CN101138346A - Disinfectant liquid containing coral ginger oil and preparing method thereof - Google Patents
Disinfectant liquid containing coral ginger oil and preparing method thereof Download PDFInfo
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- CN101138346A CN101138346A CNA2007100779877A CN200710077987A CN101138346A CN 101138346 A CN101138346 A CN 101138346A CN A2007100779877 A CNA2007100779877 A CN A2007100779877A CN 200710077987 A CN200710077987 A CN 200710077987A CN 101138346 A CN101138346 A CN 101138346A
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- coral ginger
- ginger oil
- thimerosal
- coral
- oil
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Abstract
The present invention discloses a disinfection solution and the preparation method; the present invention relates to disinfection solution. The disinfection solution takes the volatile oil from the zingiber collinum as the main active component which is made into disinfection solution with the glycerol, ethanol and distilled water by emulsification; the component amounts of the disinfection solution per 1000 ml comprise volatile oil from zingiber collinum 150 ml, emulsifier 50ml, glycerol 50ml, ethanol which is purity of 95 percent 450 ml and distilled water 300ml. The preparation method comprises that the glycerol and ethanol with a purity of 95 percent are taken according to proportion to put in a mixer for mixing; and then the volatile oil from zingiber collinum is added into the mixer for continuous mixing; the mixture is put into a high-pressure fluid homogenizer for homogenization and then the mixture is filtrated; the distilled water is added and the mixture is adjusted to a specified amount to obtain the disinfection solution. The active components of the disinfection solution are natural with low toxicity and can be degraded after use with little environmental pollution; with the unique action mechanism, bacterial can hardly produce drug resistance and the service life is long. Therefore, the present invention is fit for disinfection in various environments.
Description
Technical field
The present invention is relevant with medicinal preparation, furthermore, relates to thimerosal; In particular to the thimerosal that contains coral ginger oil.
Background technology
Coral ginger (Rhizoma zingibel) flavor is pungent, and energy is clearing heat and detoxicating, detumescence (seeing 143 pages in " Chinese Plants will " 16 volumes 2 fascicles), and its volatile oil contains terpinene-4 alcohol, can be antibiotic, antimycotic.In recent years, utilize the commodity of coral ginger preparation and medicine to have several.For example Chinese patent application part ZL89100495.5 number " the medicine cigarette that contains the coral ginger content ", ZL95115953.4 number " hair care and hair growth lotion of coral ginger extract preparation ", No. 95103907.5 " coral ginger is applied to the method for health products and cosmetics ", ZL200510003033.2 number " a kind of Chinese medicinal liniment for the treatment of acne ", No. 200610051098.9 " compound turmeric acne-eliminating gel and preparation method thereof " disclose some respectively and have utilized the medicine or the commodity of coral ginger extract.But people open renewal, more efficient drug still in the new purposes of exploring and study coral ginger.
Summary of the invention
Purpose of the present invention just is to provide a kind of thimerosal that contains coral ginger oil, to increase the kind of thimerosal, enables the health service into people.
Another object of the present invention provides the preparation method of this thimerosal.
The thimerosal that contains coral ginger oil of the present invention is to be main active with the coral ginger oil, after with emulsifier emulsification, and the thimerosal formulated with glycerine, ethanol and distilled water.
The component and the consumption thereof of every this thimerosal of 1000ml are as follows:
Coral ginger oil 150ml
Emulsifier 50ml
Glycerine 50ml
95% ethanol 450ml
Distilled water 300ml.
Coral ginger is because of the extracting method difference in the present invention's prescription, and the volatile oil active constituent content has certain discrepancy, differs 2%～8% usually; But require that wherein the pure content of terpinene-4 is greater than 30%, the high more Disinfection Effect of content is good more.
In the above-mentioned thimerosal auxiliary material, emulsifier is a soil temperature, and effect stable and that disperse is arranged, and emulsifier commonly used is a soil temperature 80; Soil temperature 60, soil temperature 40 also can be used; Glycerine has the skin moisten effect; Ethanol and distilled water are solvents.
The preparation method who contains the thimerosal of coral ginger oil of the present invention comprises:
(1) get coral ginger medicinal material, through selection, cleaning, drying is ground into meal, places volatile oil extractor to add water, extracts coral ginger oil with steam distillation, and is standby;
(2) standby coral ginger oil is put in the stainless steel heated, under agitation slowly add soil temperature 80, it is even to be stirred to emulsification, leaves standstill;
(3) by formula rate get glycerine, 95% ethanol is put in the agitator and is stirred, again that previous step emulsification is good coral ginger oil adds in the agitator, continue to mix stir after, place high pressure liquid stream homogenizer homogeneous, filter then;
(4) with the filtrate adding distil water in the 3rd step, the ormal weight that is adjusted to prescription is promptly made the thimerosal that contains coral ginger oil of the present invention; Through after the assay was approved, cannedly go into bottle, packing is dispatched from the factory.
In the above-mentioned first step, the baking temperature after coral ginger medicinal material cleans is 60 ℃, drying time 8h; The meal fineness of pulverizing was 24 mesh sieves; The water quality that adds in the volatile oil extractor is 7 times of coral ginger; The time that steam distillation is extracted coral ginger oil is 5h.
In above-mentioned second step, it is to adopt electromagnetic oven heating that coral ginger oil is put in the stainless steel heating, heating-up temperature to 70 ℃; Time of repose is 24h after the emulsification.
In above-mentioned the 3rd step, glycerine, 95% ethanol put that mixing time is 10min in the agitator; The time that adds coral ginger oil continuation stirring is 30min; Filter type adopts plate basket formula filter press to filter.
The thimerosal that contains coral ginger oil of the present invention almost all has killing action to all bacteriums, test with staphylococcus aureus, Escherichia coli, pseudomonas aeruginosa, candida albicans, under 20 ± 1 ℃ of conditions, it is 0.5min that this thimerosal of 40% is killed staphylococcus aureus action time, the dissipation Escherichia coli are 0.8min, dissipation pseudomonas aeruginosa 1.0min action time, dissipation candida albicans 2.0min action time.
The thimerosal active component that contains coral ginger oil of the present invention is a natural materials, and toxicity own is lower, uses the back degradable, and environmental pollution is minimum; Because of this thimerosal mechanism of action uniqueness, bacterium is difficult to develop immunity to drugs, and service life is long.Be applicable to all-environment sterilization.
Embodiment
Embodiment prepares the thimerosal that contains coral ginger oil of the present invention according to the following step:
(1) get coral ginger medicinal material, pass through selection, clean, at 60 ℃ of following dry 8h, be ground into the meal of 24 mesh sieves, place volatile oil extractor to add water, the water quality of adding is 7 times of coral ginger; Then extract coral ginger oil with steam distillation 5h, standby;
(2) standby coral ginger oil is put in the stainless steel and to be adopted electromagnetic oven heating to 70 ℃, under agitation slowly add soil temperature 80, it is even to be stirred to emulsification, leaves standstill 24h;
(3) by formula rate get glycerine, 95% ethanol is put and is stirred 10min in the agitator, again that previous step emulsification is good coral ginger oil adds in the agitator, continue to mix stir 30min after, place high pressure liquid stream homogenizer homogeneous, filter with plate basket formula filter press then;
(4) with the filtrate adding distil water in the 3rd step, the ormal weight that is adjusted to prescription is promptly made the thimerosal that contains coral ginger oil of the present invention; Through after the assay was approved, cannedly go into bottle, add operation instructions, Product labelling, dispatch from the factory with carton and packed in cases.
For the ease of memory and use, this product called after Sha Shi thimerosal.
Claims (7)
1. a thimerosal that contains coral ginger oil is characterized in that this thimerosal is is main active with the coral ginger oil, after with emulsifier emulsification, and the thimerosal formulated with glycerine, ethanol and distilled water; The component and the consumption thereof of every this thimerosal of 1000ml are as follows:
Coral ginger oil 150ml
Emulsifier 50ml
Glycerine 50ml
95% ethanol 450ml
Distilled water 300ml.
2. according to the described thimerosal that contains coral ginger oil of claim 1, it is characterized in that the pure content of terpinene in the described coral ginger oil-4 is greater than 30%.
3. according to the described thimerosal that contains coral ginger oil of claim 1, it is characterized in that used emulsifier is a soil temperature 80, or soil temperature 60, or soil temperature 40.
4. according to the described compound method that contains the thimerosal of coral ginger oil of claim 1, its feature comprises:
(1) get coral ginger medicinal material, through selection, cleaning, drying is ground into meal, places volatile oil extractor to add water, extracts coral ginger oil with steam distillation, and is standby;
(2) standby coral ginger oil is put in the stainless steel heated, under agitation slowly add soil temperature 80, it is even to be stirred to emulsification, leaves standstill;
(3) by formula rate get glycerine, 95% ethanol is put in the agitator and is stirred, again that previous step emulsification is good coral ginger oil adds in the agitator, continue to mix stir after, place high pressure liquid stream homogenizer homogeneous, filter then;
(4) with the filtrate adding distil water in the 3rd step, the ormal weight that is adjusted to prescription is promptly made the thimerosal that contains coral ginger oil of the present invention.
5. according to the described compound method that contains the thimerosal of coral ginger oil of claim 4, it is characterized in that in the described first step that the baking temperature after coral ginger medicinal material cleans is 60 ℃, drying time 8h; The meal fineness of pulverizing was 24 mesh sieves; The water quality that adds in the volatile oil extractor is 7 times of coral ginger; The time that steam distillation is extracted coral ginger oil is 5h.
6. according to the described compound method that contains the thimerosal of coral ginger oil of claim 4, it is characterized in that coral ginger oil is put and added the thermal recovery electromagnetic oven heating in the stainless steel in described second step, heating-up temperature to 70 ℃; Time of repose is 24h after the emulsification.
7. according to the described compound method that contains the thimerosal of coral ginger oil of claim 4, it is characterized in that in described the 3rd step that glycerine, 95% ethanol put that mixing time is 10min in the agitator; The time that adds coral ginger oil continuation stirring is 30min; Filter type adopts plate basket formula filter press to filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100779877A CN101138346A (en) | 2007-10-30 | 2007-10-30 | Disinfectant liquid containing coral ginger oil and preparing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100779877A CN101138346A (en) | 2007-10-30 | 2007-10-30 | Disinfectant liquid containing coral ginger oil and preparing method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN101138346A true CN101138346A (en) | 2008-03-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA2007100779877A Pending CN101138346A (en) | 2007-10-30 | 2007-10-30 | Disinfectant liquid containing coral ginger oil and preparing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101336966B (en) * | 2008-08-14 | 2011-07-27 | 重庆灵方生物技术有限公司 | Osmidrosis dispelling liniment containing natural essential oil of Zingiber corallinum Hance |
| CN102294045A (en) * | 2011-07-29 | 2011-12-28 | 重庆市超临界精细化工生产力促进中心有限公司 | Air freshener containing Zingiber corallinum Hance essential oil and its preparation method |
| CN102845469A (en) * | 2012-09-03 | 2013-01-02 | 南通博大生化有限公司 | Disinfectant for silver ion water |
| CN105685145A (en) * | 2016-03-18 | 2016-06-22 | 安徽三联泵业股份有限公司 | Disinfectant solution for food pump |
| CN107251920A (en) * | 2017-07-12 | 2017-10-17 | 合肥华盖生物科技有限公司 | It is a kind of for thimerosal of animal husbandry and preparation method thereof |
-
2007
- 2007-10-30 CN CNA2007100779877A patent/CN101138346A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101336966B (en) * | 2008-08-14 | 2011-07-27 | 重庆灵方生物技术有限公司 | Osmidrosis dispelling liniment containing natural essential oil of Zingiber corallinum Hance |
| CN102294045A (en) * | 2011-07-29 | 2011-12-28 | 重庆市超临界精细化工生产力促进中心有限公司 | Air freshener containing Zingiber corallinum Hance essential oil and its preparation method |
| CN102294045B (en) * | 2011-07-29 | 2013-09-25 | 重庆市超临界精细化工生产力促进中心有限公司 | Air freshener containing Zingiber corallinum Hance essential oil and its preparation method |
| CN102845469A (en) * | 2012-09-03 | 2013-01-02 | 南通博大生化有限公司 | Disinfectant for silver ion water |
| CN105685145A (en) * | 2016-03-18 | 2016-06-22 | 安徽三联泵业股份有限公司 | Disinfectant solution for food pump |
| CN107251920A (en) * | 2017-07-12 | 2017-10-17 | 合肥华盖生物科技有限公司 | It is a kind of for thimerosal of animal husbandry and preparation method thereof |
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20080312 |