CN101235074A

CN101235074A - Device for continuously producing polypeptide series products

Info

Publication number: CN101235074A
Application number: CNA2008100838437A
Authority: CN
Inventors: 胡红湘
Original assignee: Individual
Current assignee: Individual
Priority date: 2008-03-04
Filing date: 2008-03-04
Publication date: 2008-08-06

Abstract

The invention relates to a combination continuous production equipment for using polypeptide protein solution as raw material to produce polypeptide protein powder and polypeptide serial oleoyl chloride carboxylate surface activator, which can be controlled by a microprocessor or an industrial control computer, to form a continuous product line with the functions as automatic feeding, discharging and automatic start with presetting ability, belonging to chemical industry machinary and electromechanical automation industry, with wide application for the continuous combination production in the synthesis fields of adding layer, condensation and modification on variable surface activators.

Description

The device that a kind of polypeptide series products serialization is produced

Technical field

The present invention relates to polypeptide protein liquid is a kind of device of raw material production polypeptide albumen powder and polypeptide series carboxylate surface active agent, particularly protein powder and carboxylate salt two series products production equipments are arranged to the device of combination producing by microprocessor or industrial PC control, form two autofeeds of one＜font, discharging, the automatic continuous production line that starts the production technique that presets, belong to chemical industry machine commandment electromechanical industries, what can be applicable to tensio-active agent widely adds synthetic fields such as layer, condensation, modification.

Background technology

The production equipment of existing polypeptide albumen powder and polypeptide series carboxylate surface active agent all is the production equipment of intermittence or semi-batch, particularly polypeptide albumen powder and polypeptide series carboxylate surface active agent are subordinate to the chemical industry of two different field in main application fields, all be the individuality of independent production and operation separately at present, so two is mutually disjunct batch production device independently separately substantially, especially polypeptide oleoyl chloride series carboxylate surface active agent is produced masterbatch 1 polypeptide protein liquid, the machine commandment equipment configuration aspect of masterbatch 2 oleoyl chlorides and final product, traditional device aspect mainly is the masterbatch 1 production reactor that band stirred and be equipped with simple machine commandment tensimeter and thermometer at present, pressure filter, the decalcification separatory still that band stirs, band stirs and the masterbatch 2 of reliever is produced hold concurrently separatory still or establish storage branch flow container in addition of reactors, final product production human metering respectively drops into masterbatch 1, masterbatch 2 and stone, the meter material of several procedures before and after the equipment configuration, feed intake, save, it all is pure artificial periodical operation that each batch production is packed in discharging, and production efficiency and total productivity effect are all on the low side.

Summary of the invention

Purpose of the present invention: be for addressing the above problem, provide a kind of with polypeptide protein liquid production link, protein powder production link, oleoyl chloride production link, polypeptide oleoyl chloride carboxylic acid salinization production link by pipeline, electrical element and CPU control mainboard each link is connected to form＜two serializations of font control a kind of device of production line automatically, when improving production stability and product quality, reduce comprehensive cost, enhance productivity, to obtain best economy and comprehensive benefit.

The technical scheme of implementing this invention is: with the production of traditional polypeptide protein liquid, save link, the protein powder production link, oleoyl chloride production, save link, the several relatively independent batch production operations of link are produced, are saved in the salinization of polypeptide oleoyl chloride carboxylic acid, by pipeline, electrical element and instrument, with each link by the requirement of production technique carry out machine commandment, electromechanics connects comprehensively, control by built-in CPU control chip, preferably control the device of two automatic continuous productions forming one＜font by industrial computer.

Wherein polypeptide protein liquid production link with save in the link, increase by two separatory settling tank or jars that have the liquid level probe ball, and separatory is installed respectively at separatory settling tank place is extracted measuring apparatus and start automatically and automatically controlledly warn facility with machine and be connected, the input terminus of settling tank carries out automatically controlled the commandment with machine with protein liquid production output terminal and is connected, extracting facility carries out automatically controlled the commandment with machine respectively and is connected with the facility incoming line of saving that has liquid level indication probe polypeptide protein liquid work piece, then polypeptide Amino acid work piece are saved facility outlet line and protein powder purification facility, the drying facility incoming line connects, and carries out automatically controlled the commandment with machine with the incoming line of polypeptide oleoyl chloride carboxylate salt production facility simultaneously and is connected.

Increase tail gas purification facility and layering liquid separatory are saved device and dose part flow arrangement in the oleoyl chloride production link, and be respectively equipped with to reclaim and save facility, the tail gas refined product is saved the facility outlet line and polypeptide amido acid solution production facility raw material input terminus carries out pipeline and electric, electricly connect, layering liquid reclaimed save the facility output terminal and still kettle input terminus circuit carries out pipeline and electric, electricly connect, the facility outlet line of saving that the final product production facility raw material input terminus and the oleoyl chloride product of polypeptide oleoyl chloride carboxylate salt are saved facility output terminal and polypeptide Amino acid work piece carries out pipeline and electric afterwards, electricly connect.

The subregion production arranged side by side of polypeptide oleoyl chloride carboxylic acid salinization production link and protein powder production link, raw material input end is saved jar output terminal with polypeptide protein liquid respectively and is carried out automatically controlled and machine commandment and be connected, the production of shared polypeptide protein liquid with save a jar resource, in order to improve efficient and the cycle rate that serialization is produced.

Above-mentioned all work piece and final product are saved jar and are all vacuumized channel selector, built-in pressurization washing equipment and warm air blow-dry device preferably are installed, what guarantee when ensuring the quality of products when guaranteeing life-time service that serialization produces carries out smoothly, and wherein the jar of saving of polypeptide protein mother liquor preferably is provided with thermostat.

Above-mentioned all precipitation liquid pools and save jar built-in biliquid position probe all is installed, when full liquid liquid level that the liquid level probe ball arrive to be set, the automatically controlled last procedure output liquid program that is connected will be closed automatically, when minimum liquid level that the liquid level probe ball arrive to be set, will start automatically pipeline with automatically controlled be connected on the metering production process that feeds intake together, above-mentioned all precipitation liquid pools all are equipped with the separatory flow apparatus.

Be separately installed with electric device on the connection line of above-mentioned all devices by central controller controls, above-mentioned all reactor raw material input terminus circuits all have electromagnetic valve, time, pressure, temperature, the flow electric control gear of installing by manufacturing technique requirent, and above-mentioned control electric device is preferably controlled by the industrial computer on-line operation.

Described central controller or industrial PC onboard motherboard have pressurization decompression driving circuit, automatic gauge display circuit, the temperature control display circuit, the pressure display circuit, time control display circuit, pressurized water and warm air start-up control circuit, PH tests display circuit, the production of polypeptide protein liquid, save pilot circuit, protein powder production control circuit, is saved pilot circuit at amine hydroxybenzene production, the production of polypeptide oleoyl chloride carboxylate salt, save, the discharging pilot circuit.

Feed intake and the discharging pilot circuit of above-mentioned each production link reactor are electrically connected with the signal input part of drawdown pump and force (forcing) pump startup channel selector and electromagnetic valve group respectively, and drawdown pump and force (forcing) pump start the channel selector signal output part and be electrically connected with the pressure display circuit.

The temperature signal output terminal of reactor is electrically connected with the temperature display circuit signal input part in above-mentioned each production link, and the time control signal output terminal is electrically connected with the time display circuit signal input part.

Wherein the polypeptide protein liquid pilot circuit of saving jar input terminus is electrically connected with the liquid level probe ball signal input part in polypeptide protein liquid precipitate pond, the pilot circuit of saving jar output terminal is purified with protein powder production respectively or dry link signal input part pilot circuit is electrically connected, simultaneously also with the raw materials for production input terminus pilot circuit electrical connection of polypeptide oleoyl chloride carboxylate salt.

The input terminus pilot circuit of polypeptide oleoyl chloride carboxylate salt production link raw material simultaneously and high-order alkaline agent hold hopper and amine hydroxybenzeneization and save the output terminal pilot circuit of facility and be electrically connected, the interior electrode bar of the signal input part of PH test display circuit and polypeptide oleoyl chloride carboxylate salt production equipment is electrically connected, and the polypeptide oleoyl chloride carboxylate salt output terminal pilot circuit that manufactures a finished product is electrically connected with the input terminus pilot circuit that final product is saved facility.

Operation process of the present invention is:

--semi-finished product 1 polypeptide amido acid solution the measure of production function, pressure-activated pattern and production model are set, and--starting production model 1---drawdown pump channel selector opens, and--reactor a sucks scurf or gelatin material, and----the drawdown pump channel selector cuts out, and-------start-up temperature automatic control and temporal mode 1--start discharging pattern 1---and start filter-pressing device, and------raw material is filtered in suction, and---the drawdown pump channel selector cuts out, and----------start-up temperature automatic control and temporal mode 2---start discharging pattern 2--startup separatory sedimentation basin function, and---startup layering separatory divides suction mode, and---save respectively polypeptide protein liquid semi-finished product 1--and start liquid level probe ball functional mode--starts aforementioned production model 1～2 to the startup steam cock to startup force (forcing) pump channel selector to A: manually the basic production raw material is saved respectively in the raw material accumulator tank automatically to start steam cock to start the force (forcing) pump channel selector to start limewash input valve or the sour valve of inputting to start production model 2---startup reactor b drawdown pump channel selector to suck limewash; Automatically stop to save pattern, form thus the production model A of automatic control serialization.

B: raw material is saved respectively in the raw material accumulator tank---semi-products 2 oleamide the measure of production functions, pressure-activated pattern and production model are set---start production model 4--drawdown pump switch opens---and reactor c sucks raw material 2--vavuum pump channel selector and closes--and start-up temperature automatic control and temporal mode 3--start the distilled pattern--stop the distilled pattern---(reactor d vavuum pump channel selector is opened--reactor c discharging switch opens--and the reactor d switch opens that feeds intake--the metering function on that feeds intake)--start-up temperature automatic control and temporal mode 4--start semi-products 2 discharging patterns---to be started the separating pool functional mode and--starts semi-products 2 and save functional mode (expand number represent this function can select) and--start liquid level probe ball functional mode and--close and save functional mode--and start aforementioned production model 4, form thus the production model B of automatic control serialization.

C: finished product 1 polypeptide oleoyl chloride carboxylic acid salinization the measure of production function, pressure-activated pattern and production model are set--startup production model 5--drawdown pump channel selector is opened, and---metering feeds intake, and--reactor d sucks semi-finished product 1 material, and----the drawdown pump channel selector cuts out, and--startup quantitative model 2--starts the PH potential testing device, and------startup finished product 1 is saved device, and--head tank suction alkaline agent--is closed and is saved functional mode--and start aforementioned production model 5, forms thus the production model C of automatic control serialization to start the discharging pattern for start-up temperature automatic control and temporal mode 4--suction semi-finished product 2 material in pattern 1 startup by startup liquid level probe ball functional mode.

--startup production model 6---drawdown pump channel selector is opened--suction work in-process 1 material (startup of purification pattern)--flow functions/drying startup--startup of discharging pattern---packaging final prod 2 to D: final product 2 polypeptide albumen powders are set produce metered flow function, drying temperature and production or purification pattern.

According to the serialization automatic production line that the technical program realizes, can be widely used in the serialization production that adds layer, modification production of various surfactants.

Adopt the advantage and the beneficial effect of this invention technology to be:

Effectively reduced raw material and occupation of land is held in the final product storehouse, saving of liquid half product and liquid final product adopts vacuum to save the quality guarantee period that device has effectively prolonged product, pressing the configuration of same capability reactor compares, adopt this contrive equipment to put into production, the disposable fund input of production equipment of equipment funds input ratio traditional way increases about 1 times, throughput increases more than 4 times than conventional apparatus, the full production output value increases more than 4 times than conventional apparatus, labour intensity descends 2～3 times than conventional apparatus, and equal rate ratio descends about 2～3 times than the unit cost of production.

Embodiment

The mode that the present invention gives an example now more specifically in conjunction with the drawings illustrates, the present invention is further described below in conjunction with accompanying drawing and embodiment, and this embodiment does not limit use range of the present invention.

Figure one is a mounting arrangement structural representation of the present invention.

Figure two is controller circuit structure synoptic diagram of the present invention.

Shown in figure one, two, the present invention sets and is made up of five workspaces, A

district

1,2, the 3rd, and raw material are deposited Hold tank, each saves the liquid level charactron that tank has external transparent material pipe; This part is substantially by manually-operated.

B district a, b produce reactor for polypeptide protein liquid, the even commissioning pipe that electromagnetic valve control is arranged of pan feeding port All there are flow instrument, pressurization 19, decompression 18 path electric control gears in the road on the pipeline, and is communicated with

raw material

1,20, Wherein a still discharge end is communicated with pressure filter 12 by electromagnetic valve 27, and pressure filter 12 discharging ports are by electricity Magnet valve door 28 is communicated with reactor b pan feeding port, reactor b discharging control port by electromagnetic valve 29, 30 are communicated with respectively with the sedimentation basin 4 that is built-in with level probe, 5 charging ports, and with

sedimentation basin

4,5 full Liquid indication port is electrically connected, and

sedimentation basin

4,5 discharging ports are provided with separatory indicator for flow rate 31, and respectively Be communicated with 6,7 by electromagnetic valve with semi-finished product 1

accumulator tank

6,7 that is built-in with level probe and decompressor Full liquid level indication port be electrically connected

accumulator tank

6,7 minimum with

sedimentation basin

4,5 discharging control ports Liquid level indication port starts control circuit with the production of reactor a, b and is electrically connected.

Sedimentation basin

4,5 during work When liquid level reaches the highest full liquid level indicating bit, reactor b discharging control port discharge end switch autoshutdown, Reactor b production routine stops automatically, and following reaction still a production routine stops automatically, the time of setting

Interior accumulator tank

6,7 decompression paths, 18 switch opens of automatically starting start automatic gauge and save function, hold material Tank 6, when 7 liquid levels reach the highest liquid level indicating bit, decompression path 18 switches cut out, and extract metering and save merit Can autoshutdown, accumulator tank 6, when 7 liquid levels reach the minimum liquid level indicating bit, reactor a produces start-up routine Automatically start, reactor b produces start-up routine and automatically starts subsequently the repetitive cycling aforementioned functional.

Its working process is: work in-process 1 polypeptide protein liquid function of measuring is set,------reactor a sucks scurf or gelatin material, and--suction liming 20--drawdown pump path 18 switches cut out, and------start-up temperature automatic control and temporal mode 1--startup discharging pattern 1---start filter-pressing device 12---startup production model 2---startup reactor b drawdown pump path 18 switches, and----drawdown pump path 18 switches cut out--starts liming and imports valve or sour input valve--start-up temperature automatic control that startup force (forcing) pump path 19 switches--start steam cock--and temporal mode 2---startup discharging pattern 2--startup separatory settling tank 4 to startup force (forcing) pump path 19 switch opens to the startup function of measuring to suck the filtration raw material to start steam cock to start production model 1---drawdown pump path 18 switch opens for pressure-activated pattern and production model,--start layering liquid divides suction branch row pattern--to start the pattern of saving--respectively at 6 to 5 functions, save polypeptide protein liquid work in-process 1--in 7 and start level probe deixis pattern--return startup automatically and repeat

aforementioned production model

1,2.

C district c, d is an amine hydroxybenzene production reactor, respectively with No. 2, No. 3 raw material is communicated with, wherein the d still is equipped with tail gas purification facility 32 and saves jar 11, save jar 11 discharge ends by electromagnetic valve 33,34 respectively with reactor a, b pan feeding control port carries out pipe connection and electrical connection, make to regulate PH or cleaning function usefulness, and reactor d discharging port is by electromagnetic valve 35,36 save branch flow container 8 with the work piece 2 that are built-in with level probe respectively, 9 connect, save branch flow container 8,9 full liquid level indication ports are electrically connected with reactor d discharging control port, minimum liquid level indication port is produced the start-up routine pilot circuit with reactor d and is electrically connected, save branch flow container 8,9 discharging ports are by electromagnetic valve 37,38 save jar 10 with separatory indicator for flow rate 39 and parting liquid is connected, and the port of discharging simultaneously carries out pipe connection by pipeline 40 and electromagnetic valve 41 with reactor g pan feeding control port and is electrically connected.

Its course of work is: semi-products 2 oleamide the measure of production functions, pressure-activated pattern and production model are set---start production model 3--drawdown pump path 18 switch opens---and reactor c sucks raw material 2--vavuum pump path 18 switches and closes--and start-up temperature automatic control and temporal mode 3--start the distilled pattern--stop the distilled pattern---(reactor d vavuum pump channel selector is opened--reactor c discharging switch opens--and the reactor d switch opens that feeds intake--the metering function on that feeds intake)--start-up temperature automatic control and temporal mode 4--start semi-products 2 discharging patterns, and-------starting semi-products 2 saves functional mode (expand number represent this function can select)--starting level probe deixis pattern---auto-returned and starts and also repeat aforementioned production model 3～4 to start metering separatory discharge mode to start the separating pool functional mode.

D district g is that reactor is produced in the salinization of polypeptide oleoyl chloride carboxylic acid, and e, f are that protein powder is purified, moisture eliminator; Wherein reactor g pan feeding control port by electromagnetic valve 41,42 and flow instrument respectively with the discharging control port that holds batch can 6,7 of work piece 1, the discharging control port 40 of saving jar 8,9 of work piece 2 carries out pipe connection and electrical connection, and is electrically connected with the minimum liquid level indication pilot circuit of saving

jars

6,7,8,9 respectively, reactor g stops production sequence automatically when saving the minimum indication flow of any one liquid level of jar and do not reach the flow that reactor g presets; Reactor g discharge port holds batch can 15,16 through strainer 13 with the final product 2 that is built-in with level probe and is communicated with, full liquid level indication port is electrically connected with reactor g discharging control port, and minimum liquid level indication port is produced the start-up routine pilot circuit with reactor g and is electrically connected; E is the protein powder purifier, holds batch can 6,7 by electromagnetic valve and work piece 1 and is communicated with, and f is a moisture eliminator.

Present technique is a kind of collection automatic charging, discharging, saves, and starts processing sequence at regular time and quantity in one and the automated installation produced by the serialization of microprocessor or industrial PC control,

Its working process is:

1, final product 1 polypeptide oleoyl chloride carboxylic acid salinization is set produces function of measuring,--startup production model 5--drawdown pump channel selector is opened, and--metering feeds intake, and--reactor d sucks work in-process 1 material, and--the drawdown pump channel selector cuts out 6--and starts the PH potential testing device, and--------start final product 1 and save device--starting level probe deixis pattern--returns startup and repeats aforementioned production model 5 startup discharging pattern automatically to suck work in-process 2 material and alkali for start-up temperature automatic control and temporal mode 4--startup quantitative model in pattern 5 startups for pressure-activated pattern and production model.

2,--startup production model 6---drawdown pump channel selector is opened--suction work in-process 1 material (startup of purification pattern)--flow functions/drying startup--startup of discharging pattern---packaging final prod 2 final product 2 polypeptide albumen powders production metered flow function, drying temperature and production or purification pattern to be set

E

district

15,16 saves jar for final product polypeptide oleoyl chloride carboxylate salt, local area is saved jar and is provided with vacuum pump startup path and electrical means, the vacuum pump start-up control circuit of saving jar is electrically connected with reactor g discharging pilot circuit, save a jar Artificial Control discharging packing, wherein preferably select for use the electric pump stock to the transfer cask tank car, transport directly to the hold tank output products of user side by tank car.

Its working process is: pressure-activated pattern is set, and--startup final product 1 is saved device, and------starting level probe deixis pattern--returns startup automatically and repeats aforementioned production model 5 to close raw material input switch-Artificial Control electric pump stock to the transfer cask tank car to start level probe deixis pattern.

The above reactor a, b, c, d, e, g pan feeding port are equipped with flow instrument, be communicated with corresponding material channel respectively by electromagnetic valve on the flow instrument, pressurization 19 and decompression 18 passages that electromagnetic valve control is arranged respectively under the flow instrument, are saved jar and are separately installed with built-in pressurization washing equipment and warm air blow-dry device 26 above-mentioned all precipitation liquid pools.

Because above-mentioned communication processor; the route protection monitoring device; valve; pipeline; reactor and gauge and other protector etc. can use existing technology and equipment; therefore for the concrete formation of said apparatus; specification; model; necessity that the size of quantity and capacity etc. does not further describe; but those skilled in the art can be according to the present invention the technical scheme that limits of claim; technical data increases and decreases the specification of order and the quantity and the equipment thereof of some device and device; capacity etc. are made amendment, and these are revised all in the protection domain of claims of the present invention.

Claims

1, the device that a kind of polypeptide albumen powder and the serialization of polypeptide series carboxylate surface active agent are produced, it is characterized in that: with polypeptide protein mother liquor reactor, save link, protein powder production is purified, dry link, polypeptide series carboxylate surface active agent masterbatch 2 oleoyl chlorides are produced reactor, save link, polypeptide oleoyl chloride carboxylate surface active agent is produced reactor, save link, by producing, save, intermediate links and complete processing require to carry out the machine commandment, dynamo-electric connection comprehensively, and the production equipment of controlling by built-in CPU control chip, and preferably by industrial PC control formation two autofeeds of one＜font, discharging, automatically start the device of the serialization automatic production line of the production sequence that presets.

2, the device of a kind of polypeptide albumen powder and the serialization of polypeptide series carboxylate surface active agent production is characterized in that: polypeptide protein mother liquor reactor and polypeptide protein mother liquor are saved 1-2 separatory settling tank or jar between the link.

3, the automatic starting device of a kind of combination producing according to claim 2 is characterized in that:

(1) separatory settling tank or jar have biliquid position probe, and the high-order indicator signal of level probe is electrically connected with polypeptide protein liquid reactor raw material output terminal automatically controlled signal, and the low level indicator signal is produced the start-up routine signal with polypeptide protein liquid reactor and is electrically connected.

(2) separatory settling tank or jar have separatory metering and extract discharge equipment, and are electrically connected with input circuit signal that the polypeptide protein mother liquor is saved facility.

(3) the polypeptide protein mother liquor raw material output circuit signal of saving facility is electrically connected with the production start-up routine signal that reactor is produced in protein powder purification, drying and the salinization of polypeptide oleoyl chloride carboxylic acid respectively.

(4) the polypeptide protein mother liquor is saved facility and is provided with thermostat.

4, the device produced of a kind of polypeptide albumen powder and the serialization of polypeptide series carboxylate surface active agent is characterized in that: the production of 2 oleoyl chlorides of the masterbatch of polypeptide series carboxylate surface active agent, saves in the link,

(1) tail gas recycle of producing reactor is saved and is increased purifying plant in the link, and the output terminal of purification tail gas being saved link carries out the machine commandment with the reactor raw material input terminus of polypeptide protein mother liquor and is connected with electromechanics.

(2) jar of saving of oleoyl chloride finished product is provided with thermostat and built-in biliquid position probe, the high-order indicator signal of probe is produced reactor raw material output terminal automatically controlled signal with oleoyl chloride and is electrically connected, and the low level indicator signal is produced reactor start-up routine signal with oleoyl chloride and is electrically connected.

(3) the raw material output terminal of saving jar is electrically connected with the raw material input terminus and the production start-up routine signal of polypeptide series carboxylate surface active agent reactor.

5, the device of a kind of polypeptide albumen powder and the serialization of polypeptide series carboxylate surface active agent production, it is characterized in that: the link of saving of polypeptide series oleoyl chloride carboxylate surface active agent final product is provided with built-in biliquid position probe, the high-order indicator signal of probe is electrically connected with this production reactor raw material output terminal automatically controlled signal, and the low level indicator signal is produced the start-up routine signal with this production reactor and is electrically connected.

6, a kind of device according to claim 1, it is characterized in that: described built-in CPU control mainboard, mainboard comprises that polypeptide protein mother liquor, protein powder production, oleoyl chloride production, polypeptide oleoyl chloride carboxylic acid salinization production control touch piece, be respectively equipped with that piece is touched in signal input and piece is touched in signal output, each control is touched piece and is built-in with automatic gauge, temperature, pressure, time display and pilot circuit respectively.

7, the device of a kind of polypeptide albumen powder and the serialization of polypeptide series carboxylate surface active agent production, it is characterized in that: the jar of saving of all aqueous mother liquors, final product is equipped with built-in annular pressurization wash water pipeline and hot-air seasoning device, and all are saved jar and are equipped with and vacuumize path and electric control gear.