CN101148565B - Wax polish and preparation method thereof - Google Patents
Wax polish and preparation method thereof Download PDFInfo
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- CN101148565B CN101148565B CN2007100302158A CN200710030215A CN101148565B CN 101148565 B CN101148565 B CN 101148565B CN 2007100302158 A CN2007100302158 A CN 2007100302158A CN 200710030215 A CN200710030215 A CN 200710030215A CN 101148565 B CN101148565 B CN 101148565B
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Abstract
The process provides one kind of polishing wax and its preparation process. The polishing wax consists of silicone oil 3-8 wt%, vaseline 0.2-5 wt%, polyethylene 0.1-8 wt%, montan wax 0.1-0.5 wt%, coumarone-indene resin 0.1-5 wt%, carnauba wax 0.1-1 wt%, C12 fatty alcohol polyoxyethylene ether 0.5-3 wt%, nonylphenol polyoxyethylene ether 1-5 wt%, alkyl alcohol amide 2-5 wt%, ammonium hexadecyl trimethyl chloride or ammonium octadecyl trimethyl chloride 2-8 wt%, bentonite 1-5 wt%, glutaraldehyde 0.05-0.1 wt% and water 46.4-89.85 wt%. The polishing wax has no corrosion to the paint surface, and can eliminate dirt from paint surface, make paint surface clean and bright, and form protecting film with high heat resistance, less ageing and good luster.
Description
Technical field
The present invention relates to a kind of polishing wax, and the preparation method of this polishing wax.
Background technology
Vehicle travel, in the parking period, deterioration is got dirty, is subjected to the lacquer painting of its appearance easily, just need clean at set intervals, cleaning is waxed, is polished lacquer painting with polishing wax often.
Existing polishing wax mostly is solvent-borne type polishing wax greatly, and the essentially consist of solvent-borne type polishing wax is polystyrene and organic solvent, and a spot of tensio-active agent and polishing powder.Though solvent-borne type polishing wax has stronger soil removability, but because lacquer can be dissolved in organic solvent, therefore when on lacquer painting, brushing polishing wax, lacquer painting can be subjected to burn into infiltration and impaired, jaundice becomes coarse easily, makes lacquer painting lack gloss, and can hardening, be full of cracks, peel off gradually, thereby make the appearance of car day by day old and feeble; Organic solvent in the solvent-borne type polishing wax has flavor and/or inflammable, and organic solvent is toxic substance, thus solvent-borne type polishing wax use dangerous, harmful to HUMAN HEALTH; Some polishing powder is coarse, hard in the solvent-borne type polishing wax, and lacquer painting can wear and tear; Polystyrene in the solvent-borne type polishing wax is a film forming material, can only be heat-resisting 80 ℃, and the easily aging embrittlement of the protective membrane that forms behind the carwash, and the gloss refractive index has only 1.60.
Existing solvent-borne type polishing wax is used for the light time on the leatherware surface, and organic solvent wherein can make leather hardening, be full of cracks.
Summary of the invention
Technical problem to be solved by this invention provides a kind of polishing wax; this polishing wax does not contain organic solvent, can not corrode lacquer painting, and soil removability is strong; safe in utilization, and can on lacquer painting, form better, difficult aging embrittlement of resistance toheat and the brighter protective membrane of gloss.The technical scheme that adopts is as follows:
On the one hand, the invention provides a kind of polishing wax, the component of this polishing wax and the weight percent content of each component are:
Silicone oil 3～8%; Vaseline 0.2～5%; Polyethylene 0.1～8%; Montanin wax 0.1～0.5%; Coumarone-indene resin 0.1～5%; Carnauba wax 0.1～1%; C
12Aliphatic alcohol polyethenoxy (n) ether 0.5～3%, C
12N=3～15 in aliphatic alcohol polyethenoxy (n) ether; Nonyl pheno (n) ether 1～5%, n=4～15 in Nonyl pheno (n) ether; Alkylol amide 2～5%; Palmityl trimethyl ammonium chloride or octadecyl trimethyl ammonium chloride 2～8%; Wilkinite 1～5%; Glutaraldehyde 0.05～0.1%; Water 46.4～89.85%.
Above-mentioned silicone oil is lubricant, makes polishing wax be easy to smear, and makes the protective membrane hydrophobic effect of formation good.
The protective membrane that above-mentioned Vaseline forms polishing wax plays antirust, anti-ultraviolet effect, and makes protective membrane can send fluorescence.
Above-mentioned polyethylene is the main material that forms protective membrane, and can repair the lacquer painting cut, makes protective membrane durable in use.
Protective membrane good luster, smooth degree height that above-mentioned montanin wax forms polishing wax.
The protective membrane good luster that above-mentioned coumarone-indene resin forms polishing wax can make the refractive index of protective membrane reach 1.628-1.64.
Above-mentioned carnauba wax is used to regulate the zero pour of polishing wax, can make polishing wax be solid paste or starchiness.
Above-mentioned C
12Aliphatic alcohol polyethenoxy (n) ether is emulsifying agent, also is stain remover simultaneously, is used for emulsification entry such as polyethylene, montanin wax and coumarone-indene resins, and removes the dirt on the lacquer painting when cleaning lacquer painting.
Above-mentioned Nonyl pheno (n) ether is emulsifying agent, also is stain remover simultaneously, is used for emulsification entry such as polyethylene, montanin wax and coumarone-indene resins, and is penetrated in the dirt when cleaning lacquer painting, removes the dirt on the lacquer painting.
The abovementioned alkyl alcohol amide is an emulsifying agent, also is stain remover simultaneously, is used for emulsification entry such as polyethylene, montanin wax and coumarone-indene resins, and removes the dirt on the lacquer painting when cleaning lacquer painting.The preferred alkyl alcohol amide is coconut oil diethanol amide (1: 1 type) or coconut oil diethanol amide (1: 2 type).
Above-mentioned palmityl trimethyl ammonium chloride, octadecyl trimethyl ammonium chloride are tensio-active agents, have emulsive effect and anlistatig function, and the protective membrane smooth degree height that polishing wax is formed.
Above-mentioned wilkinite can polish lacquer painting; Be filled in after the suction in the polishing wax, can make the polishing wax typing.
That above-mentioned glutaraldehyde has is anticorrosion, mildew-resistant, germ-resistant function, and that the protective membrane that polishing wax is formed plays is anticorrosion, mildew-resistant, germ-resistant effect.
On the other hand, the invention provides the preparation method of above-mentioned polishing wax, the preparation method of this polishing wax may further comprise the steps: with silicone oil 3～8 grams, Vaseline 0.2～5 gram, polyethylene 0.1～8 gram, montanin wax 0.1～0.5 gram, coumarone-indene resin 0.1～5 gram, carnauba wax 0.1～1 gram, C
12Aliphatic alcohol polyethenoxy (n) ether 0.5～3 gram, Nonyl pheno (n) ether 1～5 gram and alkylol amide 2～5 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 98～102 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 5～10 gram temperature in filtrate is 95～100 ℃ water, and adding the used time of water process is 10～30 seconds; Make emulsification cool to 48～52 ℃ with the oil bath assorted pot then, add the bentonite slurry that 5～25 grams have absorbed water in the oil bath assorted pot to emulsification, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 10～40 gram weight percentage concentrations in the oil bath assorted pot to emulsification then is 20% the palmityl trimethyl ammonium chloride aqueous solution or the octadecyl trimethyl ammonium chloride aqueous solution; Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 90～95 ℃ then, stir, cool to 50～60 ℃ again, splash into glutaraldehyde 0.05～0.1 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 50～60 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.The polishing wax tank filling, the encapsulation of cooling back.
Above-mentioned silicone oil, Vaseline, polyethylene, montanin wax, coumarone-indene resin, carnauba wax, C
12The consumption of aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and alkylol amide is all by net weight.
During the lacquer painting of cleaning vehicle, at first remove dust on the lacquer painting etc., use above-mentioned polishing wax wiping lacquer painting then, can remove the dirt on the lacquer painting, and form one deck and cover protective membrane on the lacquer painting.
But the present invention utilizes the characteristics of polyethylene, montanin wax and coumarone-indene resin emulsification entry, utilizes C
12Aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether, alkylol amide and palmityl trimethyl ammonium chloride or octadecyl trimethyl ammonium chloride etc. are with its emulsification entry, form oil-in-water type polishing wax, owing to do not contain organic solvent in the polishing wax, do not have inflammable or flavor, toxic ingredient are arranged, therefore this polishing wax can not corrode lacquer painting or make the leather sex change, and safe in utilization; The fusing point of polyethylene, montanin wax and coumarone-indene resin is all more than 100 ℃, wherein the refractive index of coumarone-indene resin reaches 1.628-1.64, and the protective membrane resistance toheat that polishing wax is formed is better, is difficult for aging embrittlement, gloss is better, and montanin wax also can improve the smooth degree of protective membrane; That the protective membrane that Vaseline in the polishing wax, palmityl trimethyl ammonium chloride or octadecyl trimethyl ammonium chloride, glutaraldehyde etc. also make polishing wax form plays is antirust, the effect of uvioresistant, antistatic, anticorrosion, mildew-resistant, feels more during dusk that automobile finish protective membrane fluorescence is glittering; C
12Therefore aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and alkylol amide all have strong soil removability, and this polishing wax can be removed the dirt on the lacquer painting, make that lacquer painting keeps clean, light.Polishing wax provided by the invention can be used for the surperficial glazing of automobile finish, leatherware, furniture, stone slab etc.
Embodiment
Embodiment 1
Make polishing wax according to the following steps: with silicone oil 3.5 grams, Vaseline 0.3 gram, polyethylene 5 grams, montanin wax 0.2 gram, coumarone-indene resin 4.5 grams, carnauba wax 0.6 gram, C
12Nine kinds of raw materials such as aliphatic alcohol polyethenoxy (n) ether 2.8 grams, Nonyl pheno (n) ether 3 grams and coconut oil diethanol amide (1: 1 type) 2.5 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 100 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 10 gram temperature are 100 ℃ water in filtrate, and adding the used time of water process is 20 seconds; Make emulsification cool to 50 ℃ with the oil bath assorted pot then, add the bentonite slurry that 15 grams have absorbed water to emulsification in the oil bath assorted pot, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 12.5 gram concentration to emulsification in the oil bath assorted pot then is the palmityl trimethyl ammonium chloride aqueous solution of 20% (weight ratio); Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 95 ℃ then, stir, cool to 55 ℃ again, splash into glutaraldehyde 0.06 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 55 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.The polishing wax tank filling, the encapsulation of cooling back.
Above-mentioned silicone oil, Vaseline, polyethylene, montanin wax, coumarone-indene resin, carnauba wax, C
12The consumption of aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and coconut oil diethanol amide (1: 1 type) is all by net weight.C
12N=10 in aliphatic alcohol polyethenoxy (n) ether; N=8 in Nonyl pheno (n) ether.
Contain in the 100 gram polishing waxs of making: silicone oil 3.5 grams, Vaseline 0.3 gram, polyethylene 5 grams, montanin wax 0.2 gram, coumarone-indene resin 4.5 grams, carnauba wax 0.6 gram, C
12Aliphatic alcohol polyethenoxy (n) ether 2.8 grams, Nonyl pheno (n) ether 3 grams, coconut oil diethanol amide (1: 1 type) 2.5 grams, palmityl trimethyl ammonium chloride 2.5 grams, wilkinite 3 grams, glutaraldehyde 0.06 gram, water 72.04 grams.
Being equipped with raw material during batch process according to the above ratio gets final product.
Embodiment 2
Make polishing wax according to the following steps: with silicone oil 8 grams, Vaseline 5 grams, polyethylene 8 grams, montanin wax 0.5 gram, coumarone-indene resin 0.2 gram, carnauba wax 0.2 gram, C
12Nine kinds of raw materials such as aliphatic alcohol polyethenoxy (n) ether 3 grams, Nonyl pheno (n) ether 5 grams and coconut oil diethanol amide (1: 2 type) 4.5 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 99 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 6 gram temperature are 99 ℃ water in filtrate, and adding the used time of water process is 15 seconds; Make emulsification cool to 48 ℃ with the oil bath assorted pot then, add the bentonite slurry that 22.5 grams have absorbed water to emulsification in the oil bath assorted pot, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 37.5 gram concentration to emulsification in the oil bath assorted pot then is the palmityl trimethyl ammonium chloride aqueous solution of 20% (weight ratio); Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 90 ℃ then, stir, cool to 50 ℃ again, splash into glutaraldehyde 0.09 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 52 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.The polishing wax tank filling, the encapsulation of cooling back.
Above-mentioned silicone oil, Vaseline, polyethylene, montanin wax, coumarone-indene resin, carnauba wax, C
12The consumption of aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and coconut oil diethanol amide (1: 2 type) is all by net weight.C
12N=14 in aliphatic alcohol polyethenoxy (n) ether; N=5 in Nonyl pheno (n) ether.
Contain in the 100 gram polishing waxs of making: silicone oil 8 grams, Vaseline 5 grams, polyethylene 8 grams, montanin wax 0.5 gram, coumarone-indene resin 0.2 gram, carnauba wax 0.2 gram, C12 aliphatic alcohol polyethenoxy (n) ether 3 grams, Nonyl pheno (n) ether 5 grams, coconut oil diethanol amide (1: 2 type) 4.5 grams, palmityl trimethyl ammonium chloride 7.5 grams, wilkinite 4.5 grams, glutaraldehyde 0.09 gram, water 53.51 grams.
Being equipped with raw material during batch process according to the above ratio gets final product.
Embodiment 3
Make polishing wax according to the following steps: with silicone oil 5 grams, Vaseline 3 grams, polyethylene 7.5 grams, montanin wax 0.1 gram, coumarone-indene resin 1 gram, carnauba wax 0.8 gram, C
12Nine kinds of raw materials such as aliphatic alcohol polyethenoxy (n) ether 0.5 gram, Nonyl pheno (n) ether 1 gram and coconut oil diethanol amide (1: 1 type) 3.5 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 101 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 8 gram temperature are 98 ℃ water in filtrate, and adding the used time of water process is 12 seconds; Make emulsification cool to 51 ℃ with the oil bath assorted pot then, add the bentonite slurry that 12.5 grams have absorbed water to emulsification in the oil bath assorted pot, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 22.5 gram concentration to emulsification in the oil bath assorted pot then is the octadecyl trimethyl ammonium chloride aqueous solution of 20% (weight ratio); Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 92 ℃ then, stir, cool to 55 ℃ again, splash into glutaraldehyde 0.1 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 58 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.The polishing wax tank filling, the encapsulation of cooling back.
Above-mentioned silicone oil, Vaseline, polyethylene, montanin wax, coumarone-indene resin, carnauba wax, C
12The consumption of aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and coconut oil diethanol amide (1: 1 type) is all by net weight.C
12N=8 in aliphatic alcohol polyethenoxy (n) ether; N=12 in Nonyl pheno (n) ether.
Contain in the 100 gram polishing waxs of making: silicone oil 5 grams, Vaseline 3 grams, polyethylene 7.5 grams, montanin wax 0.1 gram, coumarone-indene resin 1 gram, carnauba wax 0.8 gram, C12 aliphatic alcohol polyethenoxy (n) ether 0.5 gram, Nonyl pheno (n) ether 1 gram, coconut oil diethanol amide (1: 1 type) 3.5 grams, octadecyl trimethyl ammonium chloride 4.5 grams, wilkinite 2.5 grams, glutaraldehyde 0.1 gram, water 70.5 grams.
Being equipped with raw material during batch process according to the above ratio gets final product.
Embodiment 4
Make polishing wax according to the following steps: with silicone oil 3.5 grams, Vaseline 0.3 gram, polyethylene 1.5 grams, montanin wax 0.2 gram, coumarone-indene resin 1.2 grams, carnauba wax 0.6 gram, C
12Nine kinds of raw materials such as aliphatic alcohol polyethenoxy (n) ether 0.8 gram, Nonyl pheno (n) ether 1.5 grams and coconut oil diethanol amide (1: 2 type) 2.2 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 100 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 9 gram temperature are 100 ℃ water in filtrate, and adding the used time of water process is 28 seconds; Make emulsification cool to 49 ℃ with the oil bath assorted pot then, add the bentonite slurry that 7.5 grams have absorbed water to emulsification in the oil bath assorted pot, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 12.5 gram concentration to emulsification in the oil bath assorted pot then is the palmityl trimethyl ammonium chloride aqueous solution of 20% (weight ratio); Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 93 ℃ then, stir, cool to 53 ℃ again, splash into glutaraldehyde 0.05 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 56 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.The polishing wax tank filling, the encapsulation of cooling back.
Above-mentioned silicone oil, Vaseline, polyethylene, montanin wax, coumarone-indene resin, carnauba wax, C
12The consumption of aliphatic alcohol polyethenoxy (n) ether, Nonyl pheno (n) ether and coconut oil diethanol amide (1: 2 type) is all by net weight.C
12N=10 in aliphatic alcohol polyethenoxy (n) ether; N=10 in Nonyl pheno (n) ether.
Contain in the 100 gram polishing waxs of making: silicone oil 3.5 grams, Vaseline 0.3 gram, polyethylene 1.5 grams, montanin wax 0.2 gram, coumarone-indene resin 1.2 grams, carnauba wax 0.6 gram, C
12Aliphatic alcohol polyethenoxy (n) ether 0.8 gram, Nonyl pheno (n) ether 1.5 grams, coconut oil diethanol amide (1: 2 type) 2.2 grams, palmityl trimethyl ammonium chloride 2.5 grams, wilkinite 1.5 grams, glutaraldehyde 0.05 gram, water 84.15 grams.
Being equipped with raw material during batch process according to the above ratio gets final product.
Claims (3)
1. a polishing wax is characterized in that the weight percent content of its component and each component is: silicone oil 3～8%; Vaseline 0.2～5%; Polyethylene 0.1～8%; Montanin wax 0.1～0.5%; Coumarone-indene resin 0.1～5%; Carnauba wax 0.1～1%; C
12Aliphatic alcohol polyethenoxy (n) ether 0.5～3%, C
12N=3～15 in aliphatic alcohol polyethenoxy (n) ether; Nonyl pheno (n) ether 1～5%, n=4～15 in Nonyl pheno (n) ether; Alkylol amide 2～5%; Palmityl trimethyl ammonium chloride or octadecyl trimethyl ammonium chloride 2～8%; Wilkinite 1～5%; Glutaraldehyde 0.05～0.1%; Water 46.4～89.85%.
2. polishing wax according to claim 1 is characterized in that: described alkylol amide is 1: 1 type coconut oil diethanol amide or 1: 2 type coconut oil diethanol amide.
3. the preparation method of the described polishing wax of claim 1 is characterized in that may further comprise the steps: with silicone oil 3～8 grams, Vaseline 0.2～5 gram, polyethylene 0.1～8 gram, montanin wax 0.1～0.5 gram, coumarone-indene resin 0.1～5 gram, carnauba wax 0.1～1 gram, C
12Aliphatic alcohol polyethenoxy (n) ether 0.5～3 gram, Nonyl pheno (n) ether 1～5 gram and alkylol amide 2～5 grams join esterification with in the oil bath assorted pot, be heated to each raw material fusing, esterification, filter then, filter rear filtrate and place emulsification oil bath assorted pot; Emulsification remains on 98～102 ℃ with the temperature of the filtrate in the oil bath assorted pot, and under condition of stirring, adding 5～10 gram temperature in filtrate is 95～100 ℃ water, and adding the used time of water process is 10～30 seconds; Make emulsification cool to 48～52 ℃ with the oil bath assorted pot then, add the bentonite slurry that 5～25 grams have absorbed water in the oil bath assorted pot to emulsification, stir, bentonitic weight percent content is 20% in the used bentonite slurry; Adding 10～40 gram weight percentage concentrations in the oil bath assorted pot to emulsification then is 20% the palmityl trimethyl ammonium chloride aqueous solution or the octadecyl trimethyl ammonium chloride aqueous solution; Then add water in the oil bath assorted pot to emulsification, making emulsification is 100 grams with material gross weight in the oil bath assorted pot, be warming up to 90～95 ℃ then, stir, cool to 50～60 ℃ again, splash into glutaraldehyde 0.05～0.1 gram in the oil bath assorted pot to emulsification, adding temperature in the oil bath assorted pot to emulsification then is 50～60 ℃ water, because of heating evaporable water, making emulsification is 100 grams with material gross weight in the oil bath assorted pot with compensation, obtains 100 gram polishing waxs.
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| CN2007100302158A CN101148565B (en) | 2007-09-08 | 2007-09-08 | Wax polish and preparation method thereof |
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| CN2007100302158A CN101148565B (en) | 2007-09-08 | 2007-09-08 | Wax polish and preparation method thereof |
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| CN101148565A CN101148565A (en) | 2008-03-26 |
| CN101148565B true CN101148565B (en) | 2010-10-06 |
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|---|---|---|---|---|
| CN1311279A (en) * | 2000-03-03 | 2001-09-05 | 李松波 | Method for producing wax polish of slabstone |
| CN1521227A (en) * | 2003-01-27 | 2004-08-18 | 上海江通环保科技有限公司 | Photoprotectant for wood olein floor and furniture and its preparing process |
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| Publication number | Publication date |
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| CN101148565A (en) | 2008-03-26 |
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