CN101104001A - Method for manufacturing water soluble pearl powder - Google Patents
Method for manufacturing water soluble pearl powder Download PDFInfo
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- CN101104001A CN101104001A CNA2006100947401A CN200610094740A CN101104001A CN 101104001 A CN101104001 A CN 101104001A CN A2006100947401 A CNA2006100947401 A CN A2006100947401A CN 200610094740 A CN200610094740 A CN 200610094740A CN 101104001 A CN101104001 A CN 101104001A
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Abstract
The invention relates to a production method of water-solution pearl powder. The method is practiced in detail like that the pearl powder is dissolved by edible lactic acid; pearl powder lactic acid solution and undissolved sediment containing pearl protein are produced after the pearl powder is centrifugalized; the sediment is made easy for enzymatic hydrolysis after boiled in a pressure sterilizer, then pearl hydrolysate is produced after the sediment is processed by enzymatic hydrolysis; hereby the water-solution pear powder is produced by the mixture of the pearl hydrolysate and the pearl lactic acid solution. The invention is simple for production and process and high in efficiency, improving the hydrolysis effect of pearl protein (with the hydrolysis rate more than 75 percent). The water-solution pearl powder which is very easy to be digested and absorbed by the body and the skin of a human being is applicable to additive for medicine, nourishment and skin care products.
Description
Technical field
The present invention relates to the Margarita powder processing technique field of a kind of medical or food, used for cosmetic, particularly a kind of manufacture method of water soluble Margarita powder.
Background technology
Margarita is a kind of famous and precious Chinese crude drug, have calm the nerves, make eye bright, the effect of detoxifcation and aesthetic health care.Modern science the analysis showed that Margarita contains nearly 20 seed amino acids, 20 various trace elements, porphyrin and abundant calcium class.But Margarita has the hybrid nanostructured, calcium carbonate sandwich one layer thickness of two-layer nepheline structure is several protein layers to tens nano thickness, this makes Margarita have very high hardness and toughness, with be insoluble in water, therefore usually Margarita is processed into water soluble Margarita powder, so that absorption of human body.The processing method of traditional water dissolving pearl powder is with food acids such as lactic acid Margarita powder to be dissolved, and is diluted to add enzyme behind the finite concentration and be hydrolyzed, then directly with the solution drying.Pearl protein is a glutelin, contains abundant sulfenyl, and structure is tight, the similar hair of character, and extremely difficult by the hydrolysis of enzyme institute, human body is difficult to absorb. and therefore, such processing does not almost act on pearl protein. and prior art is to be difficult to the direct enzyme hydrolysis of pearl protein.
Summary of the invention
The present invention is to be difficult to the direct enzyme hydrolysis of pearl protein is caused the low shortcoming of human absorptivity in order to overcome prior art, and a kind of manufacture method of water soluble Margarita powder is provided.
The technical solution adopted for the present invention to solve the technical problems is: the manufacture method of water soluble Margarita powder,
The step of described method comprises: (1), utilize edible lactic acid that Margarita powder heat in water to dissolve, and solution separates through sedimentation-type centrifuge while hot, must clarify the Margarita lactic acid solution and contain the insoluble precipitum of pearl protein;
(2), the insoluble precipitum of pearl protein is adjusted pH value to 3.0-4.5 with lactic acid, by pressure cooker steaming and decocting 10-24 hour, obtain pastel;
(3), with the pastel thin up, transfer pH value to 6.5-8.5 with 10%Ca (OH) 2 suspensions, reuse alkaline protease (consumption be gross mass 0.05%) was handled 6-8 hour at 45-50 ℃, again through ℃ deactivation, then through decanter type centrifuging and taking clear filtrate;
(4), above-mentioned clear filtrate and Margarita lactic acid solution be heated to 80-100 ℃ mix, obtain water soluble Margarita powder after spray-dried.
The manufacture method that the invention has the beneficial effects as follows water soluble Margarita powder is simple, the efficient height; High cooking under high-temperature and high-pressure conditions makes lactic acid that the pearl protein sulfydryl is loosened, and makes the pearl protein easy hydrolysis that becomes, and has improved pearl protein hydrolysis effect (percent hydrolysis can up to more than 75%).Water soluble Margarita powder is easy to be absorbed by human consumption, also easily by skin absorbs, is suitable for medicine, nutrition and skin care item and uses as additive.
The specific embodiment
Embodiment
In the 100L enamel reactor, with water 40kg, Margarita powder 10kg, be warming up to 100 ℃, slowly add edible lactic acid 18kg while stirring, reinforced finishing constant temperature 30-60 minute, with sufficient reacting, discharging while hot, feed liquid is poured in the sedimentation-type centrifuge settlement separate while hot, 1800 rev/mins of centrifuge speeds, centrifugal 10 minutes, it was standby to get 60.5kg Margarita lactic acid clear liquor; Get the 0.23kg centrifugal deposition.Centrifugal deposition uses 1kg water to mix, and transfers PH to 3.0-4.5 with lactic acid (concentration 80%), is placed on high-pressure sterilizing pot then and presses steaming and decocting 10-24 hour (121 ℃ of pressure 97KPa, temperature), obtains pastel 10%Ca (OH)
2Suspension is transferred PH to 6.5-8.5, places in the enzymatic hydrolysis reaction device, adds gross mass 0.05% alkaline protease, constant temperature 45-50 ℃, constantly stir, reacted 6-8 hour, take out reactant liquor and after sedimentation-type centrifuge centrifugalize (1800 rev/mins), get its clear liquor, obtain the about 1.19kg of clear liquor.The Margarita lactic acid clear liquor that this clear liquor and above-mentioned steps are obtained mixes, and heats 80 to 100 ℃, stirs, and spray drying promptly gets water-soluble fully water soluble Margarita powder.
Manufacture method of the present invention is simple, technology is simple, the efficient height; Improved pearl protein hydrolysis effect (percent hydrolysis can up to more than 75%).Water soluble Margarita powder is easy to be absorbed by human consumption, also easily by skin absorbs, is suitable for medicine, nutrition and skin care item and uses as additive.
Claims (1)
1. the manufacture method of water soluble Margarita powder, it is characterized in that: the step of described method comprises:
(1), utilize edible lactic acid that Margarita powder heat in-depth in water, solution is while hot through the sedimentation-type centrifuge separation, must clarify the Margarita lactic acid solution and contain the insoluble precipitum of pearl protein;
(2), the insoluble precipitum of pearl protein is adjusted pH value to 3.0-4.5 with lactic acid, by pressure cooker steaming and decocting 10-24 hour, obtain pastel;
(3), pastel is added water 5kg dilution, transfer pH value to 6.5-8.5 with 10%Ca (OH) 2 suspensions, reuse alkaline protease (consumption be gross mass 0.05%) was handled 6-8 hour at 45-50 ℃, again through 100 ℃ of deactivations, then through decanter type centrifuging and taking clear filtrate;
(4), above-mentioned clear filtrate and Margarita lactic acid solution be heated to 80-100 ℃ mix, obtain water soluble Margarita powder after spray-dried.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006100947401A CN101104001A (en) | 2006-07-12 | 2006-07-12 | Method for manufacturing water soluble pearl powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006100947401A CN101104001A (en) | 2006-07-12 | 2006-07-12 | Method for manufacturing water soluble pearl powder |
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| Publication Number | Publication Date |
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| CN101104001A true CN101104001A (en) | 2008-01-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA2006100947401A Pending CN101104001A (en) | 2006-07-12 | 2006-07-12 | Method for manufacturing water soluble pearl powder |
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| CN (1) | CN101104001A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018727B (en) * | 2009-09-18 | 2012-06-13 | 桂林莱茵生物科技股份有限公司 | Preparation method of pearl hydrolysate |
| DE102011078260A1 (en) * | 2011-06-29 | 2013-01-03 | Beiersdorf Ag | Cosmetic product e.g. cloth from a composition comprising either an inorganic compound or an extract with inorganic compound, or pearl hydrolyzate and a nonwoven comprising fibers of cotton and/or bamboo |
| CN105998077A (en) * | 2016-05-10 | 2016-10-12 | 赫尔森江苏医药有限公司 | Water-soluble pearl powder and preparation method and application thereof |
| CN106265412A (en) * | 2016-08-04 | 2017-01-04 | 海南京润珍珠生物技术股份有限公司 | A kind of method utilizing probiotics fermention to prepare Margarita hydrolyzed solution |
| CN106511225A (en) * | 2016-11-24 | 2017-03-22 | 湖州珍露生物制品有限公司 | Preparation process of instant pearl powder |
| EP3228625A4 (en) * | 2015-01-15 | 2017-12-13 | Osmun Biological Co., Ltd. | Preparation method for conchiolin, and water-soluble conchiolin and acid-soluble conchiolin prepared by using method |
| CN110368350A (en) * | 2019-07-08 | 2019-10-25 | 海南京润珍珠生物技术股份有限公司 | A kind of one brush is the pearl powder and preparation method thereof of change |
-
2006
- 2006-07-12 CN CNA2006100947401A patent/CN101104001A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018727B (en) * | 2009-09-18 | 2012-06-13 | 桂林莱茵生物科技股份有限公司 | Preparation method of pearl hydrolysate |
| DE102011078260A1 (en) * | 2011-06-29 | 2013-01-03 | Beiersdorf Ag | Cosmetic product e.g. cloth from a composition comprising either an inorganic compound or an extract with inorganic compound, or pearl hydrolyzate and a nonwoven comprising fibers of cotton and/or bamboo |
| EP3228625A4 (en) * | 2015-01-15 | 2017-12-13 | Osmun Biological Co., Ltd. | Preparation method for conchiolin, and water-soluble conchiolin and acid-soluble conchiolin prepared by using method |
| JP2018502151A (en) * | 2015-01-15 | 2018-01-25 | 欧詩漫生物股▲ふん▼有限公司Ｏｓｍ Ｂｉｏｌｏｇｙ Ｃｏ．， Ｌｔｄ． | Method for preparing pearl protein, water-soluble pearl protein and acid-soluble pearl protein prepared by the method |
| CN105998077A (en) * | 2016-05-10 | 2016-10-12 | 赫尔森江苏医药有限公司 | Water-soluble pearl powder and preparation method and application thereof |
| CN106265412A (en) * | 2016-08-04 | 2017-01-04 | 海南京润珍珠生物技术股份有限公司 | A kind of method utilizing probiotics fermention to prepare Margarita hydrolyzed solution |
| CN106265412B (en) * | 2016-08-04 | 2019-03-26 | 海南京润珍珠生物技术股份有限公司 | A method of hydrolyzed pearl solution is prepared using probiotics fermention |
| CN106511225A (en) * | 2016-11-24 | 2017-03-22 | 湖州珍露生物制品有限公司 | Preparation process of instant pearl powder |
| CN110368350A (en) * | 2019-07-08 | 2019-10-25 | 海南京润珍珠生物技术股份有限公司 | A kind of one brush is the pearl powder and preparation method thereof of change |
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Open date: 20080116 |