CN101341966A - Lixiviation apparatus for zanthoxylum oil and digestion method - Google Patents
Lixiviation apparatus for zanthoxylum oil and digestion method Download PDFInfo
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- CN101341966A CN101341966A CNA2008100459977A CN200810045997A CN101341966A CN 101341966 A CN101341966 A CN 101341966A CN A2008100459977 A CNA2008100459977 A CN A2008100459977A CN 200810045997 A CN200810045997 A CN 200810045997A CN 101341966 A CN101341966 A CN 101341966A
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- chinese prickly
- leaching device
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Abstract
The invention discloses an extracting device and an extracting method for zanthoxylum oil and is characterized in that an oil joint (3) at the left upper end of a low temperature refluxing extracting device (16) is connected with a plant oil heater by a first oil transportation pump(2); the right upper end is connected with a spiral propeller (4); a slag outlet (8) at the left side of the low temperature refluxing extracting device is connected with a squeezer (9); the oil outlet of the squeezer after being jointed with the oil outlet (15) of the low temperature refluxing extracting device is connected with a filter (10); the filter is connected with a clarifying pool (12) by a second oil transportation pump(11); the clarifying pool is connected with a filling machine (14)by a third oil transportation pump(13). The materials are added according to a mass ratio that the ratio of plant oil to zanthoxylum is 2:0.5 to 1. The plant oil is added into a heater (1) to pre-heat to be 80 to 90 DEG C; the zanthoxylum is added into a cracker (6) for being crashed to 20 to 40 meshes; the materials are respectively and continuously fed into the low temperature refluxing extracting device (16) at the two ends; the temperature in the low temperature refluxing extracting device (16) is maintained between 80 to 90 DEG C. The left side of the low temperature refluxing extracting device (16) is for fueling and discharges the slag; the right side is for feeding and discharges the oil to obtain the fished product of the zanthoxylum oil.
Description
Technical field
The present invention relates to a kind of leaching device and leach extraction method thereof of Chinese prickly ash oil, belong to the manufacture field of food or flavouring.
Background technology
Traditional Chinese prickly ash oil preparation method is that Lay seed oil is heated to about 100 ℃, drops into a certain amount of fresh flower green pepper or dried flower green pepper, and artificial the stirring and lixiviate approximately after half an hour leaches Chinese prickly ash, promptly gets the Chinese prickly ash oil product.Because manual operations, the Chinese prickly ash inequality of being heated, unstable product quality, production can not serialization, and output is restricted.
Chinese patent 96117607.5 discloses " Chinese prickly ash oil making technology and equipment thereof ", this invention adopts the serialization operation to improve output, and temperature control is constant, and Chinese prickly ash is heated evenly, product quality gets a promotion, and has overcome some shortcomings that traditional Chinese prickly ash oil handicraft workshop formula is produced.But leaching device has adopted spiral conveyer, does not simultaneously also consider to contain in the Chinese prickly ash characteristic of a lot of lower boiling volatile materials, in 100～200 ℃ of lixiviates of temperature, makes in the Chinese prickly ash fragrance matter of a lot of low volatilities scatter and disappear and can not get effective reservation.
Chinese patent 03117388.8 discloses " a kind of Chinese prickly ash oil and preparation method thereof and the production equipment that is used for this method ", and this invention and 96117607.5 has a lot of similarities, exists extraction temperature too high equally, the shortcoming that extracting efficiency is lower.In addition, though it is the production and processing of raw material that this invention can be applicable to the dried flower green pepper, but the granularity to the dried flower green pepper does not claim, Chinese prickly ash and vegetable oil all enter from an end of spiral conveyer in leaching process, belong to and flow extraction, cause unstable product quality, the active constituent content of products obtained therefrom is lower.
Summary of the invention
The objective of the invention is to provide a kind of leaching device and leach extraction method thereof of Chinese prickly ash oil at the deficiencies in the prior art, be characterized in adopting the lixiviate of low temperature adverse current method, keep fragrance matter and the low-boiling point material in the Chinese prickly ash effectively, improved the quality of Chinese prickly ash oil.
Purpose of the present invention is realized that by following technical measures wherein said raw material umber is parts by weight except that specifying.
The leaching device of Chinese prickly ash oil is connected with the vegetable oil heater by first oil transfer pump by the upper end oil interface of low temperature adverse current leaching device, upper right side is connected with spiral propeller, spiral propeller is connected with pulverizer by feed hopper, low temperature adverse current leaching device left side slag notch is connected with squeezer, the oil-out of squeezer be connected filter after the oil-out of low temperature adverse current leaching device converges, filter is connected with depositing reservoir by second oil transfer pump, and depositing reservoir is connected with bottle placer by the 3rd oil transfer pump.
Establish turning cylinder in the low temperature adverse current leaching device, turning cylinder is connected with motor, establishes spiral pushing device on the turning cylinder, the peripheral hardware heat-insulation layer.
The installation of low temperature adverse current leaching device body is tilted 3～8 ° to horizontal axis, and the rotating speed of turning cylinder is 50～200rpm.
The leach extraction method of the leaching device of Chinese prickly ash oil may further comprise the steps:
(1) presses vegetable oil: the weight ratio of Chinese prickly ash=2: 0.5～1, vegetable oil added be warming up to 80～90 ℃ in the heater, Chinese prickly ash added be crushed to 20～60 orders in the pulverizer, raw material are respectively from two ends input low temperature adverse current leaching device, when vegetable oil when first oil transfer pump is added to 2/3 volume of low temperature adverse current leaching device, suspend to refuel; Zanthoxylum powder after will pulverizing again passes through spiral propeller through loading hopper, in the input low temperature adverse current leaching device, open the motor of main shaft, zanthoxylum powder rotates with spiral pushing device, propelling from right to left, constantly stir, roll, all the time be kept in motion fully to soak into and contact with vegetable oil, behind 8～10min, open Chinese prickly ash oil oil-out, the Chinese prickly ash dregs of fat are discharged from slag notch, beginning adds vegetable oil and zanthoxylum powder continuously, keeping the oily temperature in the low temperature adverse current leaching device is 80～90 ℃, and the left side of low temperature adverse current leaching device is refueled and slagged tap, and the right side is reinforced and fuel-displaced;
(2) dregs of fat of discharging from slag notch enter to squeeze the squeezer and remove slag, the oil that the oil of squeezing out and oil-out flow out converges to enter in the filter and filters, leach the Chinese prickly ash slag, fluid passes through second oil transfer pump to depositing reservoir, pass through the 3rd oil transfer pump at last to the bottle placer can, obtain finished product Chinese prickly ash oil.
Vegetable oil is any in rapeseed oil, salad oil, peanut oil or the soybean oil.
The present invention compared with prior art has the following advantages:
(1) extraction efficiency height, it is short to extract operation hours;
(2) parameter is easy to control, and equipment operates steadily with artificial few;
(3) extraction effect is good, and the concentration gradient of contained Chinese prickly ash fragrance and fiber crops flavor material changes the characteristics of just suitable Chinese prickly ash lixiviate in the Chinese prickly ash oil in the leaching process, makes Chinese prickly ash oil keep the color of former Chinese prickly ash oil to greatest extent.
Description of drawings
Fig. 1 is a Chinese prickly ash oil low temperature adverse current leaching device schematic diagram.
Fig. 2 is the structural representation of Chinese prickly ash oil low temperature adverse current leaching device.
Wherein: 1. heater, 2. first oil transfer pump, 3. oil-collecting hole, 4. spiral propeller, 5. feed hopper, 6. pulverizer, 7. motor, 8. slag notch, 9. squeezer, 10. filter, 11. second oil transfer pumps, 12. depositing reservoirs, 13. the 3rd oil transfer pump, 14. bottle placers, 15. oil-outs, 16. low temperature adverse current leaching device, 17. spiral pushing devices, 18. turning cylinders.
The specific embodiment
Below by embodiment the present invention is carried out entity description; be necessary to be pointed out that at this present embodiment only is used for the present invention is further specified; can not be interpreted as limiting the scope of the invention, the person skilled in the art in this field can make some nonessential improvement and adjustment according to the content of the invention described above.
Embodiment 1:
Press rapeseed oil and dry fruit Chinese prickly ash with 2: 1 part by weight, take by weighing rapeseed oil 1000kg, Chinese prickly ash 500kg;
Rapeseed oil is heated to 80 ℃ by heater 1, squeezes into oil-in 3, enter in the low temperature adverse current leaching device 16 by first oil transfer pump 2, when rapeseed oil be full of low temperature adverse current leaching device volume 2/3 the time, suspend to refuel; Meanwhile, the dry fruit Chinese prickly ash is joined in the pulverizer 6 that rotating speed is 3000～4000r/min, the Chinese prickly ash after the pulverizing adds in the material bin 5;
The liquid valve 15 of opening Chinese prickly ash oil liquid outlet behind the 8min goes out Chinese prickly ash oil, and the Chinese prickly ash dregs of fat are discharged from slag notch 8; Beginning is continuously with rapeseed oil, and the temperature of maintenance low temperature adverse current leaching device is at 80 ℃.Equipment enters normal operation, and the side loading that low temperature adverse current leaching device is low is fuel-displaced, and a high side is refueled out the dregs of fat;
The slag of discharging from slag notch 8 enters to squeeze the squeezer 9 and removes slag, the oil that oil of squeezing out and oil-out 15 flow out flows in the lump in the microporous membrane filters 10 and filters, squeeze into second oil transfer pump 11 then and clarified in the depositing reservoir 12 3～5 days, squeeze in the bottle placer 14 the can Chinese prickly ash oil that gets product by the 3rd oil transfer pump 13 at last.
Embodiment 2:
Press rapeseed oil and dry fruit Chinese prickly ash with 2: 0.8 part by weight, take by weighing rapeseed oil 1000kg, Chinese prickly ash 400kg;
Rapeseed oil is heated to 85 ℃ by heater 1, squeezes into oil-in 3, enter in the low temperature adverse current leaching device 16 by first oil transfer pump 2, when rapeseed oil be full of low temperature adverse current leaching device volume 2/3 the time, suspend to refuel; Meanwhile, the dry fruit Chinese prickly ash is joined in the pulverizer 6 that rotating speed is 3000～4000r/min, the Chinese prickly ash after the pulverizing adds in the material bin 5;
The liquid valve 15 of opening Chinese prickly ash oil liquid outlet behind the 10min goes out Chinese prickly ash oil, and the Chinese prickly ash dregs of fat are discharged from slag notch 8; Beginning is continuously with rapeseed oil, and the temperature of maintenance low temperature adverse current leaching device is at 80 ℃.Equipment enters normal operation, and the side loading that low temperature adverse current leaching device is low is fuel-displaced, and a high side is refueled out the dregs of fat;
The slag of discharging from slag notch 8 enters to squeeze the squeezer 9 and removes slag, the oil that oil of squeezing out and oil-out 15 flow out flows in the lump in the microporous membrane filters 10 and filters, squeeze into second oil transfer pump 11 then and clarified in the depositing reservoir 12 3～5 days, squeeze in the bottle placer 14 the can Chinese prickly ash oil that gets product by the 3rd oil transfer pump 13 at last.
Embodiment 3:
Press rapeseed oil and dry fruit Chinese prickly ash with 2: 0.5 part by weight, take by weighing rapeseed oil 1000kg, Chinese prickly ash 250kg;
Rapeseed oil is heated to 90 ℃ by heater 1, squeezes into oil-in 3, enter in the low temperature adverse current leaching device 16 by first oil transfer pump 2, when rapeseed oil be full of low temperature adverse current leaching device volume 2/3 the time, suspend to refuel; Meanwhile, the dry fruit Chinese prickly ash is joined in the pulverizer 6 that rotating speed is 3000～4000r/min, the Chinese prickly ash after the pulverizing adds in the material bin 5;
The liquid valve 15 of opening Chinese prickly ash oil liquid outlet behind the 12min goes out Chinese prickly ash oil, and the Chinese prickly ash dregs of fat are discharged from slag notch 8; Beginning is continuously with rapeseed oil, and the temperature of maintenance low temperature adverse current leaching device is at 80 ℃.Equipment enters normal operation, and the side loading that low temperature adverse current leaching device is low is fuel-displaced, and a high side is refueled out the dregs of fat;
The slag of discharging from slag notch 8 enters to squeeze the squeezer 9 and removes slag, the oil that oil of squeezing out and oil-out 15 flow out flows in the lump in the microporous membrane filters 10 and filters, squeeze into second oil transfer pump 11 then and clarified in the depositing reservoir 12 3～5 days, squeeze in the bottle placer 14 the can Chinese prickly ash oil that gets product by the 3rd oil transfer pump 13 at last.
Claims (5)
1. the leaching device of a Chinese prickly ash oil, the upper end oil interface (3) that it is characterized in that the low temperature adverse current leaching device (16) of this device is connected with vegetable oil heater (1) by first oil transfer pump (2), upper right side is connected with spiral propeller (4), spiral propeller is connected with pulverizer (6) by feed hopper (5), low temperature adverse current leaching device (16) left side slag notch (8) is connected with squeezer (9), the oil-out of squeezer be connected filter (10) after the oil-out (15) of low temperature adverse current leaching device converges, filter is connected with depositing reservoir (12) by second oil transfer pump (11), and depositing reservoir is connected with bottle placer (14) by the 3rd oil transfer pump (13).
2. the leaching device of Chinese prickly ash oil according to claim 1 is characterized in that establishing in the low temperature adverse current leaching device (16) turning cylinder (18), and turning cylinder is connected with motor (7), establishes spiral pushing device (17) on the turning cylinder, the peripheral hardware heat-insulation layer.
3. the leaching device of Chinese prickly ash oil according to claim 1 is characterized in that the installation of low temperature adverse current leaching device (16) body is tilted 3～8 ° to horizontal axis, and the rotating speed of turning cylinder (18) is 50～200rpm.
4. as the leach extraction method of the leaching device of Chinese prickly ash oil as described in one of claim 1～3, it is characterized in that this method may further comprise the steps:
(1) presses vegetable oil: the weight ratio of Chinese prickly ash=2: 0.5～1, vegetable oil added in the heater (1) be warming up to 80～90 ℃, Chinese prickly ash added in the pulverizer (6) be crushed to 20～60 orders, raw material are respectively from two ends input low temperature adverse current leaching devices (16), when vegetable oil when first oil transfer pump (2) is added to 2/3 volume of low temperature adverse current leaching device, suspend to refuel; Zanthoxylum powder after will pulverizing again passes through spiral propeller (4) through loading hopper (5), in the input low temperature adverse current leaching device, open the motor (7) of main shaft (18), zanthoxylum powder rotates with spiral pushing device, propelling from right to left, constantly stir, roll, all the time be kept in motion fully to soak into and contact with vegetable oil, behind 8～10min, open Chinese prickly ash oil oil-out (15), the Chinese prickly ash dregs of fat are discharged from slag notch (8), beginning adds vegetable oil and zanthoxylum powder continuously, oily temperature in the low temperature adverse current leaching device remains on 80～90 ℃, and the left side of low temperature adverse current leaching device is refueled and slagged tap, and the right side is reinforced and fuel-displaced;
(2) dregs of fat of discharging from slag notch (8) enter to squeeze the squeezer (9) and remove slag, the oil that oil of squeezing out and oil-out (15) flow out converges to enter in the filter (10) and filters, leach the Chinese prickly ash slag, fluid passes through second oil transfer pump (11) to depositing reservoir (12), pass through the 3rd oil transfer pump (13) at last to bottle placer (14) can, obtain finished product Chinese prickly ash oil.
5. as the leach extraction method of the leaching device of Chinese prickly ash oil as described in the claim 4, it is characterized in that vegetable oil is any in rapeseed oil, salad oil, peanut oil or the soybean oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008100459977A CN101341966A (en) | 2008-09-08 | 2008-09-08 | Lixiviation apparatus for zanthoxylum oil and digestion method |
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| CNA2008100459977A CN101341966A (en) | 2008-09-08 | 2008-09-08 | Lixiviation apparatus for zanthoxylum oil and digestion method |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101606676B (en) * | 2009-07-13 | 2012-07-04 | 周大甫 | Production technology of fresh zanthoxylum oil |
| CN103074211A (en) * | 2013-01-30 | 2013-05-01 | 山东贝隆杜仲生物工程有限公司 | Continuous enzymolysis device for eucommia seeds |
| CN103749742A (en) * | 2013-12-31 | 2014-04-30 | 安顺市西秀区百岁陈德文牌食品加工厂 | Production method of zanthoxylum oil |
| CN104172067A (en) * | 2014-07-17 | 2014-12-03 | 江苏华桑食品科技有限公司 | Method for preparing green prickleyash extract |
| CN104365878A (en) * | 2013-08-15 | 2015-02-25 | 四川帅青花椒开发有限公司 | Method for producing fresh zanthoxylum oil |
| CN106147991A (en) * | 2016-08-16 | 2016-11-23 | 张�杰 | A kind of equipment and the method utilizing this equipment production chilli oil |
| CN106174419A (en) * | 2016-07-23 | 2016-12-07 | 洪雅县和鑫农业科技发展有限公司 | A kind of Pericarpium Zanthoxyli beans manufacture method |
| CN106244312A (en) * | 2016-08-16 | 2016-12-21 | 张�杰 | A kind of microwave equipment preparing chilli oil and preparation method |
| CN106262643A (en) * | 2016-08-16 | 2017-01-04 | 张�杰 | A kind of production line preparing chilli oil and preparation method |
| CN106281651A (en) * | 2016-08-16 | 2017-01-04 | 张�杰 | A kind of chilli oil ultrasonic extraction device and preparation method |
| CN106350196A (en) * | 2016-08-16 | 2017-01-25 | 张�杰 | System and method for producing chili oil |
| CN106509167A (en) * | 2016-11-08 | 2017-03-22 | 四川农业大学 | Production technology for preparing fresh zanthoxylum bungeanum oil by pressing method |
| CN106942395A (en) * | 2016-08-16 | 2017-07-14 | 张�杰 | A kind of production line and preparation method for preparing chilli oil |
| CN107177414A (en) * | 2017-07-14 | 2017-09-19 | 云南宏绿辣素有限公司 | A kind of method that spiral oil press produces Zanthoxylum essential oil |
| CN107927205A (en) * | 2017-11-29 | 2018-04-20 | 成都新润油脂有限责任公司 | A kind of green zanthoxylum oil production process |
| CN108244594A (en) * | 2016-12-29 | 2018-07-06 | 中粮集团有限公司 | A kind of Zanthoxylum essential oil and preparation method thereof |
| CN110651839A (en) * | 2019-10-31 | 2020-01-07 | 宁夏回春生物科技有限公司 | Preparation method of grape seed nutritional oil |
| CN113208076A (en) * | 2021-05-21 | 2021-08-06 | 小金县四姑娘山天然沙棘食品有限公司 | Low-sugar sea-buckthorn jam preparation system |
| CN114292692A (en) * | 2021-11-19 | 2022-04-08 | 重庆智青阳油脂有限公司 | Pepper extraction tank |
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2008
- 2008-09-08 CN CNA2008100459977A patent/CN101341966A/en active Pending
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101606676B (en) * | 2009-07-13 | 2012-07-04 | 周大甫 | Production technology of fresh zanthoxylum oil |
| CN103074211A (en) * | 2013-01-30 | 2013-05-01 | 山东贝隆杜仲生物工程有限公司 | Continuous enzymolysis device for eucommia seeds |
| CN104365878A (en) * | 2013-08-15 | 2015-02-25 | 四川帅青花椒开发有限公司 | Method for producing fresh zanthoxylum oil |
| CN103749742A (en) * | 2013-12-31 | 2014-04-30 | 安顺市西秀区百岁陈德文牌食品加工厂 | Production method of zanthoxylum oil |
| CN104172067A (en) * | 2014-07-17 | 2014-12-03 | 江苏华桑食品科技有限公司 | Method for preparing green prickleyash extract |
| CN104172067B (en) * | 2014-07-17 | 2015-12-09 | 江苏华桑食品科技有限公司 | A kind of preparation method of pericarpium zanthoxyli schinifolii extract |
| CN106174419A (en) * | 2016-07-23 | 2016-12-07 | 洪雅县和鑫农业科技发展有限公司 | A kind of Pericarpium Zanthoxyli beans manufacture method |
| CN106281651A (en) * | 2016-08-16 | 2017-01-04 | 张�杰 | A kind of chilli oil ultrasonic extraction device and preparation method |
| CN106262643A (en) * | 2016-08-16 | 2017-01-04 | 张�杰 | A kind of production line preparing chilli oil and preparation method |
| CN106147991A (en) * | 2016-08-16 | 2016-11-23 | 张�杰 | A kind of equipment and the method utilizing this equipment production chilli oil |
| CN106350196A (en) * | 2016-08-16 | 2017-01-25 | 张�杰 | System and method for producing chili oil |
| CN106942395A (en) * | 2016-08-16 | 2017-07-14 | 张�杰 | A kind of production line and preparation method for preparing chilli oil |
| CN106244312A (en) * | 2016-08-16 | 2016-12-21 | 张�杰 | A kind of microwave equipment preparing chilli oil and preparation method |
| CN106509167A (en) * | 2016-11-08 | 2017-03-22 | 四川农业大学 | Production technology for preparing fresh zanthoxylum bungeanum oil by pressing method |
| CN108244594A (en) * | 2016-12-29 | 2018-07-06 | 中粮集团有限公司 | A kind of Zanthoxylum essential oil and preparation method thereof |
| CN108244594B (en) * | 2016-12-29 | 2021-07-13 | 中粮集团有限公司 | Zanthoxylum oil and preparation method thereof |
| CN107177414A (en) * | 2017-07-14 | 2017-09-19 | 云南宏绿辣素有限公司 | A kind of method that spiral oil press produces Zanthoxylum essential oil |
| CN107927205A (en) * | 2017-11-29 | 2018-04-20 | 成都新润油脂有限责任公司 | A kind of green zanthoxylum oil production process |
| CN110651839A (en) * | 2019-10-31 | 2020-01-07 | 宁夏回春生物科技有限公司 | Preparation method of grape seed nutritional oil |
| CN113208076A (en) * | 2021-05-21 | 2021-08-06 | 小金县四姑娘山天然沙棘食品有限公司 | Low-sugar sea-buckthorn jam preparation system |
| CN113208076B (en) * | 2021-05-21 | 2023-10-24 | 小金县四姑娘山天然沙棘食品有限公司 | Low-sugar sea buckthorn jam preparation system |
| CN114292692A (en) * | 2021-11-19 | 2022-04-08 | 重庆智青阳油脂有限公司 | Pepper extraction tank |
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Open date: 20090114 |