CN101148633A - Water-base type wax mould cleaning agent and preparation method thereof - Google Patents
Water-base type wax mould cleaning agent and preparation method thereof Download PDFInfo
- Publication number
- CN101148633A CN101148633A CNA2007100529956A CN200710052995A CN101148633A CN 101148633 A CN101148633 A CN 101148633A CN A2007100529956 A CNA2007100529956 A CN A2007100529956A CN 200710052995 A CN200710052995 A CN 200710052995A CN 101148633 A CN101148633 A CN 101148633A
- Authority
- CN
- China
- Prior art keywords
- consumption
- water
- cleaning agent
- wax mould
- base type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Abstract
The water-base wax mold cleaning agent consists of nonylphenol polyoxyethylene ether 10-15 weight portions, coconut fatty acid diethanolamide 8-12 weight portions, trichloroethane 2-5 weight portions, fatty acid polyoxyethylene ether sulfate 10-18 weight portions, ethanol 1-2 weight portions and pure water 20-25 weight portions. It is superior to available wax mold cleaning agent with high volatility, toxicity and environmental pollution, and has high activity, no smell, no toxicity, no corrosion and other advantages. The present invention also discloses the preparation process of the water-base wax mold cleaning agent.
Description
Technical field
The present invention relates to a kind of water-base type wax mould cleaning agent, the present invention also discloses the preparation method of this water-base type wax mould cleaning agent.
Background technology
The precision casting industry is a labor force, the intensive relatively industry of resource, China's resources of production are abundant, labor cost is low, and this provides very big development space for China's precision casting production, and precision casting is produced just progressively and expanded and transfer to developing country from developed country and area.According to incompletely statistics, state-owned all kinds of smart cast more than 2000 families of enterprise, 1,000,000 tons of throughput, practitioner 500,000 people in.After the accession to WTO, China's economy incorporates world's big market, enterprise is immediately following international advanced technology, improve management, integrate with international standard, play an active part in international competition, enlarge the mechanical component of production aerospace high added value, develop towards " accurate, large-scale, slim " direction, so the demand of the cleaning agent of wax mould material of high-performance, safety and environmental protection constantly increases.
Various countries, the world today more and more pay attention to safety and environmental protection, and high-performance, oligosaprobic novel material will inevitably be favored by market.Before this, we are by a large amount of market surveys, and wax-pattern cleans to pass through with organic solvent (acetone, MEK) and makes to clean raw material both at home and abroad, and this kind solvent high volatility is poisonous to human body, harmful, and contaminate environment, and the infringement worker's is healthy.Publication number is the prescription that the patent application of CN1793308A discloses a kind of cleaning agent of wax mould by retrieval, and its composition comprises pure water, Sodium Nitrite, Soxylat A 25-7 etc.But Sodium Nitrite wherein is poisonous, and be carcinogenic substance, in the Sodium Nitrite molecule, the Oxidation Number of nitrogen is+3, be a kind of intermediate oxidation attitude, very big to healthy harm, so this cleaning agent of wax mould does not solve poison, the evil property problem of cleaning agent of wax mould fully yet, and through adapted, the result of use extreme difference of this product.
Summary of the invention
The objective of the invention is to overcome above-mentioned existing disadvantages of background technology part, and a kind of water-base type wax mould cleaning agent is provided.
Another object of the present invention provides a kind of preparation method who prepares this water-base type wax mould cleaning agent.
The objective of the invention is to reach: water-base type wax mould cleaning agent by following measure, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 10-15 weight part, cocoanut fatty acid diethanolamide is that 8-12 weight part, trichloroethane consumption are that the consumption of 2-5 weight part, aliphatic acid polyethenoxy ether vitriol is that 10-18 weight part, consumption of ethanol are the 1-2 weight part, and the pure water consumption is the 20-30 weight part.
Prepare the method for above-mentioned water-base type wax mould cleaning agent, it comprises the steps:
1, each raw material is weighed,
2, promoting agent cocoanut fatty acid diethanolamide, trichloroethane and aliphatic acid polyethenoxy ether vitriol are mixed,
3, add solvent pure water homogeneous and disperse,
4, add the emulsifying agent polyoxyethylene nonylphenol ether,
5, drip the neutralization of auxiliary agent ethanol,
6, under 60-80 degree temperature, to stir with 600 rev/mins of speed, the time is 50-70 minute, gained solution is water-base type wax mould cleaning agent.
Traditional wax-pattern cleaning material passes through with organic solvent (acetone, MEK), and cleaning performance is better, but unavoidably has drawback: 1, boiling point is low, has great security risk in inflammable and explosive, transportation, storage, the production process; 2, volatility is big, strong smell, and exciting eye, nose and the upper respiratory tract, irritated situation can appear in toxic side effect, and the work situation Air quality is poor, and workers ' health is worked the mischief; 3, behind the residual liquid discharge, water resources and soil all there is certain harm.
MEK cleaning agent of wax mould performance index:
| Index name | Index |
| MEK content % | ≥99.7 |
| Relative density (20/4 ℃) | 0.8054 |
| Moisture % | ≤0.1 |
| Acidity wt% | ≤0.001 |
| Flash-point (open cup) ℃ | -6 |
| Naturally ℃ | 515.6 |
| Boiling point ℃ | 79.6±0.5 |
| Specific refractory power | 1.3788 |
The present invention substitutes organic solvent with aq. type emulsion clean-out system, has advantages such as superpower activity, tasteless, nontoxic, no burn into machining oil is strong, washing is stable, and hanging is effective.
Safe and reliable, energy-efficient, washing effect is good, and it is obvious to reduce the cleaning cost simultaneously, has greatly improved productivity, and market application foreground is wide, excellent product performance.
Water-base type wax mould cleaning agent performance index of the present invention
| Index name | Index | ||||||
| Outward appearance | Milky white liquid, evenly not stratified, there is not precipitation | ||||||
| PH value | 6-8 (neutrality) | ||||||
| Proportion | 1.08 | ||||||
| Working substance content (%) | ≥46 | ||||||
| Cleaning performance | Machining oil power is strong, and soil dispersion is fast, the wax-pattern any surface finish | ||||||
| Cleansing power washing oil rate % weighting method | ≥99 | ||||||
| Flash-point | Do not have | Boiling point | 96℃ | Corrodibility | Do not have | Toxicity | Do not have |
From above performance index as can be seen, MEK (CAS 78-93-3), belong to and very easily fire toxic liquid, suction can make mucous membrane irriates such as human eye, nose, larynx, upper respiratory tract infection and causing inflammation, long-term contact to the people can vomit, out of breath, spasm even the stupor or the temporary disturbance of consciousness, have a strong impact on the healthy of direct labor.Behind the residual liquid discharge, atmosphere, soil, vegetation, water body all there is certain destruction.
In sum, excellent product performance of the present invention, comparative advantages are superior, and social benefit and economic benefit are obvious.
Description of drawings
Fig. 1 is the process flow sheet of preparation water-base type wax mould cleaning agent of the present invention.
Embodiment
Describe performance of the present invention in detail below in conjunction with accompanying drawing, but they do not constitute limitation of the invention, only give an example.
Consult accompanying drawing as can be known: water-base type wax mould cleaning agent of the present invention, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 10-15 weight part, cocoanut fatty acid diethanolamide is that 8-12 weight part, trichloroethane consumption are that the consumption of 2-5 weight part, aliphatic acid polyethenoxy ether vitriol is that 10-18 weight part, consumption of ethanol are that 1-2 weight part, pure water consumption are the 20-25 weight part.
Prepare the method for above-mentioned water-base type wax mould cleaning agent, it comprises the steps:
1, each raw material is weighed,
2, promoting agent cocoanut fatty acid diethanolamide, trichloroethane and aliphatic acid polyethenoxy ether vitriol are mixed,
3, add solvent pure water homogeneous and disperse,
4, add the emulsifying agent polyoxyethylene nonylphenol ether,
5, add the neutralization of auxiliary agent ethanol,
6, under 60-80 degree temperature, to stir with 600 rev/mins of speed, the time is 50-70 minute, gained solution is water-base type wax mould cleaning agent.
Water-base type wax mould cleaning agent of the present invention has following characteristics:
1, scientific formula: with nontoxic free from corrosion emulsifying agent, tensio-active agent, auxiliary agent, pure water is system component, and the science modulation is a kind of high performance cleaning agent of wax mould, and more than screening draws prescription through science.
2, adopt water-dispersion physics synthetic technology: raw material makes high-performance and superpower active water-base type wax mould cleaning agent by composite, homogeneous, dropping, high-speed stirring, emulsification, neutralization.
Water-base type wax mould cleaning agent performance characteristics of the present invention is: nontoxic, the no burn into of white emulsifying aq does not have volatilization, soluble in water; molecular particle and water energy homodisperse; have remarkable stability, perviousness, cutting oiliness, to the thickening property of water, soil dispersion and skin care.
Water-base type wax mould cleaning agent of the present invention detects through Switzerland Hong Kong notary company limited, and every safety, environmental protection index data symbols merge the standard that is better than the current international practice.
Result of use: excellent product performance of the present invention, not only simplify working process easy construction and reducing production costs obviously.This product before use can be according to the requirement of foundry goods precision, blend water by different ratios and mix and use, and after tested, one group of vegetable wax mould only needs 3-5 once to clean second to finish, and it is thorough to remove greasy dirt, and the wax-pattern hanging is effective.Through the contrast experiment relatively: on equivalent amount, product of the present invention is bigger by about 300% than the group tree quantity that MEK cleans, and one well matchedly once expects about 5000 groups of trees capable of washing, and with the MEK cleaning of equivalent amount, the general 1600-2000 of cleaning group is set and will be changed, and comprehensive comparative advantages are obvious.
Embodiment 1
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 11 weight parts, cocoanut fatty acid diethanolamide is that 11.5 weight parts, trichloroethane consumption are that the consumption of 2.5 weight parts, aliphatic acid polyethenoxy ether vitriol is that 10 weight parts, consumption of ethanol are that 1.5 weight parts, pure water consumption are 23 weight parts.
The preparation method is as follows:
1, each raw material is weighed,
2, with promoting agent cocoanut fatty acid diethanolamide, trichloroethane and aliphatic acid polyethenoxy ether vitriol, mix,
3, add solvent pure water homogeneous and disperse,
4, add the emulsifying agent polyoxyethylene nonylphenol ether,
5, add the neutralization of auxiliary agent ethanol,
6, under 60 degree temperature, stir with 600 rev/mins of speed, the time is 50 minutes, and gained solution is water-base type wax mould cleaning agent.
Embodiment 2
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 14 weight parts, cocoanut fatty acid diethanolamide is that 9 weight parts, trichloroethane consumption are that the consumption of 3 weight parts, aliphatic acid polyethenoxy ether vitriol is that 18 weight parts, consumption of ethanol are that 1 weight part, pure water consumption are 21 weight parts.
The preparation method, temperature is under 70 degree in step 6, stirs with 600 rev/mins of speed, the time is 60 minutes.Other is with embodiment 1.
Embodiment 3
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 13 weight parts, cocoanut fatty acid diethanolamide is that 12 weight parts, trichloroethane consumption are that the consumption of 4 weight parts, aliphatic acid polyethenoxy ether vitriol is that 15 weight parts, consumption of ethanol are that 2 weight parts, pure water consumption are 22 weight parts.
The preparation method, temperature is 80 degree in step 6, stirs with 600 rev/mins of speed, the time is 70 minutes.Other is with embodiment 1.
Embodiment 4
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 11 weight parts, cocoanut fatty acid diethanolamide is that 9 weight parts, trichloroethane consumption are that the consumption of 3 weight parts, aliphatic acid polyethenoxy ether vitriol is that 12 weight parts, consumption of ethanol are that 1.5 weight parts, pure water consumption are 23 weight parts.
The preparation method, temperature is 70 degree in step 6, stirs with 600 rev/mins of speed, the time is 60 minutes.Other is with embodiment 1.
Embodiment 5
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 10 weight parts, cocoanut fatty acid diethanolamide is that 8 weight parts, trichloroethane consumption are that the consumption of 2 weight parts, aliphatic acid polyethenoxy ether vitriol is that 17 weight parts, consumption of ethanol are that 1 weight part, pure water consumption are 20 weight parts.
The preparation method, temperature is 80 degree in step 6, stirs with 600 rev/mins of speed, the time is 50 minutes.Other is with embodiment 1.
Embodiment 6
Water-base type wax mould cleaning agent, it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, and the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 15 weight parts, cocoanut fatty acid diethanolamide is that 12 weight parts, trichloroethane consumption are that the consumption of 5 weight parts, aliphatic acid polyethenoxy ether vitriol is that 14 weight parts, consumption of ethanol are that 2 weight parts, pure water consumption are 25 weight parts.
The preparation method, temperature is 50 degree in step 6, stirs with 600 rev/mins of speed, the time is 70 minutes.Other is with embodiment 1.
Claims (2)
1. water-base type wax mould cleaning agent, it is characterized in that it comprises polyoxyethylene nonylphenol ether, cocoanut fatty acid diethanolamide, trichloroethane, aliphatic acid polyethenoxy ether vitriol, ethanol, pure water, the consumption of described polyoxyethylene nonylphenol ether is that the consumption of 10-15 weight part, cocoanut fatty acid diethanolamide is that 8-12 weight part, trichloroethane consumption are that the consumption of 2-5 weight part, aliphatic acid polyethenoxy ether vitriol is that 10-18 weight part, consumption of ethanol are the 1-2 weight part, and the pure water consumption is the 20-30 weight part.
2. the method for preparing the described water-base type wax mould cleaning agent of claim 1 is characterized in that it comprises the steps:
(1), each raw material weighs,
(2), promoting agent cocoanut fatty acid diethanolamide, trichloroethane and aliphatic acid polyethenoxy ether vitriol are mixed,
(3), add solvent pure water homogeneous and disperse,
(4), add the emulsifying agent polyoxyethylene nonylphenol ether,
(5), drip the neutralization of auxiliary agent ethanol,
(6), under the 60-80 temperature, stir with 600 rev/mins of speed, the time is 50-70 minute, gained solution is water-base type wax mould cleaning agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100529956A CN100543121C (en) | 2007-08-20 | 2007-08-20 | Water-base type wax mould cleaning agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100529956A CN100543121C (en) | 2007-08-20 | 2007-08-20 | Water-base type wax mould cleaning agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101148633A true CN101148633A (en) | 2008-03-26 |
| CN100543121C CN100543121C (en) | 2009-09-23 |
Family
ID=39249330
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007100529956A Expired - Fee Related CN100543121C (en) | 2007-08-20 | 2007-08-20 | Water-base type wax mould cleaning agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100543121C (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101870936A (en) * | 2010-06-25 | 2010-10-27 | 武汉市智发科技开发有限公司 | Low-carbon environment-friendly wax pattern cleaning agent formula and preparation method thereof |
| CN101880607A (en) * | 2010-06-29 | 2010-11-10 | 王永生 | Water-based dewaxing agent |
| CN106566700A (en) * | 2016-11-08 | 2017-04-19 | 广东富行洗涤剂科技有限公司 | Wax mold cleaning agent |
| CN108130207A (en) * | 2018-01-17 | 2018-06-08 | 江门市新灵科技有限公司 | A kind of environment-friendly wax pattern cleaning agent and preparation method thereof |
| CN111763579A (en) * | 2020-06-04 | 2020-10-13 | 山东将军烟草新材料科技有限公司 | Paraffin cleaning agent in production of cigarette blasting beads as well as preparation method and use method thereof |
-
2007
- 2007-08-20 CN CNB2007100529956A patent/CN100543121C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101870936A (en) * | 2010-06-25 | 2010-10-27 | 武汉市智发科技开发有限公司 | Low-carbon environment-friendly wax pattern cleaning agent formula and preparation method thereof |
| CN101880607A (en) * | 2010-06-29 | 2010-11-10 | 王永生 | Water-based dewaxing agent |
| CN106566700A (en) * | 2016-11-08 | 2017-04-19 | 广东富行洗涤剂科技有限公司 | Wax mold cleaning agent |
| CN108130207A (en) * | 2018-01-17 | 2018-06-08 | 江门市新灵科技有限公司 | A kind of environment-friendly wax pattern cleaning agent and preparation method thereof |
| CN111763579A (en) * | 2020-06-04 | 2020-10-13 | 山东将军烟草新材料科技有限公司 | Paraffin cleaning agent in production of cigarette blasting beads as well as preparation method and use method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100543121C (en) | 2009-09-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100543121C (en) | Water-base type wax mould cleaning agent and preparation method thereof | |
| CN106047522B (en) | A kind of anhydrous liquid detergent of hyperconcetration type and preparation method thereof and solidifying pearl of doing washing | |
| CN101406928B (en) | Organosilicon microemulsion antisticking agent and preparation method thereof | |
| CN102021089A (en) | Water-based automobile asphalt cleaning agent and preparation method thereof | |
| CN106318689B (en) | A kind of automobile washing liquid and preparation method thereof | |
| CN103590044A (en) | Metal polishing agent and preparation method thereof | |
| CN103524201B (en) | Composite material for vegetation restoration and preparation method thereof | |
| CN103205332A (en) | Liquid laundry detergent and preparation method thereof | |
| CN102925305B (en) | Water-based cleaning agent for silicone grease and silicone oil | |
| CN101422164B (en) | Chlorpyrifos and Imidacloprid suspension emulsion and preparation method thereof | |
| CN109574423A (en) | A kind of high-efficiency oil sludge demulsifier and preparation method thereof | |
| CN111560293B (en) | Detergent containing folium artemisiae argyi essential oil microcapsules and preparation method thereof | |
| CN103194338A (en) | Hand sanitizer and preparation method thereof | |
| CN105297044A (en) | Water-based stainless steel cleaner | |
| CN101251723B (en) | Negative colorful photoresist degumming agent and method for preparing the same | |
| CN105326727A (en) | Wild chrysanthemum flower washing-free hand sanitizer and preparation method thereof | |
| CN105456098A (en) | Oenothera biennis waterless hand sanitizer and preparation method thereof | |
| CN105232374A (en) | Efficient moderate moist type cleansing cream | |
| CN101836627B (en) | Dimethomorph-containing pesticide suspension concentrate and preparation method thereof | |
| CN108865494A (en) | A kind of highly-efficient glass cleaning agent and preparation method thereof | |
| CN103255010B (en) | Dishwashing liquid and preparation method thereof | |
| CN1190121A (en) | Preparation of plant composition detergent | |
| CN109762645A (en) | A kind of high-lubricity polysilicon slice water base cutting liquid and preparation method thereof | |
| CN105165808B (en) | A kind of benzene-series solvent replacements sulfonated kerosene and its application in carbosulfan missible oil | |
| CN107646833A (en) | A kind of flowers and water support plant antistaling agent, preparation method and preserved flower |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: WUHAN YIQIANG TECHNOLOGY DEVELOPMENT CO., LTD. Free format text: FORMER OWNER: CHEN ZHIXIANG Effective date: 20100730 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20100730 Address after: 430200, 17, leading Street, paper Fang street, Jiangxia District, Hubei, Wuhan Patentee after: Wuhan Yiqiang Science Expoittation Co., Ltd. Address before: 430200, 17, leading Street, paper Fang street, Jiangxia District, Hubei, Wuhan Patentee before: Chen Zhixiang |
|
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090923 Termination date: 20110820 |