CN101313883B - Emulsifying agent for cosmetics and preparation method thereof - Google Patents
Emulsifying agent for cosmetics and preparation method thereof Download PDFInfo
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- CN101313883B CN101313883B CN2008100648254A CN200810064825A CN101313883B CN 101313883 B CN101313883 B CN 101313883B CN 2008100648254 A CN2008100648254 A CN 2008100648254A CN 200810064825 A CN200810064825 A CN 200810064825A CN 101313883 B CN101313883 B CN 101313883B
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- cosmetics
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- glycerol
- emulsifying agent
- phosphatidyl choline
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Abstract
The invention provides an emulsifier for cosmetics and a preparation method thereof. The emulsifier comprises the following compositions in weight percent: 10 to 20 portions of hydrogenated soybean phosphatidylcholine, 2 to 5 portions of ornitrol, 1 to 3 portions of polyoxyethylene castor oil, 2 to 3 portions of tannic acid, 5 to 10 portions of glycerol, 1 to 3 portions of glycerol monostearate sucrose esters and 56 to 79 portions of de-ionized water. The emulsifier has strong antioxygenic property, is fully natural without side effects, and has various health care functions. The emulsifier for the cosmetics is prepared by taking the hydrogenated soybean phosphatidylcholine as main raw material, along with the ornitrol, the polyoxyethylene castor oil, the tannic acid, the glycerol, the glycerol monostearate sucrose esters and the de-ionized water, is fully natural without side effects, and can protect epidermal cells of human body from being invaded by freeradicals after long-term use, thereby having the efficacy of delaying senescence.
Description
(1) technical field
The present invention relates to a kind of emulsifying agent for cosmetics, relate in particular to a kind of cosmetic emulsifier based on active hydrogenated soya phosphatide and preparation method thereof.
(2) technical background
The emulsifying agent for cosmetics majority is the chemosynthesis material, and long-term eating has certain toxic action to skin.Hydrogenated soy phosphatidyl choline is owing to use catalysis and hydrogenation technique; the unsaturated chain of unsaturated fatty acid in the soybean phospholipid molecular structure is disappeared; thereby improve chemical stability, dispersibility, the emulsibility of lecithin widely; it is a kind of good naturally occurring emulsifying agent; human body skin had protective effect, so can be widely used in the various cosmetics.
(3) summary of the invention
The object of the present invention is to provide a kind of very strong antioxygenic property that has, pure natural, have no side effect, be rich in the emulsifying agent for cosmetics of plurality of health care functions.
The object of the present invention is achieved like this: it comprises that percentage by weight is hydrogenated soy phosphatidyl choline 10-20 part, cholesterol 2-5 part, polyoxyethylene castor oil 1-3 part, tannic acid 2-3 part, glycerol 5-10 part, glycerol monostearate sucrose ester 1-3 part and deionized water 56-79 part.
Another object of the present invention is to provide a kind of preparation method of emulsifying agent for cosmetics: at first be that raw material is through catalytic hydrogenation with the soybean phospholipid, reaction back separating catalyst, hydrogen peroxide decolour, remove solvent, the acquisition iodine value is 20～30 hydrogenated soya phosphatide, with percentage by weight is hydrogenated soya phosphatide 10-20 part, cholesterol 2-5 part, polyoxyethylene castor oil 1-3 part, tannic acid 2-3 part, glycerol 5-10 part, glycerol monostearate sucrose ester 1-3 part and the abundant mix homogeneously of deionized water 56-79 part, makes emulsifying agent for cosmetics.
Preparation method of the present invention also has some technical characterictics like this:
1, the preparation condition of described hydrogenated soy phosphatidyl choline is with dichloromethane---alcohol mixture (V: V=3: 1) be solvent, selecting palladium catalyst, its addition for use is 5% of phospholipid consumption, at 55 ℃, Hydrogen Vapor Pressure is 0.6MPa, isothermal reaction 3h gets final product in the 1L autoclave, reaction product is after separating catalyst, hydrogen peroxide decolouring, removing solvent, can obtain iodine value is 20～30, and it is yellowish that color is, the hydrogenated soy phosphatidyl choline of no bad smell.
Soybean lecithin adopts catalytic hydrogenation method among the present invention, and the unsaturated bond fractional saturation that phospholipid is contained improves its stability and weakens or eliminate its color and abnormal smells from the patient.The present invention has adopted catalytic hydrogenation method to prepare a kind of hydrogenated soya phosphatide, for day chemical industry etc. provides a kind of novel material.
Advantage of the present invention is:
1. soybean phospholipid is through catalytic hydrogenation, and the unsaturated bond fractional saturation that phospholipid is contained improves its stability and weakens or eliminate its color and abnormal smells from the patient.
2. the present invention is body material with the hydrogenated soya phosphatide; a kind of cosmetic emulsifier that is aided with cholesterol, polyoxyethylene castor oil, tannic acid, glycerol, glycerol monostearate sucrose ester, deionized water and prepares; pure natural, have no side effect; life-time service can protect the human epidermal cell to avoid the infringement of free radical, thereby has the effect of slow down aging.
(4) specific embodiment
Below in conjunction with specific embodiment the present invention is further described:
Embodiment 1:
Present embodiment is chosen refining soybean phospholipid 200g, with dichloromethane such as 400ml---alcohol mixture (V: V=3: 1) be solvent, adding the 10g palladium catalyst, to be heated to 55 ℃, Hydrogen Vapor Pressure in the 1L autoclave be 0.6MPa, behind the isothermal reaction 3h, reaction product decolours, removes solvent through separating catalyst, hydrogen peroxide, obtaining iodine value is 20～30, and it is yellowish that color is, the hydrogenated soya phosphatide of no bad smell.
Get the hydrogenated soya phosphatide 10g of above-mentioned prepared, add cholesterol 2g, polyoxyethylene castor oil 3g, tannic acid 2g, glycerol 5g, glycerol monostearate sucrose ester 1g and deionized water 77g more respectively, above-mentioned raw materials behind high speed (5000r/m) mixing, promptly be can be applicable to various cosmetics.
Embodiment 2:
The preparation process of hydrogenated soy phosphatidyl choline is with embodiment 1 in the present embodiment, difference is to get the hydrogenated soy phosphatidyl choline 15g of above-mentioned prepared, add cholesterol 4g, polyoxyethylene castor oil 2g, tannic acid 3g, glycerol 8g, glycerol monostearate sucrose ester 2g and deionized water 66g more respectively, above-mentioned raw materials behind high speed (5000r/m) mixing, promptly be can be applicable to various cosmetics.
Embodiment 3:
The preparation process of hydrogenated soy phosphatidyl choline is with embodiment 1 in the present embodiment, difference is to get hydrogenated soy phosphatidyl choline 20g, cholesterol 5g, polyoxyethylene castor oil 3g, tannic acid 3g, glycerol 10g, glycerol monostearate sucrose ester 3g and the deionized water 56g of above-mentioned prepared, above-mentioned raw materials behind high speed (5000r/m) mixing, promptly be can be applicable to various cosmetics.
Claims (3)
1. an emulsifying agent for cosmetics is characterized in that it comprises that weight portion is hydrogenated soy phosphatidyl choline 10-20 part, cholesterol 2-5 part, polyoxyethylene castor oil 1-3 part, tannic acid 2-3 part, glycerol 5-10 part, glycerol monostearate sucrose ester 1-3 part and deionized water 56-79 part.
2. the preparation method of an emulsifying agent for cosmetics, it is characterized in that: at first be that raw material is through catalytic hydrogenation with the soybean lecithin, reaction back separating catalyst, hydrogen peroxide decolour, remove solvent, the acquisition iodine value is 20～30 hydrogenated soy phosphatidyl choline, with weight ratio is hydrogenated soy phosphatidyl choline 10-20 part, cholesterol 2-5 part, polyoxyethylene castor oil 1-3 part, tannic acid 2-3 part, glycerol 5-10 part, glycerol monostearate sucrose ester 1-3 part and the abundant mix homogeneously of deionized water 56-79 part, makes emulsifying agent for cosmetics.
3. the preparation method of emulsifying agent for cosmetics according to claim 2, it is characterized in that, the preparation condition of described hydrogenated soy phosphatidyl choline is: with dichloromethane---alcohol mixture V: V=3: 1 is solvent, select palladium catalyst for use, its addition is 5% of a phospholipid consumption, at 55 ℃, Hydrogen Vapor Pressure is 0.6MPa, isothermal reaction 3h gets final product in the 1L autoclave, reaction product is after separating catalyst, hydrogen peroxide decolouring, removing solvent, can obtain iodine value is 20～30, it is yellowish that color is, the hydrogenated soy phosphatidyl choline of no bad smell.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100648254A CN101313883B (en) | 2008-06-27 | 2008-06-27 | Emulsifying agent for cosmetics and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100648254A CN101313883B (en) | 2008-06-27 | 2008-06-27 | Emulsifying agent for cosmetics and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101313883A CN101313883A (en) | 2008-12-03 |
| CN101313883B true CN101313883B (en) | 2010-06-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2008100648254A Expired - Fee Related CN101313883B (en) | 2008-06-27 | 2008-06-27 | Emulsifying agent for cosmetics and preparation method thereof |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN117653563B (en) * | 2023-12-13 | 2024-06-04 | 奥俐莱雅（广东）家化科技有限公司 | Recombinant collagen peptide with high transdermal property and preparation process and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214199A (en) * | 2007-12-29 | 2008-07-09 | 广东拉芳日化有限公司 | Nano active acne-eliminating cosmetic composition |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214199A (en) * | 2007-12-29 | 2008-07-09 | 广东拉芳日化有限公司 | Nano active acne-eliminating cosmetic composition |
Non-Patent Citations (2)
| Title |
|---|
| 化妆品配方.日用化妆品配方Vol.30 No.3.2007,Vol.30(No.3),46-48. * |
| 化妆品配方.日用化妆品配方Vol.30No.3.2007 Vol.30(No.3) |
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| CN101313883A (en) | 2008-12-03 |
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Inventor after: Zheng Huanyu Inventor after: Cheng Tao Inventor after: Shao Meili Inventor after: Han Jianchun Inventor before: Han Jianchun Inventor before: Cheng Tao Inventor before: Shao Meili |
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Free format text: CORRECT: INVENTOR; FROM: HAN JIANCHUN CHENG TAO SHAO MEILI TO: ZHENG HUANYU CHENG TAO SHAO MEILI HAN JIANCHUN |
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