CN101497849B - Transparent perfumed soap preparation method - Google Patents
Transparent perfumed soap preparation method Download PDFInfo
- Publication number
- CN101497849B CN101497849B CN2009100370027A CN200910037002A CN101497849B CN 101497849 B CN101497849 B CN 101497849B CN 2009100370027 A CN2009100370027 A CN 2009100370027A CN 200910037002 A CN200910037002 A CN 200910037002A CN 101497849 B CN101497849 B CN 101497849B
- Authority
- CN
- China
- Prior art keywords
- acid
- soap
- transparent
- skin
- toilet soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses transparent soap and a preparation method thereof. The composite of the transparent soap is prepared and compounded by adopting a plurality of natural fatty acids, such as dodecanoic acid, hexadecanoic acid, myristic acid, stearic acid, and the like. The compound fatty acid and alkali such as sodium hydroxide or potassium hydroxide performs neutralization reaction, and then compound natural clarifier is added to prepare the natural transparent soap with high transparency. The pH value of the prepared transparent soap is controlled within 6.8-7.5; the transparent soap is neutral and soft, does not hurt the skin, has high transparency, high fatty acid content, better inoxidizability, durability, exquisite and rich foam, and very smoothness without greasy of the skin after use, can keep the skin naturally smooth and soft and resilient, and has remarkable skin protecting effect.
Description
Technical field
The present invention relates to a kind of transparent toilet soap and preparation method thereof.
Background technology
The use object of perfumed soap is different from washing soap, and it generally is at human body skin, such as washing one's hands, wash one's face and having a bath.In recent years,, not only require its function, and will have skin care, beauty treatment, sterilization and dispel some new functions such as smelly with clean skin along with the raising of people's living standard.Especially in recent years, along with green theory is rooted in the hearts of the people, the perfumed soap kind pursue day by day superior in, to the also paid more and more attention and the concern of consideration of human body and environmental safety, people more and more tend to use the pure natural perfumed soap.In addition, people have also proposed new requirement to the outward appearance of perfumed soap, and transparent toilet soap more and more is subjected to the favor in market.
At present, transparent soap has two kinds.A kind of is " adding " formula transparent soap, and adopting Oleum Cocois, sweet oil, castor-oil plant wet goods to contain the more grease of unsaturated fatty acids is raw material, and the compound lard zero pour should be between 35-38 ℃, without saltouing, the glycerine of generation stay help in the soap transparent.Add polyvalent alcohol, sucrose, ethanol etc. in addition and make transparent base, also can add crystallization inhibitor and enhance the transparency.Transparent soap is raw materials used must be highly pure, otherwise can cause muddiness.And in order to obtain fine soap crystallization, crystallisation process must be very slow.But this class " adding " formula transparent soap, because of fatty acid soaps content is low, washing effect is poor, easily corrupt, good-looking not being durable.Another kind of transparent soap is " grinding pressure " formula transparent soap, be also referred to as translucent soap (Translucent soap), its fatty acid content height, generally about 70%, it is to make original opaque soap crystal conversion become the crystal formation of vitreous state by processing such as mechanical mill, extruding repeatedly.This class translucent soap does not generally add transparent bases such as polyvalent alcohol, sucrose, ethanol, the shape that therefore is translucent, but compare with preceding a kind of transparent soap, harder, durable, low price is usually as senior washing soap.
More than the preparation method of two kinds of transparent soaps mainly have the not high and low problem of fatty acid soaps content of transparency, just become the research focus of transparent toilet soap so the preparation transparency is high with the high transparent soap of fatty acid soaps content.
Summary of the invention
The object of the present invention is to provide a kind of transparent toilet soap and preparation method thereof, the high and fatty acid soaps content height of prepared transparent toilet soap transparency.
Technical solution proposed by the invention is such: a kind of transparent toilet soap, and the composition of this transparent toilet soap is made up of following component by weight percentage:
Lauric acid 5-20; Tetradecanoic acid 0-10; Palmitinic acid 0-10;
Stearic acid 5-12; 30% sodium hydroxide or 30% potassium hydroxide 13-19;
95% ethanol 8-10; Glycerine 4-8; Sorbyl alcohol 8-10;
Sucrose 15-20; Water 5-10; Essence 0.1-0.2;
Lauryl alcohol polyethenoxy ether sodium sulfovinate salt 4-6.
By the method for above-mentioned transparent toilet soap preparation of compositions transparent toilet soap, its step of preparation process is: (1) adds water sepn with lauryl alcohol polyethenoxy ether sodium sulfovinate salt and mixes post-heating to 65-85 ℃, makes solution A; (2) glycerine, sorbyl alcohol, lauric acid, tetradecanoic acid, palmitinic acid, stearic acid, 95% ethanol are mixed, heat fused, temperature of fusion is 60-65 ℃, makes solution B; (3) will be preheating to 65-85 ℃ 30% sodium hydroxide or 30% potassium hydroxide and slowly flow in the solution B, treat that reaction in 30-40 minute is finished after, the control pH value is between 6.8-7.5, be warming up to 80-85 ℃, add solution A, after stirring, slowly be sprinkled into white sugar and stir evenly, be incubated after 30-40 minute, be cooled to 55-60 ℃, add essence, after mixing, be poured onto die for molding, promptly become transparent toilet soap.
Compared with prior art, the present invention has following unusual effect:
Transparent toilet soap of the present invention is to adopt multiple natural acid, composite as lauric acid, palmitinic acid, tetradecanoic acid, stearic acid, with compound fat acid and alkali, make fatty acid soaps as sodium hydroxide, potassium hydroxide generation neutralization reaction, then, add the composite natral transparent base, make the high natural transparent toilet soap of transparency, its pH value is controlled between the 6.5-7.5.Transparent toilet soap transparency height, the fatty acid soaps content height that makes by said components and method, have good oxidation-resistance, durable, foam is fine and smooth abundant, little to skin flesh pungency, use the back skin very smooth and oiliness, can keep the smooth naturally submissive and elasticity of skin, and significant skin effect is arranged.
Embodiment
By following embodiment the present invention is further elaborated.
Embodiment 1
(1) with weight percent be 4% lauryl alcohol polyethenoxy ether sodium sulfovinate salt to add weight percent be after 5% water sepn mixes, to be heated to 65 ℃, make solution A.
(2) with weight percent be 4% glycerine, 8% sorbyl alcohol, 5% lauric acid, 9.8% tetradecanoic acid, 5% palmitinic acid, 12% stearic acid, 10% 95% ethanol mixing, heat fused, temperature of fusion is 60 ℃, makes solution B.
(3) will be preheating to 65 ℃ weight percent is that 17% 30% sodium hydroxide slowly flow in the solution B, leaves standstill after 30 minutes question responses finish, and the control pH value is 6.8, then, be warming up to 80 ℃, add solution A, after stirring, slowly be sprinkled into weight percent and be 20% white sugar and stir evenly, be incubated after 30 minutes, be cooled to 55 ℃, the adding weight percent is 0.2% essence, after mixing, be poured onto die for molding, promptly become transparent toilet soap.
Embodiment 2
The preparation method is identical with example 1, and the weight percent that difference is each component is temperature value when, and detailed row are as follows:
(1) lauryl alcohol polyethenoxy ether sodium sulfovinate salt 6%; Water 10%; Be heated to 75 ℃.
(2) glycerine 8%; Sorbyl alcohol 10%; Lauric acid 7.9%; Tetradecanoic acid 10%; Palmitinic acid 0; Stearic acid 5%; 95% ethanol 10%; Temperature of fusion is 62 ℃.
(3) 30% potassium hydroxide 13%; 75 ℃ of preheating temperatures; Left standstill 35 minutes; PH value is 7.2; Be warming up to 82 ℃; White sugar 20%; Be incubated 35 minutes; Be cooled to 58 ℃; Essence 0.1%.
Embodiment 3
The preparation method is identical with example 1, and the weight percent that difference is each component is temperature value when, and detailed row are as follows:
(1) lauryl alcohol polyethenoxy ether sodium sulfovinate salt 5; Water 5; Be heated to 85
(2) glycerine 4.8; Sorbyl alcohol 8; Lauric acid 20%; Tetradecanoic acid 0; Palmitinic acid 10%; Stearic acid 5%; 95% ethanol 8%; Temperature of fusion is 65 ℃.
(3) 30% sodium hydroxide 19%; 85 ℃ of preheating temperatures; Left standstill 40 minutes; PH value is 7.5; Be warming up to 85 ℃; White sugar 15%; Be incubated 40 minutes; Be cooled to 60 ℃; Essence 0.2%.
Claims (1)
1. the preparation method of a transparent toilet soap, it is characterized in that: the composition of described transparent toilet soap is made up of following component by weight percentage:
Lauric acid 5-20; Tetradecanoic acid 0-10; Palmitinic acid 0-10;
Stearic acid 5-12; 30% sodium hydroxide or 30% potassium hydroxide 13-19;
95% ethanol 8-10; Glycerine 4-8; Sorbyl alcohol 8-10;
Sucrose 15-20; Water 5-10; Essence 0.1-0.2;
Lauryl alcohol polyethenoxy ether sodium sulfovinate salt 4-6;
The step of preparation process of described transparent toilet soap is: (1) adds water sepn with lauryl alcohol polyethenoxy ether sodium sulfovinate salt and mixes post-heating to 65-85 ℃, makes solution A; (2) glycerine, sorbyl alcohol, lauric acid, tetradecanoic acid, palmitinic acid, stearic acid, 95% ethanol are mixed, heat fused, temperature of fusion is 60-65 ℃, makes solution B; (3) will be preheating to 65-85 ℃ 30% sodium hydroxide or 30% potassium hydroxide and slowly flow in the solution B, treat that reaction in 30-40 minute is finished after, the control pH value is between 6.8-7.5, be warming up to 80-85 ℃, add solution A, after stirring, slowly be sprinkled into white sugar and stir evenly, be incubated after 30-40 minute, be cooled to 55-60 ℃, add essence, after mixing, be poured onto die for molding, promptly become transparent toilet soap.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100370027A CN101497849B (en) | 2009-01-20 | 2009-01-20 | Transparent perfumed soap preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100370027A CN101497849B (en) | 2009-01-20 | 2009-01-20 | Transparent perfumed soap preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101497849A CN101497849A (en) | 2009-08-05 |
| CN101497849B true CN101497849B (en) | 2010-12-29 |
Family
ID=40945121
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009100370027A Active CN101497849B (en) | 2009-01-20 | 2009-01-20 | Transparent perfumed soap preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101497849B (en) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925300A (en) * | 2011-10-05 | 2013-02-13 | 郑刚 | Lavender soap and its preparation method |
| CN102978048B (en) * | 2012-11-16 | 2014-11-05 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN103232910A (en) * | 2013-04-28 | 2013-08-07 | 广州丹奇日用化工厂有限公司 | Transparent handmade soap and preparation method thereof |
| CN104694306A (en) * | 2014-03-20 | 2015-06-10 | 陈昕林 | Fancy soap with high utilization rate and manufacturing method thereof |
| CN103952248B (en) * | 2014-04-18 | 2018-04-27 | 青岛澳海生物有限公司 | A kind of cleaning article containing conjugate linoleate and preparation method thereof |
| CN104762146B (en) * | 2015-03-27 | 2017-11-03 | 榆林学院 | The method that transparent soap is prepared with radiation treatment gutter oil |
| CN105316135B (en) * | 2015-11-09 | 2018-11-27 | 重庆琥珀茶油有限公司 | A kind of tea oil anti-acne facial soap |
| CN105296234B (en) * | 2015-11-09 | 2018-08-31 | 重庆琥珀茶油有限公司 | Camellia seed underwear special-purpose soap |
| CN105713754A (en) * | 2016-01-21 | 2016-06-29 | 广西大学 | Transparent soap and preparation method thereof |
| CN105567480A (en) * | 2016-02-25 | 2016-05-11 | 青岛洁百氏科技有限公司 | Enzyme soap and preparation method thereof |
| CN106047538A (en) * | 2016-06-11 | 2016-10-26 | 张家界茶坤缘生物科技开发有限公司 | Healthy soap containing original eucommia ulmoide extract and preparation method of healthy soap |
| CN106367246A (en) * | 2016-08-26 | 2017-02-01 | 广州市香事文化传播有限公司 | Agilawood and pearl soap and preparation method thereof |
| CN106978288A (en) * | 2017-05-05 | 2017-07-25 | 陈磊 | A kind of handmade soap containing Composition of Meteorite and preparation method thereof |
| CN108531320B (en) * | 2018-05-22 | 2020-11-24 | 中北大学 | Functional soap and preparation method thereof |
| CN109112014A (en) * | 2018-10-16 | 2019-01-01 | 云南爱尔康生物技术有限公司 | A kind of essential oil soap of astaxanthin-containing and preparation method thereof |
| CN109777676A (en) * | 2019-03-18 | 2019-05-21 | 惠州市旭东实业有限公司 | A kind of craft facial soap |
| CN109846739A (en) * | 2019-03-18 | 2019-06-07 | 惠州市旭东实业有限公司 | A kind of moisturizing facial soap |
| CN109880706A (en) * | 2019-04-22 | 2019-06-14 | 仝招 | Facial mask handmade soap |
| CN110846158A (en) * | 2019-11-28 | 2020-02-28 | 安徽倾镜生物科技有限公司 | Preparation method of amino acid soap and amino acid soap |
| CN112940882A (en) * | 2019-12-11 | 2021-06-11 | 广东柏亚化妆品有限公司 | Transparent composite soap and preparation method thereof |
| CN110982636A (en) * | 2019-12-11 | 2020-04-10 | 云南省林木种苗工作总站(云南省林木种苗花卉产品质量监督检验站) | African avocado-based perfumed soap and preparation method thereof |
| CN111893005A (en) * | 2020-07-01 | 2020-11-06 | 海南星光龙健康产业科技有限公司 | Antibacterial soap added with coconut shell activated carbon powder and preparation method thereof |
-
2009
- 2009-01-20 CN CN2009100370027A patent/CN101497849B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN101497849A (en) | 2009-08-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101497849B (en) | Transparent perfumed soap preparation method | |
| CN105331469B (en) | A kind of preparation method of compound bacteriostatic soap | |
| CN104434612A (en) | Tea bran shower gel | |
| CN104928080A (en) | Method for preparing peppermint-green tea handmade soap | |
| CN103937626A (en) | Natural plant handmade soap and preparing method thereof | |
| US5874392A (en) | Soap | |
| CN105733851A (en) | Transparent rose toilet soap and preparation method thereof | |
| CN107760498A (en) | Lemon grass craft essential oil soap and preparation method thereof | |
| CN102994278A (en) | Bee glue perfumed soap and making method thereof | |
| CN102451098B (en) | Mineral salt hand sanitizer and preparation method thereof | |
| CN105342922A (en) | Shower gel and preparation method thereof | |
| CN109337770A (en) | A kind of sweet wormwood soap composition | |
| CN105586188A (en) | Glass cleaner specially used for bathroom | |
| CN104531392A (en) | Health-preserving soap for dispelling skin superficial scars and preparation method thereof | |
| US20190284515A1 (en) | Solid soap composition | |
| CN106520416A (en) | Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof | |
| CN103110537A (en) | Allergy-free hand sanitizer | |
| CN105296229A (en) | Passion flower soap and preparation method thereof | |
| JP2005171219A (en) | Rice bran oil-derived raw material composition for cosmetic | |
| CN103550081A (en) | Skin care hand sanitizer | |
| KR101792838B1 (en) | Soap composition for beauty treatment containing shindari ingredient, and the manufacturing method thereof | |
| CN106916655A (en) | A kind of Chinese medicine retaining whitening handmade soap formula and its compounding method | |
| CN106479763A (en) | A kind of pet clean skin soap | |
| CN116083183A (en) | Block detergent for sensitive skin and its preparation method | |
| Pujiastuti et al. | Increasing the value added of production citronella oil and carrageenan in Rungkut Barata Surabaya |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |