CN101485465A - Edible microcapsule mineral matter nutritive salt and preparation method thereof - Google Patents

Edible microcapsule mineral matter nutritive salt and preparation method thereof Download PDF

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CN101485465A
CN101485465A CNA2009100426709A CN200910042670A CN101485465A CN 101485465 A CN101485465 A CN 101485465A CN A2009100426709 A CNA2009100426709 A CN A2009100426709A CN 200910042670 A CN200910042670 A CN 200910042670A CN 101485465 A CN101485465 A CN 101485465A
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edible
homogeneous
nutritive salt
nutrition fortifier
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CN101485465B (en
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胡良页
罗毅
罗薇
李明兰
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Hunan Light Industry Research Institute Co Ltd
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Hunan Light Industry Research Institute Co Ltd
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Abstract

The invention discloses edible microcapsule mineral nutritive salt containing calcium, iron, zinc, selenium, and other nutritive elements and a method for preparing the same. The edible microcapsule mineral nutritive is characterized in that edible salt is mixed with a nutrition enhancer microcapsule; a wall material and a nutrition enhancer are homogenized to form an adhesive solution; the adhesive solution is sprayed on the surface of sodium chloride to form the nutrition enhancer microcapsule; and the nutrition enhancer microcapsule adopts scientific compound processing technology to prepare the edible microcapsule mineral nutritive salt according to the sanitary standard of national food nutrition enhancer. The edible microcapsule mineral nutritive salt has extremely positive meanings on greatly improving nutritive substances needed by daily lives of people.

Description

Edible microcapsule mineral matter nutritive salt and preparation method thereof
Technical field
The invention belongs to food processing field, be specifically related to microcapsules nutritive salt that contains on calcium, iron, zinc, selenium and preparation method thereof.
Background technology
At present, the processing of domestic and international common nutritive salt, report is arranged in the literature, but all be to adopt the simple physics hybrid mode, nutrition fortifier directly admixed in the salt that microcapsules technology is used widely in food industry, and after adopting microcapsules technology with calcium, iron, zinc, selenium nutrition-intensified dose of microencapsulation, microcapsules nutritive salt or microcapsules compound nutritional salt are produced in regeneration, and this type of nutritive salt does not appear in the newspapers at home as yet, also do not see the Related product listing.There is following problem in the existing nutritive salt in market:
1, nutritive salt on the market all is to adopt simple physics to mix, because the proportion of nutrient and salt is different, is difficult to mix in actual production, has caused micro-mixing inhomogeneous, directly causes the unbalanced phenomenon of people's intake.
2, because nutrition fortifier and salt color have bigger difference, owing to mix inequality, thus caused the irregular colour of nutritive salt, influenced the nutritive salt sense organ.
3, because iron enriched nutrient has bigger iron fishy taste, the simple mixing makes nutritive salt discharge heavier iron fishy taste, makes people be difficult to accept.
4, human body needs ferrous ion to improve HC, but common nutritive salt makes and increase chalybeate and place air very easily to be oxidized to ferric ion, thereby is difficult to be absorbed by people.
5, common nutritive salt all is that nutrition fortifier directly is added in the salt, can cause salt to the aggravation of water in air branch adsorption phenomena, thereby make micro-oxidation, and is rotten, even go mouldy, and nutritive salt caking etc. have shortened the nutritive salt shelf life.
Summary of the invention
The object of the present invention is to provide edible microcapsule nutritive salt of nutrition fortifiers such as containing calcium, iron, zinc, selenium and preparation method thereof.
The objective of the invention is to realize in the following manner.
Edible microcapsule mineral matter nutritive salt is to have mixed the nutrition fortifier microcapsules in edible salt, and described nutrition fortifier microcapsules are that the glue that will form behind wall material and the nutrition fortifier homogeneous is sprayed at the formation of sodium chloride surface.
Described nutrition fortifier is selected from a kind of in calcium lactate, zinc lactate, EDTA ferrisodium, the sodium selenite; Described nutritive salt contains one or more nutrition fortifier microcapsules.
Described wall material is edible Arabic gum, starch, sodium alginate and edible gelatin.
The preparation method of described edible microcapsule mineral matter nutritive salt, be that the glue that will form behind wall material and the nutrition fortifier homogeneous is through super-dry, powder essence, screening, make described nutritive salt with edible salt is mixed, form nutrition fortifier microcapsules drying again but the glue behind the homogeneous will be sprayed onto the sodium chloride surface.
Described homogenizing process has experienced twice, and the used wall material of homogeneous is edible Arabic gum and starch for the first time; The used wall material of homogeneous is sodium alginate and edible gelatin for the second time.
Described nutrition fortifier microcapsules are with behind the edible Arabic gum of 5-15g, 5-35g starch, 500-3000ml deionized water, the 20-40g nutrition fortifier homogeneous, continue the mixed solution of adding 500-3000ml sodium alginate and edible gelatin and carry out the homogeneous second time, containing sodium alginate and the mass percent that mass percent is 5-10% in the described mixed solution is the edible gelatin of 5-20%, glue 1000-6000ml behind the second time homogeneous is sprayed at 100-1000g sodium chloride surface, through super-dry, powder essence, the formation of screening back.
The concrete preparation method of described edible microcapsule mineral matter nutritive salt is as follows:
(1) it is mixed to eat Arabic gum 5-15g, starch 5-35g, deionized water 500-3000ml, and heat temperature raising is to 50-90 ℃, after fully stirring, add nutrition fortifier 20-40g, stir and put into homogenizer after 4-8 minute and carry out homogeneous, homogenization pressure is 10-50MPa, and the time is 15-50 minute; In the material behind the first time homogeneous, continue to add the mixed solution that 500-3000ml contains sodium alginate and edible gelatin and carry out the homogeneous second time, containing sodium alginate and the mass percent that mass percent is 5-10% in the described mixed solution is the edible gelatin of 5-20%, homogenization pressure is 10-50MPa for the second time, and the time is 10-40 minute;
(2) in the mixer of band heating, add sodium chloride 100-1000g, stir on the limit, the limit heating is warming up to 50-90 ℃, and the glue 1000-6000ml employing press atomization device that homogeneous is good for the second time then is sprayed at the sodium chloride surface equably, spray on the limit, stir on the limit, and mixing time is 15-30 minute, and insulation was 5-30 minute after spray finished, temperature is 40-90 ℃, makes its drying;
(3) dried material is pulverized, after 80 purpose vibratory sieves, 80 order screenings are the microcapsules nutrition fortifier;
(4) with microcapsules nutrition fortifier and edible salt, put into mixer, stirred 5-20 minute, be edible microcapsule mineral matter nutritive salt.
Make calcium lactate, zinc lactate, EDTA ferrisodium, sodium selenite hardening agent microcapsules as stated above respectively.
Take by weighing calcium lactate microcapsules 10-60g respectively, EDTA ferrisodium microcapsules 5-20g, zinc lactate microcapsules 0.5-5g, sodium selenite microcapsules 1-50mg, edible salt 1000-3000g puts into mixer, stirs 5-20 minutes.Weighing then, pack qualified after testing after, be edible microcapsule calcium, iron, zinc, selenium compound nutritional salt.
Advantage of the present invention:
1, adopt microcapsules technology to produce edible microcapsule mineral matter nutritive salt, nutrition fortifier is covered by multilayer resist, and some acid ingredients, chemically-reactive substance have all been avoided directly contacting with air and other component and the various physical-chemical reactions that cause.Solved micro-oxidation in the salt, rotten, even go mouldy, the nutritive salt caking has shortened defectives such as nutritive salt shelf life.
2, add edible sodium chloride in encapsulation process and carry out counterweight, solved because the proportion of nutrient and salt is different, be difficult to mix in actual production, the trace element that causes mixes inhomogeneous, and then causes the unbalanced phenomenon of people's intake.
3, owing to designed dissolving and releasing mechanism in advance, can be between the most in good time in the suitableeest speed release nutrient.
4, edible microcapsule mineral matter nutritive salt is compared with commercially available nutritive salt, have and mix, the pale yellow unanimity of color, characteristics such as iron taste is light, water-soluble not to develop the color, absorbability is strong, good stability, shelf life is long, security is good have greatly improved the nutritive value of nutritive salt.
Description of drawings
Fig. 1 is a process chart of the present invention.
The specific embodiment
Following embodiment and embodiment are intended to further specify the present invention, rather than restriction the present invention.
Embodiment 1
(1) filling edible Arabic gum 10g, adding deionized water 3000ml in the container of starch 20g, heat temperature raising to 90 ℃, after fully stirring, add edible calcium lactate 30g, stir and put into homogenizer after 5 minutes and carry out homogeneous, homogenization pressure is 40MPa, and the time is 40 minutes; In the material behind the first time homogeneous, continue to add the solution that 1000ml contains the edible gelatin of 8% sodium alginate and 18% and carry out the homogeneous second time, its homogenization pressure is 40MPa, the time is 30 minutes, and is stand-by;
(2) in the mixer of band heating, add sodium chloride 800g, stir on the limit, the limit heating is warming up to 90 ℃, and the glue 5000ml employing press atomization device that homogeneous is good for the second time then is sprayed at the sodium chloride surface equably, spray on the limit, stir on the limit, and mixing time is 30 minutes, and insulation was 25 minutes after spray finished, temperature is 90 ℃, makes its drying;
(3) dried material is pulverized, after 80 purpose vibratory sieves, 80 order screenings are calcium lactate hardening agent microcapsules;
(4) take by weighing calcium lactate hardening agent microcapsules 60g respectively, edible salt 3000g puts into mixer, stirs 20 minutes, is edible microcapsule calcium lactate nutritive salt.
Embodiment 2
(1) filling edible Arabic gum 5g, adding deionized water 2000ml in the container of starch 35g, heat temperature raising to 60 ℃, after fully stirring, add EDTA ferrisodium 40g, stir and put into homogenizer after 5 minutes and carry out homogeneous, homogenization pressure is 50MPa, and the time is 15 minutes; In the material behind the first time homogeneous, continue to add the solution that 2000ml contains 5% sodium alginate and 20% edible gelatin and carry out the homogeneous second time, its homogenization pressure is 50MPa, the time is 30 minutes, and is stand-by;
(2) in the mixer of band heating, add sodium chloride 1000g, stir on the limit, the limit heating is warming up to 70 ℃, and the glue 6000ml employing press atomization device that homogeneous is good for the second time then is sprayed at the sodium chloride surface equably, spray on the limit, stir on the limit, and mixing time is 25 minutes, and insulation was 30 minutes after spray finished, temperature is 80 ℃, makes its drying;
(3) dried material is pulverized, after 80 purpose vibratory sieves, 80 order screenings are EDTA ferrisodium hardening agent microcapsules;
(4) take by weighing EDTA ferrisodium hardening agent microcapsules 20g respectively, edible salt 2500g puts into mixer, stirs 20 minutes, is edible microcapsule EDTA ferrisodium nutritive salt.
Embodiment 3
(1) filling edible Arabic gum 15g, adding deionized water 500ml in the container of starch 5g, heat temperature raising to 90 ℃, after fully stirring, add sodium selenite 20g, stir and put into homogenizer after 5 minutes and carry out homogeneous, homogenization pressure is 30MPa, and the time is 30 minutes; In the material behind the first time homogeneous, continue to add the solution that 2000ml contains 10% sodium alginate and 10% edible gelatin and carry out the homogeneous second time, its homogenization pressure is 30MPa, the time is 40 minutes, and is stand-by;
(2) in the mixer of band heating, add sodium chloride 400g, stir on the limit, the limit heating is warming up to 90 ℃, and the glue 3000ml employing press atomization device that homogeneous is good for the second time then is sprayed at the sodium chloride surface equably, spray on the limit, stir on the limit, and mixing time is 30 minutes, and insulation was 25 minutes after spray finished, temperature is 90 ℃, makes its drying;
(3) dried material is pulverized, after 80 purpose vibratory sieves, 80 order screenings are sodium selenite hardening agent microcapsules;
(4) take by weighing sodium selenite hardening agent microcapsules 50mg respectively, edible salt 1000g puts into mixer, stirs 20 minutes, is edible microcapsule sodium selenite nutritive salt.
Embodiment 4
Method by embodiment 1 makes edible microcapsule zinc lactate hardening agent.
Embodiment 5
Take by weighing the calcium lactate hardening agent microcapsules 60g that makes by the foregoing description method respectively, EDTA ferrisodium hardening agent microcapsules 20g, zinc lactate hardening agent microcapsules 5g, sodium selenite hardening agent microcapsules 50mg, edible salt 3000g puts into mixer, stirs 20 minutes.Weighing then, pack qualified after testing after, be edible microcapsule calcium, iron, zinc, selenium compound nutritional salt.
The sense organ of edible microcapsule nutritive salt and commercially available iron nutritive salt relatively
Edible microcapsule iron nutritive salt, the sense organ contrast of edible microcapsule calcium, iron, zinc, selenium compound nutritional salt and commercially available iron nutritive salt, it the results are shown in Table 1.
The sense organ of table 1 nutritive salt relatively
Figure A200910042670D00081

Claims (9)

1, edible microcapsule mineral matter nutritive salt, it is characterized in that, described nutritive salt is to have mixed the nutrition fortifier microcapsules in edible salt, and described nutrition fortifier microcapsules are that the glue that will form behind wall material and the nutrition fortifier homogeneous is sprayed at the formation of sodium chloride surface.
2, edible microcapsule mineral matter nutritive salt according to claim 1 is characterized in that, described nutrition fortifier is selected from a kind of in calcium lactate, zinc lactate, EDTA ferrisodium, the sodium selenite; Described nutritive salt contains one or more nutrition fortifier microcapsules.
3, edible microcapsule mineral matter nutritive salt according to claim 1 is characterized in that, described wall material is edible Arabic gum, starch, sodium alginate and edible gelatin.
4, the preparation method of the described edible microcapsule mineral matter nutritive salt of claim 1, be that the glue that will form behind wall material and the nutrition fortifier homogeneous is through super-dry, powder essence, screening, make described nutritive salt with edible salt is mixed, it is characterized in that, the glue that forms behind the homogeneous is sprayed onto the sodium chloride surface forms nutrition fortifier microcapsules drying again.
5, the preparation method of edible microcapsule mineral matter nutritive salt according to claim 4 is characterized in that, described nutrition fortifier is selected from a kind of in calcium lactate, zinc lactate, EDTA ferrisodium, the sodium selenite; Described nutritive salt contains one or more nutrition fortifier microcapsules.
6, the preparation method of edible microcapsule mineral matter nutritive salt according to claim 4 is characterized in that, described wall material is edible Arabic gum, starch, sodium alginate and edible gelatin.
According to the preparation method of claim 4 or 6 described edible microcapsule mineral matter nutritive salts, it is characterized in that 7, described homogenizing process has experienced twice, the used wall material of homogeneous is edible Arabic gum and starch for the first time; The used wall material of homogeneous is sodium alginate and edible gelatin for the second time.
8, the preparation method of edible microcapsule mineral matter nutritive salt according to claim 7, it is characterized in that, described nutrition fortifier microcapsules are with the edible Arabic gum of 5-15g, 5-35g starch, the 500-3000ml deionized water, behind the 20-40g nutrition fortifier homogeneous, continue the mixed solution of adding 500-3000ml sodium alginate and edible gelatin and carry out the homogeneous second time, containing sodium alginate and the mass percent that mass percent is 5-10% in the described mixed solution is the edible gelatin of 5-20%, glue 1000-6000ml behind the second time homogeneous is sprayed at 100-1000g sodium chloride surface, through super-dry, powder essence, the screening back forms.
9, the preparation method of edible microcapsule mineral matter nutritive salt according to claim 4 is characterized in that following steps:
(1) it is mixed to eat Arabic gum 5-15g, starch 5-35g, deionized water 500-3000ml, and heat temperature raising is to 50-90 ℃, after fully stirring, add nutrition fortifier 20-40g, stir and put into homogenizer after 4-8 minute and carry out homogeneous, homogenization pressure is 10-50MPa, and the time is 15-50 minute; In the material behind the first time homogeneous, continue to add the mixed solution that 500-3000ml contains sodium alginate and edible gelatin and carry out the homogeneous second time, containing sodium alginate and the mass percent that mass percent is 5-10% in the described mixed solution is the edible gelatin of 5-20%, homogenization pressure is 10-50MPa for the second time, and the time is 10-40 minute;
(2) in the mixer of band heating, add sodium chloride 100-1000g, stir on the limit, the limit heating is warming up to 50-90 ℃, and the glue 1000-6000ml employing press atomization device that homogeneous is good for the second time then is sprayed at the sodium chloride surface equably, spray on the limit, stir on the limit, and mixing time is 15-30 minute, and insulation was 5-30 minute after spray finished, temperature is 40-90 ℃, makes its drying;
(3) dried material is pulverized, after 80 purpose vibratory sieves, 80 order screenings are the microcapsules nutrition fortifier;
(4) with microcapsules nutrition fortifier and edible salt, put into mixer, stirred 5-20 minute, be edible microcapsule mineral matter nutritive salt.
CN2009100426709A 2009-02-18 2009-02-18 Edible microcapsule mineral matter nutritive salt and preparation method thereof Expired - Fee Related CN101485465B (en)

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CN104782915A (en) * 2015-04-22 2015-07-22 张奎昌 Method for preparing microelement-beta-cyclodextrin or derivative inclusion compound thereof
CN105285895A (en) * 2015-10-13 2016-02-03 界首市霸味食品有限公司 Seasoning rich in trace elements
CN108125209A (en) * 2018-01-18 2018-06-08 合肥工业大学 A kind of black rice anthocyanin salt and preparation method with antioxidation
CN108371317A (en) * 2018-02-06 2018-08-07 天津佰亿达企业管理股份有限公司 A kind of person in middle and old age's salt and preparation method thereof
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CN108402439A (en) * 2018-02-06 2018-08-17 天津阿尔康生物科技有限公司 A kind of alpha-linolenic acid salt and preparation method thereof
CN110403178A (en) * 2019-09-04 2019-11-05 武汉轻工大学 Organic selenium eats the preparation method of bamboo salt
CN111357900A (en) * 2018-12-25 2020-07-03 内蒙古伊利实业集团股份有限公司 A method for preparing beverage containing milk mineral salt
CN111602821A (en) * 2020-05-26 2020-09-01 广州富诺营养科技有限公司 Microcapsule containing sialic acid and DHA and preparation method thereof
CN114568681A (en) * 2022-05-09 2022-06-03 中国农业大学 NaCl microsphere with hollow structure and preparation method thereof
CN115624163A (en) * 2022-10-28 2023-01-20 中盐西南盐业有限公司 Iodine-added zinc-rich edible salt and preparation method thereof

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CN1212849A (en) * 1997-09-26 1999-04-07 王树青 Multi-element enriched nutrient salt
CN1271541A (en) * 1999-04-28 2000-11-01 王树青 Multi-element low-sodium nutritive salt
CN101028063A (en) * 2006-10-17 2007-09-05 左金煜 Health-care nutrient salt with low sodium, calcium, potassium and iodine content and its production

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CN104782915A (en) * 2015-04-22 2015-07-22 张奎昌 Method for preparing microelement-beta-cyclodextrin or derivative inclusion compound thereof
CN105285895A (en) * 2015-10-13 2016-02-03 界首市霸味食品有限公司 Seasoning rich in trace elements
CN108125209A (en) * 2018-01-18 2018-06-08 合肥工业大学 A kind of black rice anthocyanin salt and preparation method with antioxidation
CN108371317A (en) * 2018-02-06 2018-08-07 天津佰亿达企业管理股份有限公司 A kind of person in middle and old age's salt and preparation method thereof
CN108378344A (en) * 2018-02-06 2018-08-10 天津佰亿达企业管理股份有限公司 A kind of intelligence development salt and preparation method thereof
CN108402439A (en) * 2018-02-06 2018-08-17 天津阿尔康生物科技有限公司 A kind of alpha-linolenic acid salt and preparation method thereof
CN111357900A (en) * 2018-12-25 2020-07-03 内蒙古伊利实业集团股份有限公司 A method for preparing beverage containing milk mineral salt
CN110403178A (en) * 2019-09-04 2019-11-05 武汉轻工大学 Organic selenium eats the preparation method of bamboo salt
CN111602821A (en) * 2020-05-26 2020-09-01 广州富诺营养科技有限公司 Microcapsule containing sialic acid and DHA and preparation method thereof
CN114568681A (en) * 2022-05-09 2022-06-03 中国农业大学 NaCl microsphere with hollow structure and preparation method thereof
CN114568681B (en) * 2022-05-09 2022-07-19 中国农业大学 NaCl microsphere with hollow structure and preparation method thereof
CN115624163A (en) * 2022-10-28 2023-01-20 中盐西南盐业有限公司 Iodine-added zinc-rich edible salt and preparation method thereof

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