CN101265031A - Aqueous glass heat insulation paint and preparation method thereof - Google Patents
Aqueous glass heat insulation paint and preparation method thereof Download PDFInfo
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- CN101265031A CN101265031A CNA2008100237083A CN200810023708A CN101265031A CN 101265031 A CN101265031 A CN 101265031A CN A2008100237083 A CNA2008100237083 A CN A2008100237083A CN 200810023708 A CN200810023708 A CN 200810023708A CN 101265031 A CN101265031 A CN 101265031A
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Abstract
The invention discloses a waterborne insulating glass coating and a preparation method thereof. The coating mainly comprises the following components of (weight parts): waterborne resin 50-80 and nanometer indium-tin-oxide (ITO) slurry, wherein the solid content in the slurry is 10-30 wt%. The preparation method comprises the steps of dripping ITO slurry into waterborne resin, sequentially adding adjuvants, and stirring for 10-30 min to obtain synthetic waterborne insulating glass coating. The glass made of the inventive coating has high visible light transmittance and high ultraviolet radiation and infrared radiation (thermal radiation) rejection rate, can prevent direct transmission of ultraviolet radiation and thermal radiation, and can be directly used for film coating with spontaneous hardening and convenient usage.
Description
Technical field
The present invention relates to a kind of aqueous glass heat insulation paint and preparation method thereof.
Background technology
Energy-saving glass on the market mainly contains heat reflection coated glass and low radiation coated glass at present.Heat-reflecting glass is to plate metal, nonmetal and sull at glass surface, makes it have certain reflecting effect, solar energy reflection can be returned in the atmosphere, reaches the purpose that stops in the solar thermal energy inlet chamber.Its control to sun power of the high more explanation of the reflectivity of heat-reflecting glass is strong more, but the visible light transmissivity of glass can reduce along with the rising of reflectivity, thereby light transmission is reduced, influence the daylighting effect, and the glass-reflected rate is excessive also the light pollution problem may occur.The visible light transmissivity of heat reflection coated glass is lower, is generally 20～30%, greatly influences indoor lighting.And low radiation coated glass is by apply low-emissivity coating in surface of ordinary glass, make the radiant ratio on low radiation coated glass surface be lower than simple glass, thereby can reduce the radiation loss of heat, make low radiation coated glass have good effect of heat insulation, and the transmitance to visible light of this low radiation coated glass is moderate, thereby can avoid the generation of light pollution, build good luminous environment.At present, mainly contain the low radiation coated glass that the online chemical Vapor deposition process of magnetron sputtering method and float glass process (CVD) is produced on the market, but blemish in an otherwise perfect thing is: the low radiation coated glass price is higher, is difficult to enter common people house.Therefore, usefulness is more at present: a kind of is nano transparent heat-insulating glass, and the coating of this glass surface need be carried out baking-curing in baking oven, makes very trouble; Another kind is a dual-component polyurethane glass, and the coating of this glass needs two kinds of components to be used in combination, because deployed coating is unfavorable for storing, the remaining coating in back of therefore filming often can only be discarded, and causes waste; And some two component glass heat-insulating coating also needs to add the organic solvent diluting agent that is unfavorable for environmental protection when allotment.
Summary of the invention
A technical problem to be solved by this invention is: provide a kind of be directly used in film, the aqueous glass heat insulation paint of air-set.
For solving the problems of the technologies described above, the technical solution used in the present invention is: a kind of aqueous glass heat insulation paint, the component that comprises following weight part: 50～80 parts of synthetic water-base resins, 10～40 parts in nano indium tin oxide slurry, 0～5 part in water, 0.5～5 part of film coalescence aid, 0.1～3 part of silicon-dioxide, 0.1～5 part of coupling agent, 0.1～2 part of defoamer, 0.1～2 part of flow agent, 0.1～2 part of wetting agent, wherein: the nano indium tin oxide slurry comprises the component of following weight percent again: In-Sn oxide powder 15～25%, water 35～45%, ethanol 7.5～12.5%, Virahol 7.5～12.5%, propyl carbinol 7.5～12.5%, 1-Methoxy-2-propyl acetate 7.5～12.5%, dispersion agent 0.075～0.125%, and solid content accounts for 10～30% of indium tin oxide slurry, and the particle diameter of solid content is between 20～50 nanometers.
Above-mentioned dispersion agent is the hexadecyl benzene sulfonic acid sodium salt.
Above-mentioned synthetic water-base resin is selected from vinylformic acid, urethane, modified polyurethane interpolymer, silylation and Resins, epoxy.
Above-mentioned synthetic water-base resin is a resinous varnish.
A technical problem to be solved by this invention is: a kind of preparation method who is directly used in the aqueous glass heat insulation paint of filming is provided.
For solving the problems of the technologies described above, the technical solution used in the present invention is: the preparation method of aqueous glass heat insulation paint the steps include:
1) preparation nano indium tin oxide slurry: the weight percent of each component takes by weighing In-Sn oxide powder, water, ethanol, Virahol, propyl carbinol, 1-Methoxy-2-propyl acetate and dispersion agent in weight part that accounts in coating according to above-mentioned indium tin oxide slurry and the indium tin oxide slurry, to add as water, ethanol, Virahol, propyl carbinol and the 1-Methoxy-2-propyl acetate of solvent in the dispersion machine then, then, add dispersion agent again, add In-Sn oxide powder at last, after disperseing 2 hours, can obtain the nano indium tin oxide slurry of required weight part;
2) take by weighing 0.1～2 part of 0.1～2 part of synthetic water-base resin, film coalescence aid, silicon-dioxide, coupling agent, defoamer, flow agent and the wetting agent of the described weight part of claim 1, then with the 1st) the nano indium tin oxide slurry that makes of step is added drop-wise in the water-base resin, add film coalescence aid, silicon-dioxide, coupling agent, wetting agent, defoamer and flow agent again, stirred 10～30 minutes, and can obtain finished product.
The water that adds above-mentioned weight part is in process of production adjusted the viscosity of described coating.
The invention has the beneficial effects as follows: coating of the present invention can be directly used in and film, and also can require dilute with water according to practice of construction, and the coating before having avoided need be used the shortcoming of organic solvent diluting, very environmental protection; And air-set need not be toasted after filming, and uses very convenient.In addition, the production cost of this coating and material cost are all lower.
Embodiment
A kind of aqueous glass heat insulation paint of the present invention, the component that comprises following weight part: 50～80 parts of synthetic water-base resins, 10～40 parts in nano indium tin oxide slurry, 0～5 part in water, 0.5～5 part of film coalescence aid, 0.1～3 part of silicon-dioxide, 0.1～5 part of coupling agent, 0.1～2 part of defoamer, 0.1～2 part of flow agent, 0.1～2 part of wetting agent, wherein: the nano indium tin oxide slurry comprises the component of following weight percent again: In-Sn oxide powder 15～25%, water 35～45%, ethanol 7.5～12.5%, Virahol 7.5～12.5%, propyl carbinol 7.5～12.5%, 1-Methoxy-2-propyl acetate 7.5～12.5%, dispersion agent 0.075～0.125%, and solid content accounts for 10～30% of indium tin oxide slurry, and the particle diameter of solid content is between 20～50 nanometers.In the present embodiment, described dispersion agent is the hexadecyl benzene sulfonic acid sodium salt; Described synthetic water-base resin can be selected from vinylformic acid, urethane, modified polyurethane interpolymer, silylation and Resins, epoxy, also can be resinous varnish.
Describe the preparation method of aqueous glass heat insulation paint of the present invention below in detail.
Embodiment 1:
At first take by weighing indium tin oxide (RTO) powder 200 grams, water 400 grams, ethanol 100 grams, Virahol 100 grams, propyl carbinol 100 grams, 1-Methoxy-2-propyl acetate 100 grams and dispersion agent 1 gram add water, ethanol, Virahol, propyl carbinol and 1-Methoxy-2-propyl acetate in the dispersion machine then, then, add dispersion agent again, add In-Sn oxide powder at last, after disperseing 2 hours, can obtain the nano indium tin oxide slurry of 1001 gram favorable dispersities, the solids content in the slurry is approximately 20%;
Take by weighing synthetic water-base resin 7500 grams again, film coalescence aid 200 grams, silica 1 00 gram, coupling agent 200 grams, defoamer 100 grams, flow agent 100 grams and wetting agent 100 grams, then the nano indium tin oxide slurry that makes is added drop-wise in the water-base resin, add film coalescence aid, silicon-dioxide, coupling agent, wetting agent, defoamer and flow agent again, stirred 30 minutes, can obtain finished product.The water that adds 0～450 gram is in process of production adjusted the viscosity of described coating.
Embodiment 2:
At first take by weighing indium tin oxide (RTO) powder 200 grams, water 400 grams, ethanol 100 grams, Virahol 100 grams, propyl carbinol 100 grams, 1-Methoxy-2-propyl acetate 100 grams and dispersion agent 1 gram add water, ethanol, Virahol, propyl carbinol and 1-Methoxy-2-propyl acetate in the dispersion machine then, then, add dispersion agent again, add In-Sn oxide powder at last, disperseed 2 hours, can obtain the nano indium tin oxide slurry of 1001 gram favorable dispersities, the solids content in the slurry is approximately 20%;
Take by weighing synthetic water-base resin 3000 grams, film coalescence aid 200 grams, silica 1 00 gram, coupling agent 200 grams, defoamer 100 grams, flow agent 100 grams and wetting agent 100 grams, then the nano indium tin oxide slurry that makes is added drop-wise in the water-base resin, add film coalescence aid, silicon-dioxide, coupling agent, wetting agent, defoamer and flow agent again, stirred 20 minutes, can obtain finished product.The water that adds 0～250 gram is in process of production adjusted the viscosity of described coating.
Embodiment 3:
At first take by weighing indium tin oxide (RTO) powder 200 grams, water 400 grams, ethanol 100 grams, Virahol 100 grams, propyl carbinol 100 grams, 1-Methoxy-2-propyl acetate 100 grams and dispersion agent 1 gram add water, ethanol, Virahol, propyl carbinol and 1-Methoxy-2-propyl acetate in the dispersion machine then, then, add dispersion agent again, add In-Sn oxide powder at last, disperseed 2 hours, can obtain the nano indium tin oxide slurry of 1001 gram favorable dispersities, the solids content in the slurry is approximately 20%;
Take by weighing synthetic water-base resin 1400 grams, film coalescence aid 100 grams, silicon-dioxide 50 grams, coupling agent 50 grams, defoamer 50 grams, flow agent 50 grams and wetting agent 50 grams, then the nano indium tin oxide slurry that makes is added drop-wise in the water-base resin, add film coalescence aid, silicon-dioxide, coupling agent, wetting agent, defoamer and flow agent again, stirred 10 minutes, can obtain finished product.The water that adds 0～125 gram is in process of production adjusted the viscosity of described coating.
The coating of exploitation has thermal insulation but is transparent poor though coating of the present invention has overcome in the past, though or shortcoming transparent but the thermal insulation difference, both advantages are rolled into one, to this, white glass with 6 mm thick is that example is done to be perfectly clear once contrasting: the shading coefficient SC of the white glass of 6 mm thick is 0.94, and the white glass of the 6 mm thick back shading coefficient SC that films can be low to moderate 0.61, and the shading coefficient of the back glass of filming is lower by 35% than white glass, and heat-proof quality has raising greatly; And corresponding visible light transmissivity is higher, usually about 75%.
The production technique of this coating comprises that the manufacture craft of filming in later stage is all very simple, does not need expensive facility investment, and production and cost of manufacture are all lower; The cost that adds the material that coating of the present invention adopts is all lower, and the cost of the coating that so just makes is lower, and uses the cost of coated glass of this coating material production also lower.And the smooth visuality of the smooth surface of this coated glass is good, with line rod spreader thermal insulating coating is applied to clean glass surface, and coating is levelling automatically, and surfacing is smooth, sees through glass and sees that object is also more clearly.In addition, coating of the present invention can be directly used in and film, and also can require dilute with water according to practice of construction; very environmental protection, thus the coating before having avoided need be used the shortcoming of organic solvent diluting, and after filming; air-set need not be toasted, and uses very convenient.
Claims (6)
1. aqueous glass heat insulation paint, the component that comprises following weight part: 50～80 parts of synthetic water-base resins, 10～40 parts in nano indium tin oxide slurry, 0～5 part in water, 0.5～5 part of film coalescence aid, 0.1～3 part of silicon-dioxide, 0.1～5 part of coupling agent, 0.1～2 part of defoamer, 0.1～2 part of flow agent, 0.1～2 part of wetting agent, wherein, the nano indium tin oxide slurry comprises the component of following weight percent again: 15～25% In-Sn oxide powder, 35～45% water, 7.5～12.5% ethanol, 7.5～12.5% Virahol, 7.5～12.5% propyl carbinol, 7.5～12.5% 1-Methoxy-2-propyl acetate, 0.075～0.125% dispersion agent, and solid content accounts for 10～30% of indium tin oxide slurry, and the particle diameter of solid content is between 20～50 nanometers.
2. aqueous glass heat insulation paint as claimed in claim 1 is characterized in that: described dispersion agent is the hexadecyl benzene sulfonic acid sodium salt.
3. aqueous glass heat insulation paint as claimed in claim 1 or 2 is characterized in that: described synthetic water-base resin is selected from vinylformic acid, urethane, modified polyurethane interpolymer, silylation and Resins, epoxy.
4. aqueous glass heat insulation paint as claimed in claim 1 or 2 is characterized in that: described synthetic water-base resin is a resinous varnish.
5. the preparation method of aqueous glass heat insulation paint the steps include:
1) preparation nano indium tin oxide slurry: the weight part that in coating, accounts for according to the described indium tin oxide slurry of claim 1, and the weight percent of each component takes by weighing In-Sn oxide powder in the indium tin oxide slurry, water, ethanol, Virahol, propyl carbinol, 1-Methoxy-2-propyl acetate and dispersion agent, then will be as the water of solvent, ethanol, Virahol, propyl carbinol and 1-Methoxy-2-propyl acetate add in the dispersion machine, and then adding dispersion agent, add In-Sn oxide powder at last, after disperseing 2 hours, can obtain the nano indium tin oxide slurry of required weight part;
2) take by weighing synthetic water-base resin, film coalescence aid, silicon-dioxide, coupling agent, defoamer, flow agent and the wetting agent of the described weight part of claim 1, then, with the 1st) the nano indium tin oxide slurry that makes of step is added drop-wise in the synthetic water-base resin, and then adding film coalescence aid, silicon-dioxide, coupling agent, wetting agent, defoamer and flow agent, stirred 10～30 minutes, and can obtain finished product.
6. the preparation method of aqueous glass heat insulation paint as claimed in claim 5, it is characterized in that: the water that adds the described weight part of claim 1 is in process of production adjusted the viscosity of described coating.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008100237083A CN101265031A (en) | 2008-04-18 | 2008-04-18 | Aqueous glass heat insulation paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CNA2008100237083A CN101265031A (en) | 2008-04-18 | 2008-04-18 | Aqueous glass heat insulation paint and preparation method thereof |
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| CN101265031A true CN101265031A (en) | 2008-09-17 |
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Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101851068A (en) * | 2010-06-12 | 2010-10-06 | 重庆龙者低碳环保科技有限公司 | Method for spraying and coating heat insulation film on surface of glass |
| CN102020896A (en) * | 2010-12-10 | 2011-04-20 | 湖南福湘木业有限责任公司 | Environmental-protection coating and preparation method thereof |
| CN102061117A (en) * | 2010-12-06 | 2011-05-18 | 上海奇鸣涂料有限公司 | Coating composition coated on glass surfaces and preparation method thereof |
| CN102311688A (en) * | 2011-07-26 | 2012-01-11 | 深圳佳德威油漆有限公司 | Aqueous transparent heat insulation paint and its preparation method |
| CN102363934A (en) * | 2011-06-30 | 2012-02-29 | 上海乘鹰新材料有限公司 | Environmentally-friendly quick drying aqueous glass imitation card transfer paint and preparation method as well as application thereof |
| CN101838107B (en) * | 2009-03-20 | 2012-03-21 | 深圳市奥迪博士科技有限公司 | Toughened glass heat-insulation transparent high-temperature dielectric paste and manufacturing method thereof |
| CN102559024A (en) * | 2010-12-30 | 2012-07-11 | 海洋化工研究院 | Aqueous polyurethane heat reflection coating and application thereof |
| CN102618134A (en) * | 2012-04-10 | 2012-08-01 | 江苏思力玻璃科技有限公司 | Water-based glass heat insulation paint |
| CN103351757A (en) * | 2013-07-02 | 2013-10-16 | 浙江大学 | Water-based transparent heat-insulating paint used for energy-saving doors and windows and preparation method thereof |
| CN103740190A (en) * | 2013-12-30 | 2014-04-23 | 北京京能恒基新材料有限公司 | Rare earth nano high-transparency glass insulating coating and preparation method thereof |
| CN104496199A (en) * | 2015-01-10 | 2015-04-08 | 陈霞 | Preparation method of tempered glass for vehicles |
| CN105086810A (en) * | 2015-08-14 | 2015-11-25 | 芜湖真空科技有限公司 | Surface coating material composition as well as preparation method and application thereof |
| CN105331217A (en) * | 2015-12-02 | 2016-02-17 | 长沙民德消防工程涂料有限公司 | Water-borne environment-friendly, anti-flaming and heat-insulating paint and preparation method thereof |
| CN106336797A (en) * | 2016-08-30 | 2017-01-18 | 开平市日固力涂料有限公司 | High-temperature-resistant heat insulation coating |
| CN106543794A (en) * | 2016-05-06 | 2017-03-29 | 刘秋雷 | A kind of multifunctional nano composite coating |
| CN108410338A (en) * | 2018-03-19 | 2018-08-17 | 佛山市领浩科技有限公司 | A kind of aqueous high high transparent glass insulating moulding coating and preparation method thereof firmly |
| CN110128919A (en) * | 2018-02-02 | 2019-08-16 | 孙正宇 | Insulating moulding coating and its manufacturing method |
| WO2022088114A1 (en) * | 2020-10-30 | 2022-05-05 | 河北比尔尼克新材料科技股份有限公司 | Water-based paint special for glass substrates and preparation method therefor |
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2008
- 2008-04-18 CN CNA2008100237083A patent/CN101265031A/en active Pending
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| CN101838107B (en) * | 2009-03-20 | 2012-03-21 | 深圳市奥迪博士科技有限公司 | Toughened glass heat-insulation transparent high-temperature dielectric paste and manufacturing method thereof |
| CN101851068A (en) * | 2010-06-12 | 2010-10-06 | 重庆龙者低碳环保科技有限公司 | Method for spraying and coating heat insulation film on surface of glass |
| CN101851068B (en) * | 2010-06-12 | 2012-07-18 | 重庆龙者低碳环保科技有限公司 | Method for spraying and coating heat insulation film on surface of glass |
| CN102061117A (en) * | 2010-12-06 | 2011-05-18 | 上海奇鸣涂料有限公司 | Coating composition coated on glass surfaces and preparation method thereof |
| CN102020896A (en) * | 2010-12-10 | 2011-04-20 | 湖南福湘木业有限责任公司 | Environmental-protection coating and preparation method thereof |
| CN102559024A (en) * | 2010-12-30 | 2012-07-11 | 海洋化工研究院 | Aqueous polyurethane heat reflection coating and application thereof |
| CN102363934A (en) * | 2011-06-30 | 2012-02-29 | 上海乘鹰新材料有限公司 | Environmentally-friendly quick drying aqueous glass imitation card transfer paint and preparation method as well as application thereof |
| CN102311688A (en) * | 2011-07-26 | 2012-01-11 | 深圳佳德威油漆有限公司 | Aqueous transparent heat insulation paint and its preparation method |
| CN102311688B (en) * | 2011-07-26 | 2013-05-22 | 深圳佳德威油漆有限公司 | Aqueous transparent heat insulation paint |
| CN102618134A (en) * | 2012-04-10 | 2012-08-01 | 江苏思力玻璃科技有限公司 | Water-based glass heat insulation paint |
| CN103351757A (en) * | 2013-07-02 | 2013-10-16 | 浙江大学 | Water-based transparent heat-insulating paint used for energy-saving doors and windows and preparation method thereof |
| CN103351757B (en) * | 2013-07-02 | 2015-09-16 | 浙江大学 | For the water transparent heat insulation paint and preparation method thereof of energy saving door and window |
| CN103740190A (en) * | 2013-12-30 | 2014-04-23 | 北京京能恒基新材料有限公司 | Rare earth nano high-transparency glass insulating coating and preparation method thereof |
| CN103740190B (en) * | 2013-12-30 | 2016-04-13 | 北京京能恒基新材料有限公司 | A kind of rare earth nano insulating mold coating for high-transparent glass and preparation method thereof |
| CN104496199A (en) * | 2015-01-10 | 2015-04-08 | 陈霞 | Preparation method of tempered glass for vehicles |
| CN105086810A (en) * | 2015-08-14 | 2015-11-25 | 芜湖真空科技有限公司 | Surface coating material composition as well as preparation method and application thereof |
| CN105331217A (en) * | 2015-12-02 | 2016-02-17 | 长沙民德消防工程涂料有限公司 | Water-borne environment-friendly, anti-flaming and heat-insulating paint and preparation method thereof |
| CN105331217B (en) * | 2015-12-02 | 2018-04-03 | 长沙民德消防工程涂料有限公司 | Aqueous, environmental protective flame-retardant and thermal-insulated coating and preparation method thereof |
| CN106543794A (en) * | 2016-05-06 | 2017-03-29 | 刘秋雷 | A kind of multifunctional nano composite coating |
| CN106336797A (en) * | 2016-08-30 | 2017-01-18 | 开平市日固力涂料有限公司 | High-temperature-resistant heat insulation coating |
| CN110128919A (en) * | 2018-02-02 | 2019-08-16 | 孙正宇 | Insulating moulding coating and its manufacturing method |
| CN108410338A (en) * | 2018-03-19 | 2018-08-17 | 佛山市领浩科技有限公司 | A kind of aqueous high high transparent glass insulating moulding coating and preparation method thereof firmly |
| WO2022088114A1 (en) * | 2020-10-30 | 2022-05-05 | 河北比尔尼克新材料科技股份有限公司 | Water-based paint special for glass substrates and preparation method therefor |
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Open date: 20080917 |