CN101032456B - Hairdressing combination made of natural vegetable and preparing method thereof - Google Patents
Hairdressing combination made of natural vegetable and preparing method thereof Download PDFInfo
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- CN101032456B CN101032456B CN2007100177694A CN200710017769A CN101032456B CN 101032456 B CN101032456 B CN 101032456B CN 2007100177694 A CN2007100177694 A CN 2007100177694A CN 200710017769 A CN200710017769 A CN 200710017769A CN 101032456 B CN101032456 B CN 101032456B
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Abstract
The natural botanic hairdressing composition consists of hair conditioning emulsion and hair tinting and protecting plant extract. The hair conditioning emulsion consists of C12-C16 alcohol, organic acid, saponifier, surfactant and assistant; and the hair tinting and protecting plant extract is alcohol or water extract of plant garden balsam flower. The said components are mixed and the mixture is treated through regulating pH value, grinding, homogenizing and degassing to prepare the natural botanic hairdressing composition. The natural botanic hairdressing composition may have different kinds of botanic pigments added to obtain hairdressing composition capable of tinting in different colors. The natural botanic hairdressing composition has both hair tinting and hair moistening effects.
Description
Technical field
The invention belongs to the plain technical field of hair caring, relate to a kind of hairdressing combination made of natural vegetable, the invention still further relates to the preparation method of said composition.
Background technology
Along with the raising of living standards of the people, hair dye has progressively been come into the common people as a kind of daily cosmetics that change color development, becomes the performance product of modern self-expression and pursuing individuality.On the one hand, hair dye can make the color development back to nature, remedies some congenital defects or posteriori sorry; On the other hand, as individual character and fashionable interspersing, many people require to change own single hair color, to pursue colorful color development.In recent years, hair dyeing had become the wind direction sign of fashion.But present most of hair dye all is made up of two doses of response types of chemosynthesis, all must use oxidant, and wherein the benzene that is contained, amine all have stimulation to skin, and life-time service can cause certain harm to human body.
At present more and more deep at the applied research aspect the hair dye for plant, it is the botanical hair dye of raw material that states such as France, India have succeeded in developing in succession with the hematoxylin.It is the botanical hair dye of raw material that Japan has also released with capsaicin, shellolic acid, carminic acid etc.China cosmetics expert also dyes black active component to traditional Chinese herbal medicine Galla Chinensis, Radix Polygoni Multiflori, hematoxylin, Semen Sesami Nigrum and Semen sojae atricolor etc. and has carried out broad research.Also having at present several is the hair dye listing of composition with the natural plant pigment, but these are still to have used oxidant in the hair dye of composition with the natural plant pigment, still are double-formulation, can not eliminate the harm to human body fully.
Summary of the invention
The object of the present invention is to provide a kind of hairdressing combination made of natural vegetable, said composition is not used oxidant, has solved the problem that the chemical constituent in the existing hair dye works the mischief to human body fully.
Another object of the present invention is to provide the preparation method of this hairdressing combination made of natural vegetable.
The technical solution adopted in the present invention is, hairdressing combination made of natural vegetable is made up of hair quality conditioning emulsion and natural plants hair dyeing and care extract,
The hair quality conditioning emulsion consists of: C
12～C
16Alcohols, organic acid, saponifier, surfactant and adjuvant, by quality, its proportioning is C
12～C
16Alcohols: organic acid: saponifier: surfactant: adjuvant=7～10: 18～25: 6～10: 1～3: 0.5～0.8;
Natural plants hair dyeing and care extract is the ethanol of Flos Impatientis whole flower or the extract of water.
C wherein
12The alcohols of～C16 is selected from oleyl alcohol, lauryl alcohol, hexadecanol, isopropyl alcohol or propylene glycol.
Wherein organic acid is tannic acid or gallic acid.
Wherein saponifier is triethanolamine or potash soap.
Wherein surfactant is selected from NPE, span or tween.
Wherein adjuvant is selected from essence, thickening agent, stabilizing agent, antioxidant, penetrating agent, chelating agen or wherein two or more combinations.
Wherein chelating agen is different slaine.
Another technical scheme of the present invention is, prepares the method for above-mentioned composition, and above-mentioned composition is made up of hair quality conditioning emulsion and natural plants hair dyeing and care extract,
The hair quality conditioning emulsion consists of: C
12～C
16Alcohols, organic acid, saponifier, surfactant and adjuvant, by quality, its proportioning is C
12～C
16Alcohols: organic acid: saponifier: surfactant: adjuvant=7～10: 18～25: 6～10: 1～3: 0.5～0.8;
Natural plants hair dyeing and care extract is the ethanol of Flos Impatientis whole flower or the extract of water,
This method is made up of following steps,
I, preparation hair quality conditioning emulsion,
A. by above-mentioned quality proportioning, with C
12～C
16Alcohols, organic acid, surfactant add in the reactor and mix, be warmed up to 60～65 ℃,
B. by above-mentioned quality proportioning, get saponifier and add in the deionized water, be heated to 60～65 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 1.5～2.0 hours;
D. the emulsion that step c is obtained is cooled to 40～45 ℃, adds adjuvant, is stirred to airtight preservation after the room temperature;
II, preparation natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. in the ultrasonic extraction device, be the mixed liquor of 50% second alcohol and water with the Impatientis pollen of above-mentioned processing, under 50～70 ℃ of temperature, extracted 0.5～1.5 hour with concentration, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extracts 0.5～1.5 hour under 50～70 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 0.01～1.50kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
III, with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=6.5～13.5: 1～2 mixes in blender, and regulating pH value is 7～9, again through grind, even matter, the degassing, promptly.
Hairdressing combination made of natural vegetable of the present invention adopts natural plant extracts, has avoided the damage of chemical constituent to hair quality, the extract outbreak usefulness of not only having illicit sexual relations, and itself be exactly a kind of Chinese herbal medicine that can moisten hair that contains.Said composition contains hair caring compositions such as profuse natural plants elite tannin, flavonoid, has the effect of nourishing hair, life-time service energy anti-dandruff, anticreep and hair care hair care can enter hair surface scale inside, infiltrate into every hair equably, be beneficial to hair and absorb, improve hair quality.Various nutrient elements can prevent that hair is withered, bifurcated, can prevent chapped skin, and sterilization, antipruritic, anti-dandruff effect are arranged again, recovers natural brilliance, keeps the beautiful color of hair.Energy hair care, hair care are once finished, and colour-fast lastingly.
The specific embodiment
The present invention is described in detail below in conjunction with the specific embodiment.
Hairdressing combination made of natural vegetable of the present invention is made up of hair quality conditioning emulsion and natural plants hair dyeing and care extract.
The hair quality conditioning emulsion consists of:
C
12～C
16Alcohols: be selected from oleyl alcohol, lauryl alcohol, hexadecanol, isopropyl alcohol or propylene glycol.
Organic acid: tannic acid or gallic acid.
Saponifier: triethanolamine or potash soap.
Surfactant: be selected from NPE, span or tween.
Adjuvant: be selected from essence, thickening agent, stabilizing agent, antioxidant, penetrating agent, chelating agen or wherein two or more combinations.
Thickening agent and stabilizing agent can be selected 658 thickening agents, nvp copolymer, carboxymethyl cellulose etc. for use; Antioxidant is mainly phenolic compound, as Butylated hydroxyanisole, vitamin E etc.; Penetrating agent such as Hydroxypropyl methacrylate, JFC etc.; Chelating agen is EDTA etc.
By quality, its proportioning is C
12～C
16Alcohols: organic acid: saponifier: surfactant: adjuvant=7～10: 18～25: 6～10: 1～3: 0.5～0.8.
Natural plants hair dyeing and care extract is the ethanol of Flos Impatientis whole flower or the extract of water.
Also can in prescription provided by the invention, add various plant pigment,, as required, regulate different pH value, can obtain the hair caring element of colors such as brown, chocolate color, claret, golden yellow, brown as Radix Rubiae effective ingredient-alizarin.
Embodiment 1
At first prepare the hair quality conditioning emulsion,
A. get in oleyl alcohol, tannic acid, the span adding reactor by 7: 25: 1 quality proportioning and mix, be warmed up to 60 ℃,
B. get 6 parts triethanolamine by mass ratio and add in the deionized water, be heated to 65 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 1.5 hours;
D. the emulsion that step c is obtained is cooled to 40 ℃, adds essence, thickening agent and stabilizing agent, is stirred to airtight preservation after the room temperature;
Next prepares natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. be the mixed liquor of 50% second alcohol and water with concentration with the Impatientis pollen of above-mentioned processing in the ultrasonic extraction device, extraction is 1.5 hours under 50 ℃ of temperature, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extraction is 1.5 hours under 50 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 0.01kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
Then with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=6.5: 1 mixes in blender, and regulating pH value is 7, again through grind, even matter, the degassing, promptly get the black hairdressing combination made.
Embodiment 2
At first prepare the hair quality conditioning emulsion,
A. get in lauryl alcohol, gallic acid, the tween adding reactor by 10: 18: 3 quality proportioning and mix, be warmed up to 65 ℃,
B. get 10 parts potash soap by mass ratio and add in the deionized water, be heated to 60 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 2 hours;
D. the emulsion that step c is obtained is cooled to 45 ℃, adds thickening agent, antioxidant and penetrating agent, is stirred to airtight preservation after the room temperature;
Next prepares natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. be the mixed liquor of 50% second alcohol and water with concentration with the Impatientis pollen of above-mentioned processing in the ultrasonic extraction device, extraction is 0.5 hour under 70 ℃ of temperature, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extraction is 0.5 hour under 70 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 1.50kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
Then with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=13.5: 2 mixes in blender, add the alizarin pigment, regulating pH value is 9, through grinding, sparing matter, the degassing, promptly gets the claret hairdressing combination made again.
Embodiment 3
At first prepare the hair quality conditioning emulsion,
A. get in hexadecanol, gallic acid, the NPE adding reactor by 8: 20: 2 quality proportioning and mix, be warmed up to 65 ℃,
B. get 8 parts potash soap by mass ratio and add in the deionized water, be heated to 60 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 2 hours;
D. the emulsion that step c is obtained is cooled to 45 ℃, adds essence and chelating agen, is stirred to airtight preservation after the room temperature;
Next prepares natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. be the mixed liquor of 50% second alcohol and water with concentration with the Impatientis pollen of above-mentioned processing in the ultrasonic extraction device, extraction is 1 hour under 60 ℃ of temperature, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extraction is 1 hour under 60 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 1kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
Then with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=10: 1.5 mixes in blender, add the alizarin pigment, regulating pH value is 8, through grinding, sparing matter, the degassing, promptly gets golden yellow hairdressing combination made again.
Embodiment 4
At first prepare the hair quality conditioning emulsion,
A. get in isopropyl alcohol, tannic acid, the tween adding reactor by 9: 23: 2 quality proportioning and mix, be warmed up to 60 ℃,
B. get 7 parts potash soap by mass ratio and add in the deionized water, be heated to 60 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 1.5 hours;
D. the emulsion that step c is obtained is cooled to 40 ℃, adds chelating agen, is stirred to airtight preservation after the room temperature;
Next prepares natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. be the mixed liquor of 50% second alcohol and water with concentration with the Impatientis pollen of above-mentioned processing in the ultrasonic extraction device, extraction is 1 hour under 60 ℃ of temperature, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extraction is 1 hour under 60 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 0.08kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
Then with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=10: 1.5 mixes in blender, add the alizarin pigment, regulating pH value is 8, through grinding, sparing matter, the degassing, promptly gets golden yellow hairdressing combination made again.
Embodiment 5
At first prepare the hair quality conditioning emulsion,
A. get in propylene glycol, tannic acid, the span adding reactor by 9: 23: 2 quality proportioning and mix, be warmed up to 65 ℃,
B. get 7 parts triethanolamine by mass ratio and add in the deionized water, be heated to 65 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 1 hour;
D. the emulsion that step c is obtained is cooled to 45 ℃, add stabilizing agent and antioxidant,, be stirred to airtight preservation after the room temperature;
Next prepares natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. be the mixed liquor of 50% second alcohol and water with concentration with the Impatientis pollen of above-mentioned processing in the ultrasonic extraction device, extraction is 0.5 hour under 65 ℃ of temperature, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extraction is 0.5 hour under 60 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 0.08kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
Then with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=10: 1.5 mixes in blender, add brown pigmentation, regulating pH value is 9, through grinding, sparing matter, the degassing, promptly gets brown hairdressing combination made again.
Claims (5)
1. a hairdressing combination made of natural vegetable is made up of hair quality conditioning emulsion and natural plants hair dyeing and care extract,
Described hair quality conditioning emulsion consists of: C
12～C
16Alcohols, organic acid, saponifier, surfactant and adjuvant, by quality, its proportioning is C
12～C
16Alcohols: organic acid: saponifier: surfactant: adjuvant=7～10: 18～25: 6～10: 1～3: 0.5～0.8;
Described natural plants hair dyeing and care extract is the ethanol of Flos Impatientis whole flower or the extract of water;
C wherein
12The alcohols of～C16 is selected from oleyl alcohol, lauryl alcohol, hexadecanol, isopropyl alcohol or propylene glycol;
Wherein organic acid is tannic acid or gallic acid;
Wherein saponifier is triethanolamine or potash soap;
Wherein surfactant is selected from NPE, span or tween;
Wherein adjuvant is selected from essence, thickening agent, stabilizing agent, antioxidant, penetrating agent, chelating agen or wherein two or more combinations.
2. according to the described compositions of claim 1, wherein chelating agen is different slaine.
3. the described method for compositions of preparation claim 1 is characterized in that described compositions is made up of hair quality conditioning emulsion and natural plants hair dyeing and care extract,
Described hair quality conditioning emulsion consists of: C
12～C
16Alcohols, organic acid, saponifier, surfactant and adjuvant, by quality, its proportioning is C
12～C
16Alcohols: organic acid: saponifier: surfactant: adjuvant=7～10: 18～25: 6～10: 1～3: 0.5～0.8;
Described natural plants hair dyeing and care extract is the ethanol of Flos Impatientis whole flower or the extract of water,
This method is made up of following steps,
I, preparation hair quality conditioning emulsion,
A. by above-mentioned quality proportioning, with C
12～C
16Alcohols, organic acid, surfactant add in the reactor and mix, be warmed up to 60～65 ℃,
B. by above-mentioned quality proportioning, get saponifier and add in the deionized water, be heated to 60～65 ℃,
C. the material that step a and step b are obtained mixes and stirs, and react the one-tenth emulsion 1.5～2.0 hours;
D. the emulsion that step c is obtained is cooled to 40～45 ℃, adds adjuvant, is stirred to airtight preservation after the room temperature;
II, preparation natural plants hair dyeing and care extract,
A. with the flower of raw material Flos Impatientis, cane, leaf through superfine grinding, cross 100 mesh sieves,
B. in the ultrasonic extraction device, be the mixed liquor of 50% second alcohol and water with the Impatientis pollen of above-mentioned processing, under 50～70 ℃ of temperature, extracted 0.5～1.5 hour with concentration, liquor ratio 5: 1,
C. the extract that step b is obtained is cooled to room temperature, and vacuum filtration gets filtrate,
D. 2.5: 1 the extract of filtering residue reuse liquor ratio that step c is produced further extracts, and extracts 0.5～1.5 hour under 50～70 ℃ of temperature, is cooled to room temperature, and vacuum filtration gets filtrate,
E. twice filtrate that step c and steps d are obtained is mixed, and concentrates under 0.01～1.50kPa vacuum, promptly gets Flos Impatientis natural plants hair dyeing and care extract;
III, with above-mentioned two kinds of materials in quality than hair quality conditioning emulsion: the ratio of natural plants hair dyeing and care extract=6.5～13.5: 1～2 mixes in blender, and regulating pH value is 7～9, again through grind, even matter, the degassing, promptly.
4. in accordance with the method for claim 3, it is characterized in that described adjuvant is selected from essence, thickening agent, stabilizing agent, antioxidant, penetrating agent, chelating agen or wherein two or more combinations.
5. in accordance with the method for claim 4, it is characterized in that described chelating agen is different slaine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100177694A CN101032456B (en) | 2007-04-29 | 2007-04-29 | Hairdressing combination made of natural vegetable and preparing method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100177694A CN101032456B (en) | 2007-04-29 | 2007-04-29 | Hairdressing combination made of natural vegetable and preparing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101032456A CN101032456A (en) | 2007-09-12 |
| CN101032456B true CN101032456B (en) | 2010-06-23 |
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|---|---|---|---|
| CN2007100177694A Expired - Fee Related CN101032456B (en) | 2007-04-29 | 2007-04-29 | Hairdressing combination made of natural vegetable and preparing method thereof |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102198058A (en) * | 2010-03-24 | 2011-09-28 | 北京世纪博康医药科技有限公司 | Herbal hair dye |
| CN102225043B (en) * | 2011-06-20 | 2012-05-30 | 张雯虹 | Henna hair nourishing cream and preparation method thereof |
| CN103655435B (en) * | 2013-04-28 | 2015-08-26 | 钱臻 | A kind of biofermentation hair conditioner and preparation method thereof |
| CN104095784A (en) * | 2014-06-27 | 2014-10-15 | 广西大学 | Anti-dandruff and antipruritic shampoo |
| CN105232418A (en) * | 2015-11-25 | 2016-01-13 | 济南昊泽环保科技有限公司 | Hair dye without oxidizing agent and preparing method of hair dye |
| CN105380892A (en) * | 2015-12-21 | 2016-03-09 | 济南益豪环保技术有限公司 | Composite single-agent-type hair dye |
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2007
- 2007-04-29 CN CN2007100177694A patent/CN101032456B/en not_active Expired - Fee Related
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