 parts of polyoxyethylene octylphenol ethers, 2.6 parts of polyoxyethylene nonylphenol ethers, 6 parts of hexahydroaniline, 1.7 parts of trolamines, 20 parts of positive certain herbaceous plants with big flowers alcohol, 30 parts of primary isoamyl alcohol, 20 parts in sodium hydroxide, 4 parts of isooctyl ester nitrates, 1 part of ferrocene, 2,1 part of 6-ditertbutylparacresol, 0.5 part of benzotriazole.
The prescription of No. two additives is: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
Step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, trolamine, positive certain herbaceous plants with big flowers alcohol, primary isoamyl alcohol, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 45 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 20 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, 200# solvent oil mix with an additive, stir 90 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Embodiment 5: prepare a kind of compound diesel
Prescription is: 18 parts in water, 8 parts of methyl alcohol, 35 parts of diesel oil, 10 parts of oleic acid, 25 parts of 200# solvent oils, 4 parts of additives, 1.5 parts of No. two additives.
Wherein, the prescription of an additive is: 5 parts of polyoxyethylene octylphenol ethers, 3.5 parts of polyoxyethylene nonylphenol ethers, 3 parts of hexahydroaniline, 2.4 parts of trolamines, 24 parts of positive certain herbaceous plants with big flowers alcohol, 34 parts of primary isoamyl alcohol, 17 parts in sodium hydroxide, 3 parts of isooctyl ester nitrates, 0.7 part of ferrocene, 2,1 part of 6-ditertbutylparacresol, 0.5 part of benzo three ammonia azoles.
The prescription of No. two additives is: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
Step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, trolamine, positive certain herbaceous plants with big flowers alcohol, primary isoamyl alcohol, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 45 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 20 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, 200# solvent oil mix with an additive, stir 90 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
Claims (5)
1. compound diesel, it is characterized in that: be to be prepared from by following raw material, the parts by weight of each raw material are: water 15-20 part, methyl alcohol 8-12 part, diesel oil 30-35 part, oleic acid 9-12 part, solvent oil 21-28 part, an additive 4-7 part, No. two additive 05-1.5 parts;
A described additive is that the raw material by following parts by weight is prepared from: polyoxyethylene octylphenol ether 3.5-7 part, polyoxyethylene nonylphenol ether 2.6-4 part, hexahydroaniline 3-6 part, many thanomins 1.7-3 part, straight chain alcohol 20-27 part, branched-chain alcoho 30-38 part, sodium hydroxide 13-20 part, isooctyl ester nitrate 2-4 part, ferrocene 0.5-1 part, 1 part of 2,6 ditertiary butyl p cresol, 0.5 part of benzotriazole;
Described many thanomins are a kind of or several combinations in diethanolamine, the trolamine;
Described No. two additives are that the raw material by following parts by weight is prepared from: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates;
Prepare by following preparation method:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, many thanomins, straight chain alcohol, branched-chain alcoho, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 30～60 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 10～30 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, solvent oil mix with an additive, stir 60～120 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel.
2. a kind of compound diesel according to claim 1, it is characterized in that: described solvent oil is No. 200 solvent oils.
3. a kind of compound diesel according to claim 1 is characterized in that: described straight chain alcohol is a kind of in propyl carbinol, nonylcarbinol, the n-Octanol or appoints several combinations.
4. a kind of compound diesel according to claim 1 is characterized in that: described branched-chain alcoho is a kind of in isooctyl alcohol, Virahol, the primary isoamyl alcohol or appoints several combinations.
5. the preparation method of a kind of compound diesel claimed in claim 1 is characterized in that, step is as follows:
(1) additive of preparation: get polyoxyethylene octylphenol ether, polyoxyethylene nonylphenol ether, hexahydroaniline, many thanomins, straight chain alcohol, branched-chain alcoho, sodium hydroxide, isooctyl ester nitrate, ferrocene, 2,6-ditertbutylparacresol and benzotriazole, mix, stir and got final product in 30～60 minutes;
(2) No. two additives of preparation: get hexahydroaniline, butylacetate and methylcarbonate, mix, stir and got final product in 10～30 minutes;
(3) water intaking, methyl alcohol, diesel oil, oleic acid, solvent oil mix with an additive, stir 60～120 minutes, and be limpid bright to color, adds additive No. two again, continues to stir 20 minutes, namely gets compound diesel;
The parts by weight of described each raw material are: water 15-20 part, methyl alcohol 8-12 part, diesel oil 30-35 part, oleic acid 9-12 part, solvent oil 21-28 part, an additive 4-7 part, No. two additive 05-1.5 parts;
A described additive is that the raw material by following parts by weight is prepared from: polyoxyethylene octylphenol ether 3.5-7 part, polyoxyethylene nonylphenol ether 2.6-4 part, hexahydroaniline 3-6 part, many thanomins 1.7-3 part, straight chain alcohol 20-27 part, branched-chain alcoho 30-38 part, sodium hydroxide 13-20 part, isooctyl ester nitrate 2-4 part, ferrocene 0.5-1 part, 1 part of 2,6 ditertiary butyl p cresol, 0.5 part of benzotriazole;
Described many thanomins are a kind of or several combinations in diethanolamine, the trolamine;
Described No. two additives are that the raw material by following parts by weight is prepared from: 30 parts of hexahydroaniline, 50 parts of butylacetates, 20 parts of methylcarbonates.
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| CN 200910014639 CN101514299B (en) | 2009-03-03 | 2009-03-03 | Compound diesel |
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| CN 200910014639 CN101514299B (en) | 2009-03-03 | 2009-03-03 | Compound diesel |
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| CN101514299B true CN101514299B (en) | 2013-01-09 |
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Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101768478B (en) * | 2010-03-05 | 2013-02-06 | 北京雄韬伟业能源科技发展有限公司 | Vehicle low-carbon biodiesel |
| CN102181312B (en) * | 2011-03-29 | 2013-06-05 | 汪青 | Microemulsion diesel oil and preparation method thereof |
| CN102504890A (en) * | 2011-11-08 | 2012-06-20 | 焦作市新生生物化工有限公司 | Composite methanol diesel and preparation method thereof |
| CN102517101B (en) * | 2011-12-23 | 2014-05-14 | 江苏玖尚燃油发展有限公司 | Automobile methanol diesel fuel and preparation method thereof |
| CN102585942B (en) * | 2012-03-19 | 2014-04-30 | 王少军 | Concentration emulsified diesel fuel and preparation method thereof |
| CN102643692B (en) * | 2012-05-08 | 2014-04-16 | 刘少君 | Concentrated emulsified diesel fuel and preparation method thereof |
| CN102703144B (en) * | 2012-06-29 | 2014-03-05 | 从德强 | Diesel ester and preparation method thereof |
| CN102876397A (en) * | 2012-10-26 | 2013-01-16 | 滕春合 | Nano composite diesel oil and preparation method thereof |
| CN103911182B (en) * | 2013-01-09 | 2016-05-18 | 刘粤荣 | Biofuel oil of a kind of polynary formula combination and preparation method thereof |
| CN103911183B (en) * | 2013-01-09 | 2016-02-03 | 刘粤荣 | Biofuel of a kind of polynary formula combination and preparation method thereof |
| CN103074129A (en) * | 2013-01-25 | 2013-05-01 | 西北师范大学 | Preparation method of methanol microemulsion diesel oil |
| CN103305293A (en) * | 2013-07-08 | 2013-09-18 | 太原理工大学 | F-T diesel methanol mixed fuel and preparation method thereof |
| CN103937570B (en) * | 2014-04-24 | 2017-05-31 | 朱文雷 | The processing method of new mixed diesel |
| CN105838456A (en) * | 2015-01-13 | 2016-08-10 | 赵惠霖 | High-cleanness diesel and preparation method thereof |
| CN104650998A (en) * | 2015-02-05 | 2015-05-27 | 刘杰 | Alcohol ether diesel oil and preparation method thereof |
| CN106520225A (en) * | 2016-12-20 | 2017-03-22 | 墨宝股份有限公司 | Novel fuel with energy saving and emission reducing effects and preparation method thereof |
| CN110747024A (en) * | 2019-12-02 | 2020-02-04 | 重庆正涛新能源科技有限公司 | Micro-emulsified diesel oil and preparation method thereof |
| CN111793511A (en) * | 2020-07-14 | 2020-10-20 | 张建国 | Environment-friendly mixed biodiesel |
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| CN1888029A (en) * | 2006-07-24 | 2007-01-03 | 韩福生 | Clean environment protection synthetic diesel oil |
| CN1928033A (en) * | 2006-10-13 | 2007-03-14 | 北京中天醇能源技术有限公司 | Methanol modifier and application thereof |
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