CN101421373A - 锆交联组合物及使用方法 - Google Patents
锆交联组合物及使用方法 Download PDFInfo
- Publication number
- CN101421373A CN101421373A CNA2007800134199A CN200780013419A CN101421373A CN 101421373 A CN101421373 A CN 101421373A CN A2007800134199 A CNA2007800134199 A CN A2007800134199A CN 200780013419 A CN200780013419 A CN 200780013419A CN 101421373 A CN101421373 A CN 101421373A
- Authority
- CN
- China
- Prior art keywords
- composition
- cross
- linked
- zirconium
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/50—Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
- C09K8/504—Compositions based on water or polar solvents
- C09K8/506—Compositions based on water or polar solvents containing organic compounds
- C09K8/508—Compositions based on water or polar solvents containing organic compounds macromolecular compounds
- C09K8/512—Compositions based on water or polar solvents containing organic compounds macromolecular compounds containing cross-linking agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/58—Compositions for enhanced recovery methods for obtaining hydrocarbons, i.e. for improving the mobility of the oil, e.g. displacing fluids
- C09K8/588—Compositions for enhanced recovery methods for obtaining hydrocarbons, i.e. for improving the mobility of the oil, e.g. displacing fluids characterised by the use of specific polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/60—Compositions for stimulating production by acting on the underground formation
- C09K8/62—Compositions for forming crevices or fractures
- C09K8/66—Compositions based on water or polar solvents
- C09K8/68—Compositions based on water or polar solvents containing organic compounds
- C09K8/685—Compositions based on water or polar solvents containing organic compounds containing cross-linking agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/60—Compositions for stimulating production by acting on the underground formation
- C09K8/84—Compositions based on water or polar solvents
- C09K8/86—Compositions based on water or polar solvents containing organic compounds
- C09K8/88—Compositions based on water or polar solvents containing organic compounds macromolecular compounds
- C09K8/887—Compositions based on water or polar solvents containing organic compounds macromolecular compounds containing cross-linking agents
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Medicinal Preparation (AREA)
- Colloid Chemistry (AREA)
Abstract
Description
实施例号 | %Zr | aZr | TEAb | HPEDc | 丙三醇 | 水 | gptd | 漩涡闭合时间(min.) | gptd | 漩涡闭合时间(min.) |
摩尔 | 摩尔 | 摩尔 | 摩尔 | 摩尔 | pH为4 | pH为5 | ||||
Zr-TEAe | 13.2 | 1 | 4 | 0 | 0 | 0 | 0.32 | 10:00 | 0.48 | 0:32 |
1 | 9.3 | 1 | 2 | 0.5 | 0.5 | 2.5 | 0.68 | 1:19 | 1.04 | 1:12 |
2 | 9.3 | 1 | 4 | 1 | 0 | 0 | 0.44 | 0:53 | 0.68 | 0:01 |
3 | 7.8 | 1 | 4 | 1 | 1 | 5 | 0.52 | 1:02 | 0.80 | 0:55 |
4 | 8.9 | 1 | 4 | 0.5 | 1 | 5 | 0.48 | 1:14 | 0.80 | 3:28 |
5 | 8.5 | 1 | 4 | 1 | 0.5 | 2.5 | 0.48 | 0:48 | 0.72 | 1:02 |
6 | 9.8 | 1 | 4 | 0.5 | 0.5 | 2.5 | 0.44 | 0:40 | 0.64 | 1:07 |
7 | 8.9 | 1 | 4 | 1 | 0 | 2.5 | 0.48 | 0:23 | 0.68 | 0:03 |
8 | 8.9 | 1 | 4 | 1 | 0.5 | 0 | 0.48 | 0:51 | 0.68 | 0:31 |
9 | 8.1 | 1 | 4 | 1 | 0.5 | 5 | 0.52 | 0:37 | 0.76 | 0:59 |
10 | 8.5 | 1 | 4 | 1 | 1 | 0 | 0.48 | 2:34 | 0.72 | 0:41 |
11 | 8.1 | 1 | 4 | 1 | 1 | 2.5 | 0.52 | 1:27 | 0.76 | 0:24 |
12 | 8.5 | 1 | 4 | 1 | 0 | 5 | 0.48 | 0:38 | 0.72 | 0:01 |
13 | 10.3 | 1 | 4 | 0.5 | 0.5 | 0 | 0.40 | 1:18 | 0.60 | 0:17 |
14 | 10.9 | 1 | 4 | 0.5 | 0 | 0 | 0.36 | 2:16 | 0.56 | 0:10 |
实施例 | %Zr | Zra | TEAb | HPEDc | 丙三醇 | 水 | gptd | 漩涡闭合时间(min) |
摩尔 | 摩尔 | 摩尔 | 摩尔 | 摩尔 | pH10 | |||
对比A | 12.4 | 1.44 | >10 | |||||
对比B | 13.2 | 1 | 4 | 0 | 0 | 0 | 1:36 | 0:14 |
对比C | 5.4 | 3:36 | 0.05 | |||||
2 | 9.3 | 1 | 4 | 1 | 0 | 0 | 1.92 | 1:05 |
7 | 8.9 | 1 | 4 | 1 | 0 | 2.5 | 2.0 | 2:16 |
8 | 8.9 | 1 | 4 | 1 | 0.5 | 0 | 2.0 | 3:35 |
10 | 8.5 | 1 | 4 | 1 | 1 | 0 | 2:08 | 2:56 |
12 | 8.5 | 1 | 4 | 1 | 0 | 5 | 2:12 | 4:28 |
Claims (13)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/353,765 US20070187642A1 (en) | 2006-02-14 | 2006-02-14 | Zirconium cross-linking composition and methods of use |
US11/353,765 | 2006-02-14 | ||
PCT/US2007/003203 WO2007095018A2 (en) | 2006-02-14 | 2007-02-05 | Zirconium cross-linking composition and methods of use |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101421373A true CN101421373A (zh) | 2009-04-29 |
CN101421373B CN101421373B (zh) | 2013-04-10 |
Family
ID=38261518
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2007800134199A Expired - Fee Related CN101421373B (zh) | 2006-02-14 | 2007-02-05 | 锆交联组合物及使用方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20070187642A1 (zh) |
EP (1) | EP1984471B1 (zh) |
CN (1) | CN101421373B (zh) |
CA (1) | CA2642257C (zh) |
RU (1) | RU2424270C2 (zh) |
WO (1) | WO2007095018A2 (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103375153A (zh) * | 2012-04-17 | 2013-10-30 | 中国石油化工股份有限公司 | 一种油田调剖堵水方法 |
CN104927828A (zh) * | 2015-04-29 | 2015-09-23 | 中国石油集团渤海钻探工程有限公司 | 耐高温有机锆交联剂及其制备方法以及一种压裂液冻胶及其制备方法 |
CN105579666A (zh) * | 2013-06-11 | 2016-05-11 | 索尔维美国有限公司 | 采出水硼酸盐交联组合物及使用方法 |
CN115466352A (zh) * | 2022-10-11 | 2022-12-13 | 杰瑞能源服务有限公司 | 调堵剂、调堵剂制备方法及封堵方法 |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8242060B2 (en) * | 2006-12-21 | 2012-08-14 | Dorf Ketal Specialty Catalysts, LLC | Stable solutions of zirconium hydroxyalkylethylene diamine complex and use in oil field applications |
US8236739B2 (en) * | 2007-03-30 | 2012-08-07 | Dork Ketal Speciality Catalysts, LLC | Zirconium-based cross-linker compositions and their use in high pH oil field applications |
US8697610B2 (en) * | 2007-05-11 | 2014-04-15 | Schlumberger Technology Corporation | Well treatment with complexed metal crosslinkers |
PA8785001A1 (es) * | 2007-06-18 | 2008-06-17 | Johnson Matthey Plc | Compuestos estables en agua, catalizadores y reacciones catalizadas novedosos |
US8153564B2 (en) | 2008-03-07 | 2012-04-10 | Dorf Ketal Speciality Catalysts, Llc | Zirconium-based cross-linking composition for use with high pH polymer solutions |
US8853135B2 (en) * | 2008-05-07 | 2014-10-07 | Schlumberger Technology Corporation | Method for treating wellbore in a subterranean formation with high density brines and complexed metal crosslinkers |
US8030254B2 (en) * | 2008-10-15 | 2011-10-04 | Schlumberger Technology Corporation | System, method, and apparatus for utilizing divalent brines in viscosified well treatment fluids |
CA2994540A1 (en) * | 2015-08-03 | 2017-02-09 | Ecolab Usa Inc. | Compositions and methods for delayed crosslinking in hydraulic fracturing fluids |
CA3030763A1 (en) * | 2016-07-15 | 2018-01-18 | Ecolab Usa Inc. | Compositions and methods for delayed crosslinking in hydraulic fracturing fluids |
CN106928959B (zh) * | 2017-03-27 | 2018-10-26 | 成都劳恩普斯科技有限公司 | 交联剂、全悬浮压裂液及其制备方法 |
WO2019110290A1 (en) * | 2017-12-04 | 2019-06-13 | Unilever N.V. | An antiperspirant composition comprising zirconium |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2824114A (en) * | 1952-09-09 | 1958-02-18 | Du Pont | Water soluble group iv-a metal esters of amino alcohols and their preparation |
US2824115A (en) * | 1954-11-09 | 1958-02-18 | Nat Lead Co | Titanium and zirconium organic compounds |
GB786388A (en) * | 1954-11-09 | 1957-11-20 | Nat Lead Co | Titanium and zirconium organic compounds |
US4683068A (en) * | 1981-10-29 | 1987-07-28 | Dowell Schlumberger Incorporated | Fracturing of subterranean formations |
US4534870A (en) * | 1982-06-28 | 1985-08-13 | The Western Company Of North America | Crosslinker composition for high temperature hydraulic fracturing fluids |
US4477360A (en) * | 1983-06-13 | 1984-10-16 | Halliburton Company | Method and compositions for fracturing subterranean formations |
US4460751A (en) * | 1983-08-23 | 1984-07-17 | Halliburton Company | Crosslinking composition and method of preparation |
US4664713A (en) * | 1984-05-04 | 1987-05-12 | Halliburton Company | Composition for and method of altering the permeability of a subterranean formation |
US4749041A (en) * | 1986-02-19 | 1988-06-07 | Dowell Schlumberger Incorporated | Hydraulic fracturing method using delayed crosslinker composition |
US4798902A (en) * | 1987-02-09 | 1989-01-17 | E. I. Du Pont De Nemours And Company | Zirconium chelates and their use for cross-linking |
US4883605A (en) * | 1987-02-09 | 1989-11-28 | E. I. Du Pont De Nemours And Company | Zirconium chelates and their use for cross-linking |
US5460887A (en) * | 1990-12-13 | 1995-10-24 | E. I. Du Pont De Nemours And Company | Stain-resistant polyamide substrates |
US5466846A (en) * | 1994-11-16 | 1995-11-14 | Benchmark Research And Technology, Inc. | Process for preparation of stable aqueous solutions of zirconium chelates |
US6737386B1 (en) * | 1999-05-26 | 2004-05-18 | Benchmark Research And Technology Inc. | Aqueous based zirconium (IV) crosslinked guar fracturing fluid and a method of making and use therefor |
US6227295B1 (en) * | 1999-10-08 | 2001-05-08 | Schlumberger Technology Corporation | High temperature hydraulic fracturing fluid |
JP3935831B2 (ja) * | 2001-11-30 | 2007-06-27 | 松本製薬工業株式会社 | 水性組成物および水溶性ポリマー用架橋剤 |
US6810959B1 (en) * | 2002-03-22 | 2004-11-02 | Bj Services Company, U.S.A. | Low residue well treatment fluids and methods of use |
US6737485B1 (en) * | 2003-04-22 | 2004-05-18 | E. I. Du Pont De Nemours And Company | Titanium chelate dispersions |
US7268100B2 (en) * | 2004-11-29 | 2007-09-11 | Clearwater International, Llc | Shale inhibition additive for oil/gas down hole fluids and methods for making and using same |
-
2006
- 2006-02-14 US US11/353,765 patent/US20070187642A1/en not_active Abandoned
-
2007
- 2007-02-05 WO PCT/US2007/003203 patent/WO2007095018A2/en active Application Filing
- 2007-02-05 CA CA2642257A patent/CA2642257C/en not_active Expired - Fee Related
- 2007-02-05 EP EP07750083.3A patent/EP1984471B1/en not_active Expired - Fee Related
- 2007-02-05 CN CN2007800134199A patent/CN101421373B/zh not_active Expired - Fee Related
- 2007-02-05 RU RU2008136866/03A patent/RU2424270C2/ru not_active IP Right Cessation
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103375153A (zh) * | 2012-04-17 | 2013-10-30 | 中国石油化工股份有限公司 | 一种油田调剖堵水方法 |
CN105579666A (zh) * | 2013-06-11 | 2016-05-11 | 索尔维美国有限公司 | 采出水硼酸盐交联组合物及使用方法 |
CN105579666B (zh) * | 2013-06-11 | 2021-01-22 | 索尔维美国有限公司 | 采出水硼酸盐交联组合物及使用方法 |
CN104927828A (zh) * | 2015-04-29 | 2015-09-23 | 中国石油集团渤海钻探工程有限公司 | 耐高温有机锆交联剂及其制备方法以及一种压裂液冻胶及其制备方法 |
CN115466352A (zh) * | 2022-10-11 | 2022-12-13 | 杰瑞能源服务有限公司 | 调堵剂、调堵剂制备方法及封堵方法 |
Also Published As
Publication number | Publication date |
---|---|
EP1984471B1 (en) | 2018-08-08 |
RU2424270C2 (ru) | 2011-07-20 |
CA2642257A1 (en) | 2007-08-23 |
CN101421373B (zh) | 2013-04-10 |
WO2007095018A2 (en) | 2007-08-23 |
CA2642257C (en) | 2013-05-28 |
EP1984471A2 (en) | 2008-10-29 |
US20070187642A1 (en) | 2007-08-16 |
WO2007095018A3 (en) | 2007-10-04 |
RU2008136866A (ru) | 2010-03-20 |
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Owner name: DORF KETAL SPECIAL CATALYST LLC Free format text: FORMER OWNER: E.I. DU PONT DE NEMOURS AND CO. Effective date: 20110804 |
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Effective date of registration: 20110804 Address after: American Texas Applicant after: Dov Ketal Special Catalyst Co.,Ltd. Address before: Delaware, USA Applicant before: E. I. du Pont de Nemours and Co. |
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Granted publication date: 20130410 Termination date: 20210205 |