CN101167794A - Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof - Google Patents
Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof Download PDFInfo
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- CN101167794A CN101167794A CNA2007101579863A CN200710157986A CN101167794A CN 101167794 A CN101167794 A CN 101167794A CN A2007101579863 A CNA2007101579863 A CN A2007101579863A CN 200710157986 A CN200710157986 A CN 200710157986A CN 101167794 A CN101167794 A CN 101167794A
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Abstract
The invention discloses concentrated water-paste pills of poultice extract of deer foetus and process for preparation. The effective components of the concentrated water-paste pills are the following raw materials by weight ratio: fresh deer foetus 5-15, pilose antler 5-15, deer tail 5-15, unhairing deer testes and penis 5-10, leonurus japonicus 10-20, American ginseng 5-10, licorice 5-8, anoelica sinensis 5-10 and red ginseng 5-8, wherein leonurus japonicus, American ginseng, licorice, anoelica sinensis and red ginseng are boiled into medicament liquid, and fresh foetus, pilose antler, deer tail, unhairing deer testes and penis are charged into the medicament liquid and boiled into paste-like material and then the concentrated water-paste pills can be obtained through carbon dioxide supercritical extraction. The invention employs proportion of compatibility between monarch and ministerial drug of various materials and the concentrated water-paste pills are prepared through boiling, concentrating and carbon dioxide supercritical extracting. The water-paste pills are convenient to take and store, and furthermore appropriate all effective components of various materials can be extracted by the process for preparation. Compared with traditional poultice extract of deer foetus, the medicament-effect of the water-paste pills product is greatly enhanced and utilization ratio of medicament materials is increased.
Description
Technical field
The present invention relates to Chinese medicine health-care goods and preparation method thereof, especially a kind of with concentrated watered pill that forms of Embryo cervi paste and preparation method thereof.
Background technology
Embryo cervi is a kind of famous and precious Chinese crude drug, according to " Compendium of Materia Medica " record, has benefiting qi and nourishing blood, the regulating menstruation cold expelling, the kidney invigorating and essence nourishing, effects such as YIN nourishing skin care often are that primary raw material is prepared into Embryo cervi paste with the Embryo cervi, as the Chinese medicine product of directly taking, Embryo cervi paste is in the history of taking of existing centuries of China, also classified as big benefit treasure during the Qing Dynasty by imperial palace, among the people " god of unusual strength's medicine " or " big tonic " also arranged say that short-term is taken in a large number and caused " the getting angry " that it has often been said easily.Embryo cervi paste is owing to be the paste medicine, inconvenience when taking, preserve also oxidized easily, go mouldy; And because preparation technology's restriction, Embryo cervi paste fails the active ingredient of each crude drug is all extracted, and the Embryo cervi paste that causes like this making usually can't reach the effect of expection, has also caused the waste of crude drug simultaneously.Existing Chinese medicine product is also usually made pill, and it is taking convenience not only, and easily preserves.But, also there is situation easily oxidized, that go mouldy because medicinal raw materials self such as Embryo cervi directly adopt the existing method for preparing pill.
Summary of the invention
Goal of the invention: the invention provides a kind of Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof, its objective is that solve existing Embryo cervi tonic makes unguentum more, not only take inconvenience, also should not preserve for a long time, also cause " getting angry " easily, can not effectively extract the composition of crude drug, the problem of performance drug effect.
Technical scheme: the present invention is achieved through the following technical solutions:
A kind of Poultice extract of deer foetus concentrated water-paste pill, it is characterized in that: the effective ingredient of this concentrated watered pill is each raw material of following weight ratio: bright Embryo cervi 5～15, Cornu Cervi Pantotrichum 5～15, Cauda cervi 5～15, unhairing Penis et testis cervi 5～10, Herba Leonuri 10～20, Radix Panacis Quinquefolii 5～10, Radix Glycyrrhizae 5～8, Radix Angelicae Sinensis 5～10, Radix Ginseng Rubra 5～8, boil the medicinal liquid that obtains with Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra and add bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi and be brewed into paste, the concentrated watered pill of quenching and obtaining through CO 2 supercritical.
Described bright Embryo cervi is the Embryo cervi behind firm retention of dead fetus, that have amniotic fluid and the high temperature sterilization.
Described each raw-material preferred weight ratio is: bright Embryo cervi 10, Cornu Cervi Pantotrichum 8, Cauda cervi 7, unhairing Penis et testis cervi 6, Herba Leonuri 15, Radix Panacis Quinquefolii 6, Radix Glycyrrhizae 6, Radix Angelicae Sinensis 7, Radix Ginseng Rubra 6.
A kind of preparation method of Poultice extract of deer foetus concentrated water-paste pill as claimed in claim 1 is characterized in that: undertaken by following step:
Get bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi by the described weight ratio of claim 1, Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, each raw material of Radix Ginseng Rubra;
Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry post-heating to boil and obtains medicinal liquid;
The described bright Embryo cervi of adding, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi are brewed into the thickness paste in the medicinal liquid that obtains after boiling;
To pulverizing after the described thickness paste oven dry that obtains;
The material obtain is pulverized in oven dry packed in the extractor, feed CO2 gas from the extractor bottom, the control temperature is 33～70 ℃, and pressure is 25～55MPa, and the extraction time is 1～20 hour;
To extract that the thickness paste that reclaims adds water and edible adhesive is made the watered pill through granulator from extractor.
Describedly Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry heating boil the step that obtains medicinal liquid and comprise:
Adding the weight of entry and the ratio of each raw material gross weight is: 3～5: 1; Temperature when heating boils is: 60～80 ℃; Boil 0.5～5 hour time.
Describedly will add the edible binding agent that water and edible adhesive make the step of the watered pill through granulator from the thickness paste of extractor Separation and Recovery and comprise: the mixture of starch or starch and edible glue.
Describedly will add the step that water and edible adhesive make the watered pill through granulator from the material of extractor Separation and Recovery and comprise: the weight by every during the preparation watered pill is 1～2g, contains that to extract the back the effective elements of the medicine be 0.2～0.8g in every.
Advantage and effect: by the enforcement of technical solution of the present invention, can solve existing Embryo cervi medicine well and make unguentum more, not only take inconvenience, also should not preserve for a long time, and can not effectively extract the composition of crude drug, the problem of performance drug effect.The present invention is with the ratio of plurality of raw materials medicine the monarch and his subjects compatibility, and employing makes the watered pill through the critical mode of getting of quenching of carbon dioxide after boiling and concentrating again.Taking convenience not only, and be convenient to preserve, and this mode can almost all extract the active ingredient in each crude drug increases substantially the drug effect of the more traditional Embryo cervi paste of the watered pill goods that obtain, has also improved the utilization rate of raw material medicine.
The specific embodiment
The invention provides a kind of Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof, this concentrated watered pill mainly contains bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi, Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are pressed each raw material that certain weight ratio is formed, the medicinal liquid that boils with wherein Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra is brewed into paste with bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi, the concentrated watered pill of quenching and obtaining through CO 2 supercritical.The concentrate active ingredient of each crude drug of this concentrated watered pill makes its easier being absorbed by the body, and to endocrine regulation, improves body immunity, strengthens sexual function, and there is magical effect delaying female climacteric.And this watered pill volume is little, the nourishing healthy beautification product that taking convenience is the person in middle and old age man, the woman is best.
For ease of understanding, the present invention is specifically described below in conjunction with embodiment.
Embodiment 1:
The present invention is a kind of Poultice extract of deer foetus concentrated water-paste pill, mainly contain following raw material by weight forming: bright Embryo cervi 50g, Cornu Cervi Pantotrichum 50g, Cauda cervi 50g, unhairing Penis et testis cervi 50g, Herba Leonuri 200g, Radix Panacis Quinquefolii 100g, Radix Glycyrrhizae 80g, Radix Angelicae Sinensis 100g, Radix Ginseng Rubra 80g, the water that boils with Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra is brewed into paste with bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi, the concentrated watered pill of quenching and obtaining through CO 2 supercritical.
Concrete preparation method is:
Herba Leonuri in the crude drug, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry heating to boil and obtains medicinal liquid, amount of water is 3 times of each crude drug gross weight, promptly adds 2180g water, adopt 50 ℃ moderate heat to boil 1.5 hours after, with the medicinal residues filtering, obtain medicinal liquid;
The described bright Embryo cervi of adding, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi boil in the medicinal liquid that obtains after boiling, and become the thickness paste to be as the criterion with the material that obtains, and the heating-up temperature when boiling can be chosen between 50～80 ℃; Described bright Embryo cervi is the Embryo cervi behind firm retention of dead fetus, that have amniotic fluid and the high temperature sterilization.
The described thickness paste that obtains is dried, and pulverize with 100 orders the oven dry back;
The material obtain is pulverized in oven dry packed in the extractor, feed CO from the extractor bottom
2Gas, the control temperature is 33～70 ℃, and pressure is 25～55MPa, and the extraction time is 1～20 hour;
To add water from the thickness paste that extractor reclaims and make the watered pill as the starch of edible adhesive through granulator, and be black behind the described watered pill that obtains, the specification of preparation is: the active ingredient of per 1 intragranular pastille is 0.2g～1g.
Said method is not only simple, and has cheap, nontoxic, safe, advantage efficiently, almost the active ingredient of each crude drug all can be extracted, so the watered pill that makes is than traditional Embryo cervi unguentum taking convenience not only, and better effects if.Embryo cervi nutritive value behind the also high temperature sterilization just retention of dead fetus, that had amniotic fluid is high, is big tonic product, and unguentum is made in 5000～6000 yuan/of market price or pill is easy to corruption, and the edible easy again mouth and nose of short-term are given birth to and wrapped, flushing loss of hairs; And by the present invention with other ministerial drug balance, and make the watered pill of little metering, the people who just in time is fit to have a delicate constitution takes.
Embodiment 2:
Get each crude drug by following weight ratio: bright Embryo cervi 1000g, Cornu Cervi Pantotrichum 800g, Cauda cervi 700g, unhairing Penis et testis cervi 600g, Herba Leonuri 1500g, Radix Panacis Quinquefolii 600g, Radix Glycyrrhizae 600g, Radix Angelicae Sinensis 700g, Radix Ginseng Rubra 600g;
Herba Leonuri in the crude drug, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry heating to boil and obtains medicinal liquid, amount of water is 4 times of each crude drug gross weight, promptly adds 28400g water, adopt 65 ℃ moderate heat to boil 2 hours after, with the medicinal residues filtering, obtain medicinal liquid;
The described bright Embryo cervi of adding, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi boil in the medicinal liquid that obtains after boiling, and become the thickness paste to be as the criterion with the material that obtains, and the heating-up temperature when boiling can be chosen between 50～80 ℃;
The described thickness paste that obtains is dried, and pulverize with 80 orders the oven dry back;
The material obtain is pulverized in oven dry packed in the extractor, feed CO from the extractor bottom
2Gas, the control temperature is 33～70 ℃, and pressure is 25～55MPa, and the extraction time is 1～20 hour;
To add water from the material that extractor reclaims and make the watered pill as the edible adhesive edible glue through granulator, and be black behind the described watered pill that obtains, the specification of preparation is: the active ingredient of every intragranular pastille is 0.2g～1g, and the weight of every pill is 2g.
Embodiment 3:
Get each crude drug by following weight ratio: bright Embryo cervi 1500g, Cornu Cervi Pantotrichum 1500g, Cauda cervi 1500g, unhairing Penis et testis cervi 1000g, Herba Leonuri 1000g, Radix Panacis Quinquefolii 500g, Radix Glycyrrhizae 500g, Radix Angelicae Sinensis 500g, Radix Ginseng Rubra 500g;
Herba Leonuri in the crude drug, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry heating to boil and obtains medicinal liquid, amount of water is 5 times of each crude drug gross weight, promptly adds 42500g water, adopt 75 ℃ moderate heat to boil 3 hours after, with the medicinal residues filtering, obtain medicinal liquid;
The described bright Embryo cervi of adding, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi boil in the medicinal liquid that obtains after boiling, and become the thickness paste to be as the criterion with the material that obtains, and the heating-up temperature when boiling can be chosen between 50～80 ℃;
The described thickness paste that obtains is dried, and pulverize with 60 orders the oven dry back;
The material obtain is pulverized in oven dry packed in the extractor, feed CO from the extractor bottom
2Gas, the control temperature is 33～70 ℃, and pressure is 25～55MPa, and the extraction time is 1～20 hour;
To add water from the material that extractor reclaims and edible adhesive is made the watered pill through granulator, and be black behind the described watered pill that obtains, the specification of preparation is: the active ingredient of every intragranular pastille is 0.2g～1g, and the weight of every pill is 2g.
Medical mechanism: Embryo cervi paste, especially for Embryo cervi firm retention of dead fetus, that have amniotic fluid, can not with the big medicine compatibility of mending such as Radix Ginseng, more suitable with Radix Panacis Quinquefolii, Radix Ginseng Rubra interworking.Total Saponin (content is 5%～10%) is the main pharmaceutical component of Radix Panacis Quinquefolii, and is similar to Radix Ginseng, and just ratio is different; Radix Ginseng total saponins stresses diuresis and resisting fatigue, and total panaquilon more stresses calmness, promotes hemopoietic.Herba Leonuri has another name called Herba Leonuri, Herba Leonuri flower etc., is the upright herbaceous plant of Labiatae.It is the good medicine that the successive dynasties traditional Chinese medical science is used for treating gynaecopathia, beneficial body skin care, and Compendium of Material Medica points out, the Herba Leonuri removing blood stasis of invigorating blood circulation, regulating menstruation detoxifcation.Modern pharmacology proves, Herba Leonuri contains compositions such as leonurine, stachydrine, lauric acid, the water logging agent of Herba Leonuri has obviously faces upward the effect of system fungus, also have effects such as excited uterus, diuresis, blood pressure lowering, therefore this product has immunity, the endocrine regulation that increases the people, YIN nourishing skin care, the effect of becoming pregnant and preventing miscarriage.
Claims (7)
1. Poultice extract of deer foetus concentrated water-paste pill, it is characterized in that: the effective ingredient of this concentrated watered pill is each raw material of following weight ratio: bright Embryo cervi 5～15, Cornu Cervi Pantotrichum 5～15, Cauda cervi 5～15, unhairing Penis et testis cervi 5～10, Herba Leonuri 10～20, Radix Panacis Quinquefolii 5～10, Radix Glycyrrhizae 5～8, Radix Angelicae Sinensis 5～10, Radix Ginseng Rubra 5～8, boil the medicinal liquid that obtains with Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra and add bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi and be brewed into paste, the concentrated watered pill of quenching and obtaining through CO 2 supercritical.
2. Poultice extract of deer foetus concentrated water-paste pill according to claim 1 is characterized in that: described bright Embryo cervi is the Embryo cervi behind firm retention of dead fetus, that have amniotic fluid and the high temperature sterilization.
3. Poultice extract of deer foetus concentrated water-paste pill according to claim 1 is characterized in that: described each raw-material preferred weight ratio is: bright Embryo cervi 10, Cornu Cervi Pantotrichum 8, Cauda cervi 7, unhairing Penis et testis cervi 6, Herba Leonuri 15, Radix Panacis Quinquefolii 6, Radix Glycyrrhizae 6, Radix Angelicae Sinensis 7, Radix Ginseng Rubra 6.
3. the preparation method of a Poultice extract of deer foetus concentrated water-paste pill as claimed in claim 1 is characterized in that: undertaken by following step:
Get bright Embryo cervi, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi by the described weight ratio of claim 1, Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, each raw material of Radix Ginseng Rubra;
Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry post-heating to boil and obtains medicinal liquid;
The described bright Embryo cervi of adding, Cornu Cervi Pantotrichum, Cauda cervi, unhairing Penis et testis cervi are brewed into the thickness paste in the medicinal liquid that obtains after boiling;
To pulverizing after the described thickness paste oven dry that obtains;
The material obtain is pulverized in oven dry packed in the extractor, feed CO from the extractor bottom
2Gas, the control temperature is 33～70 ℃, and pressure is 25～55MPa, and the extraction time is 1～20 hour;
To extract that the thickness paste that reclaims adds water and edible adhesive is made the watered pill through granulator from extractor.
4. the preparation method of Poultice extract of deer foetus concentrated water-paste pill according to claim 3 is characterized in that: describedly Herba Leonuri, Radix Panacis Quinquefolii, Radix Glycyrrhizae, Radix Angelicae Sinensis, Radix Ginseng Rubra are added in the entry heating boil the step that obtains medicinal liquid and comprise:
Adding the weight of entry and the ratio of each raw material gross weight is: 3～5: 1; Temperature when heating boils is: 60～80 ℃; Boil 0.5～5 hour time.
5. the preparation method of Poultice extract of deer foetus concentrated water-paste pill according to claim 3 is characterized in that: describedly will add the edible binding agent that water and edible adhesive make the step of the watered pill through granulator from the thickness paste of extractor Separation and Recovery and comprise: the mixture of starch or starch and edible glue.
6. the preparation method of Poultice extract of deer foetus concentrated water-paste pill according to claim 3; it is characterized in that: describedly will add the step that water and edible adhesive make the watered pill through granulator from the thickness paste of extractor Separation and Recovery and comprise: the weight by every during the preparation watered pill is 1～2g, contains that to extract the back the effective elements of the medicine be 0.2～0.8g in every.
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| Application Number | Priority Date | Filing Date | Title |
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| CNA2007101579863A CN101167794A (en) | 2007-11-07 | 2007-11-07 | Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof |
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| CNA2007101579863A CN101167794A (en) | 2007-11-07 | 2007-11-07 | Poultice extract of deer foetus concentrated water-paste pill and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104997079A (en) * | 2015-08-06 | 2015-10-28 | 万雄集团股份有限公司 | A whole deer Chinese herbal medicine health-care decoction and a preparation method thereof |
| CN105343669A (en) * | 2015-11-30 | 2016-02-24 | 刘兆君 | Beauty maintaining pills and preparing method |
| CN105816620A (en) * | 2016-03-30 | 2016-08-03 | 张志仁 | Traditional Chinese medicine health care product formula |
| CN114343175A (en) * | 2021-12-29 | 2022-04-15 | 林杨 | Deer fetus paste instant powder |
-
2007
- 2007-11-07 CN CNA2007101579863A patent/CN101167794A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104997079A (en) * | 2015-08-06 | 2015-10-28 | 万雄集团股份有限公司 | A whole deer Chinese herbal medicine health-care decoction and a preparation method thereof |
| CN105343669A (en) * | 2015-11-30 | 2016-02-24 | 刘兆君 | Beauty maintaining pills and preparing method |
| CN105816620A (en) * | 2016-03-30 | 2016-08-03 | 张志仁 | Traditional Chinese medicine health care product formula |
| CN114343175A (en) * | 2021-12-29 | 2022-04-15 | 林杨 | Deer fetus paste instant powder |
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Open date: 20080430 |