CN101239098B - Inclusion peppermint oil and manufacture method thereof - Google Patents
Inclusion peppermint oil and manufacture method thereof Download PDFInfo
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- CN101239098B CN101239098B CN2008100694680A CN200810069468A CN101239098B CN 101239098 B CN101239098 B CN 101239098B CN 2008100694680 A CN2008100694680 A CN 2008100694680A CN 200810069468 A CN200810069468 A CN 200810069468A CN 101239098 B CN101239098 B CN 101239098B
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- oleum menthae
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- sucrose ester
- volatile oil
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Abstract
The invention provides a coated mint oil and the production thereof, characterized in that the oil coated by emulsifier comprises by weight: 1 parts of mint oil, 0.4 to 0.6 parts of sucrose ester S-15, 1 to 1.8 parts of purified water. Comparing to the prior art similar products, the invention is capable of ensuring the quality and effectiveness of products during the available period, with a greatly reduced production cost, a simple production process and an easy operation.
Description
Technical field
The present invention relates to a kind of Oleum menthae that is wrapped and preparation method thereof.
Background technology
The volatile oil that Oleum menthae promptly extracts from mint plants is the usual component in the Chinese medicine preparation.Present pharmaceutical industry normally directly extracts volatile oil with Oleum menthae and is used as medicine from mint plants, but because Oleum menthae is wanted evaporable characteristics in the preservation process, makes its medicine that contains constituent of peppermint oil can not guarantee its quality and curative effect before the deadline.The loss of constituent of peppermint oil also has Oleum menthae is handled in the medicine, be used as medicine after adopting beta cyclodextrin with the Oleum menthae parcel, but its manufacturing cost increases greatly.
Summary of the invention
Purpose of the present invention just is to provide a kind of volatilization that can prevent constituent of peppermint oil in the medicine effectively guaranteeing its drug quality and curative effect, and the Oleum menthae that is wrapped of low cost of manufacture.
Another object of the present invention provides the preparation method of the Oleum menthae of this parcel.
The object of the present invention is achieved like this: a kind of Oleum menthae that is wrapped is characterized in that it is the Oleum menthae that forms the emulsifying parcel.
The Oleum menthae of above-mentioned emulsifying parcel is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-150.4～0.6, purified water 1.0～1.8.
The volatile oil of above-mentioned raw materials Oleum menthae for from mint plants, extracting.
The another object of the present invention i.e. preparation method of the Oleum menthae of this parcel is: at first the sucrose ester S-15 in the said ratio is placed container, the purified water that adds again in the said ratio stirs, add at last after Oleum menthae in the said ratio stirs 45～60 minutes in the lump, place and got final product in 10～16 hours.
The volatile oil of above-mentioned raw materials Oleum menthae for from mint plants, extracting.
The above-mentioned volatile oil that extracts from mint plants is that mint plants is added the volatile oil that water distillation and extraction obtained after 2～4 hours.
The above-mentioned distillation extraction time is preferably 3 hours, and the ratio of mint plants and water is 1: 6～10 in the distillation extraction.
The invention has the beneficial effects as follows: (1) the present invention comes Oleum menthae is handled by the sucrose ester S-15 that adds suitable proportioning in Oleum menthae, to prevent the loss of Oleum menthae in the preservation process.Sucrose ester S-15 is an oil-in-water emulsifiers, has emulsifiability, when it and Oleum menthae mix homogeneously and after placing a period of time, because a kind of physics chemical action each other, the molecule of Oleum menthae and the molecule of sucrose ester S-15 closely are embedded in together, form so-called emulsifying parcel, this parcel relatively more can prevent Oleum menthae simple physics parcel the volatilization of Oleum menthae effectively with beta cyclodextrin.(2) inventor will carry out a large amount of contrast experiments with beta cyclodextrin parcel Oleum menthae in the present invention and the prior art, its comparing result is: sucrose ester S-15 consumption is few among the present invention, and consumption only is 0.4～0.6 times of Oleum menthae, and price is low, its price is 12 yuan/kg, and processing technology is simple; If adopt the beta cyclodextrin parcel, its consumption is that 20～25 times of ability of Oleum menthae are all wrapped up, and beta cyclodextrin price height, and its price is 85 yuan/kg; Use beta cyclodextrin packing technology complexity in addition, man-hour, consumption was big.So both relatively, the present invention has not only saved cost greatly, and effect is good, and the volatilization that can prevent constituent of peppermint oil in the medicine effectively is to guarantee its drug quality and curative effect.(3) Oleum menthae of the Oleum menthae that will not wrap up respectively of the inventor, product of the present invention and beta-schardinger dextrin-parcel is made silver-colored bavin granule by identical proportioning, according to WS
3-B-2612-97 standard detects, and it the results are shown in Table 1.
The effect of table 1 the present invention and prior art relatively
In a word, product of the present invention and preparation method that a large amount of practices by the inventor obtain, compare with like product of the prior art, not only guaranteed product of the present invention quality and curative effect before the deadline, and reduced its production cost widely, its production technology is simple, easy to operate simultaneously.
The specific embodiment
Mode below by embodiment further specifies the present invention, does not therefore limit the present invention among the described scope of embodiments.
Embodiment 1
A kind of Oleum menthae that is wrapped is characterized in that it is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.4, purified water 1.0.
Its preparation method is: at first be that the sucrose ester S-15 in the said ratio is placed container, the purified water that adds again in the said ratio stirs, and adds at last after Oleum menthae in the said ratio stirs 45 minutes in the lump, places to get final product in 12 hours.
Embodiment 2
A kind of Oleum menthae that is wrapped is characterized in that it is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.5, purified water 1.2.
Its preparation method is:
At first from mint plants, extract volatile oil, its extraction step is: get the Herba Menthae medical material and put in the multi-function extractor, the drinking water that adds 8 times of amounts of medical material, open Steam Heating, carry out distillation extraction 3 hours, and collected distillate, put calm putting, separation obtains the upper strata oily mater and is above-mentioned Oleum menthae, and is standby;
Sucrose ester S-15 in the said ratio is placed container, and the purified water that adds again in the said ratio stirs, and adds after Oleum menthae stirs 60 minutes in the lump by said ratio at last, places to get final product in 10 hours:
Embodiment 3
A kind of Oleum menthae that is wrapped is characterized in that it is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.6, purified water 1.4.
Before this sucrose ester S-15 in the said ratio was placed container headed by its preparation method, the purified water that adds again in the said ratio stirs, and adds at last after Oleum menthae in the said ratio stirs 55 minutes in the lump, places to get final product in 16 hours
Embodiment 4
A kind of Oleum menthae that is wrapped is characterized in that it is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.45, purified water 1.6.
Its preparation method is with embodiment 1.
Embodiment 5
A kind of Oleum menthae that is wrapped is characterized in that it is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.55, purified water 1.8.
Its preparation method is with embodiment 2.
Claims (6)
1. Oleum menthae that is wrapped, it is the Oleum menthae of the emulsifying parcel that forms, it is characterized in that the Oleum menthae of described emulsifying parcel is made by the following weight parts proportion raw material: Oleum menthae 1, sucrose ester S-15 0.4～0.6, purified water 1.0～1.8.
2. the Oleum menthae that is wrapped as claimed in claim 1, the volatile oil of wherein said raw material Oleum menthae for from mint plants, extracting.
3. the preparation method of the Oleum menthae that is wrapped as claimed in claim 1, it is characterized in that at first the sucrose ester S-15 in the described proportioning being placed container, the purified water that adds again in the described proportioning stirs, add at last after Oleum menthae in the described proportioning stirs 45～60 minutes in the lump, place and got final product in 10～16 hours.
4. the preparation method of the Oleum menthae that is wrapped as claimed in claim 3, the volatile oil of wherein said raw material Oleum menthae for from mint plants, extracting.
5. the preparation method of the Oleum menthae that is wrapped as claimed in claim 4, the wherein said volatile oil that extracts from mint plants is that mint plants is added the volatile oil that water distillation and extraction obtained after 2～4 hours.
6. the preparation method of the Oleum menthae that is wrapped as claimed in claim 5, the wherein said distillation extraction time is 3 hours, the ratio of mint plants and water is 1: 6～10 in the distillation extraction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2008100694680A CN101239098B (en) | 2008-03-13 | 2008-03-13 | Inclusion peppermint oil and manufacture method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2008100694680A CN101239098B (en) | 2008-03-13 | 2008-03-13 | Inclusion peppermint oil and manufacture method thereof |
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| Publication Number | Publication Date |
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| CN101239098A CN101239098A (en) | 2008-08-13 |
| CN101239098B true CN101239098B (en) | 2011-01-26 |
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| CN2008100694680A Active CN101239098B (en) | 2008-03-13 | 2008-03-13 | Inclusion peppermint oil and manufacture method thereof |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107854516A (en) * | 2017-10-24 | 2018-03-30 | 安徽恒达药业有限公司 | A kind of preparation technology of the peppermint oil with slow release |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
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2008
- 2008-03-13 CN CN2008100694680A patent/CN101239098B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
Non-Patent Citations (7)
| Title |
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| JP平5-7766A 1993.01.19 |
| Pablo Monllor et al..Characterization of the behaviour of flavour microcapsulesincotton fabrics.European Polymer Journal 43.2007,(43),2481-2490. |
| Pablo Monllor et al..Characterization of the behaviour of flavour microcapsulesincotton fabrics.European Polymer Journal 43.2007,(43),2481-2490. * |
| 丁燕飞等.薄荷油乙基纤维素微囊的制备.湖南中医学院学报23 3.2003,23(3),21-22. |
| 丁燕飞等.薄荷油乙基纤维素微囊的制备.湖南中医学院学报23 3.2003,23(3),21-22. * |
| 陈玉霞等.薄荷油的胶束增溶体系.无锡轻工大学学报20 3.2001,20(3),238-242. |
| 陈玉霞等.薄荷油的胶束增溶体系.无锡轻工大学学报20 3.2001,20(3),238-242. * |
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| CN101239098A (en) | 2008-08-13 |
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Owner name: TIANSHENG PHARMACEUTICAL GROUP CO., LTD. Free format text: FORMER NAME: CHONGQING TIANSHENG PHARMACEUTICAL CO., LTD. |
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| CP01 | Change in the name or title of a patent holder |
Address after: Chaoyang Industrial Park, 408300 Chongqing County of Dianjiang city (Dianjiang Guixi) Patentee after: Tiansheng Pharmaceutical Group Co., Ltd. Address before: Chaoyang Industrial Park, 408300 Chongqing County of Dianjiang city (Dianjiang Guixi) Patentee before: Chongqing Tiansheng Pharmaceutical Co., Ltd. |