CN101003756A - Synthetized diesel oil - Google Patents
Synthetized diesel oil Download PDFInfo
- Publication number
- CN101003756A CN101003756A CN 200710000280 CN200710000280A CN101003756A CN 101003756 A CN101003756 A CN 101003756A CN 200710000280 CN200710000280 CN 200710000280 CN 200710000280 A CN200710000280 A CN 200710000280A CN 101003756 A CN101003756 A CN 101003756A
- Authority
- CN
- China
- Prior art keywords
- diesel oil
- parts
- oil
- solvent
- kilograms
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002283 diesel fuel Substances 0.000 title claims abstract description 80
- 239000002904 solvent Substances 0.000 claims abstract description 28
- 239000000654 additive Substances 0.000 claims abstract description 20
- 230000000996 additive effect Effects 0.000 claims abstract description 20
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims abstract description 14
- 239000003350 kerosene Substances 0.000 claims abstract description 12
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 claims abstract description 9
- KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims abstract description 9
- DLINORNFHVEIFE-UHFFFAOYSA-N hydrogen peroxide;zinc Chemical compound [Zn].OO DLINORNFHVEIFE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940105296 zinc peroxide Drugs 0.000 claims abstract description 9
- 239000003921 oil Substances 0.000 claims description 31
- 238000012986 modification Methods 0.000 claims description 15
- 230000004048 modification Effects 0.000 claims description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 14
- 230000008774 maternal effect Effects 0.000 claims description 14
- 229910052799 carbon Inorganic materials 0.000 claims description 13
- 238000002360 preparation method Methods 0.000 claims description 8
- 229910002651 NO3 Inorganic materials 0.000 claims description 7
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 7
- -1 isooctyl Chemical group 0.000 claims description 7
- 238000000034 method Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 239000002131 composite material Substances 0.000 abstract 2
- NNKQLUVBPJEUOR-UHFFFAOYSA-N 3-ethynylaniline Chemical compound NC1=CC=CC(C#C)=C1 NNKQLUVBPJEUOR-UHFFFAOYSA-N 0.000 abstract 1
- 239000000047 product Substances 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 239000002551 biofuel Substances 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000007084 catalytic combustion reaction Methods 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Lubricants (AREA)
Abstract
This invention relates to synthetic diesel oil, which is produced by: (1) mixing isooctyl nitrate 30 wt.%, cyclohexylamine 30 wt.%, ferrocene 30 wt.%, and zinc peroxide 10 wt.% to obtain composite additive; (2) mixing fossil-grade diesel oil 10-40 parts and the composite additive 0.3-2 parts to obtain mother diesel oil; (3) mixing 200# solvent oil 10-30 parts and lightweight aviation kerosene 5-20 parts to obtain modified 200# solvent oil; (4) mixing fatty acid methyl ester or C9 10-60 parts, the mother diesel oil and the modified 200# solvent oil to obtain the synthetic diesel oil. The synthetic diesel oil has such advantages as low cost, simple process and abundant raw materials, and can be used for replacing standard fossil-grade diesel oil.
Description
Technical field
The present invention relates to a kind of diesel oil substitute products, relate to a kind of combined diesel oil particularly.
Background technology
Diesel oil has a wide range of applications in every field as a kind of energy, but because crude oil is non-renewable resource, increase along with the crude oil energy consumption, the a lot of countries in the world all generally are faced with the situation of energy shortage even shortage, make and the high enterprise of energy prices had a strong impact on expanding economy in China.Therefore develop energy, exploitation substitute energy by all kinds of means, the use cost that improve utilization efficiency of energy, reduces the energy is the problem that people generally face.
Summary of the invention
The objective of the invention is at the problems referred to above, provide a kind of cost low, preparation is simple, the combined diesel oil that is used for alternate standard diesel oil of wide material sources.
For achieving the above object, technical scheme of the present invention is: a kind of combined diesel oil, and it follows these steps to formulated: 1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get 10～40 parts of fossil standard diesel oil and above-mentioned additive by weight and be deployed into maternal diesel oil for 0.3～2 part; 3) get 10～30 parts of 200# solvent oils and become modification 200# solvent oil with 5～20 parts of mixing preparations of lightweight aviation kerosene; 4) getting 9 10～60 parts in fatty acid methyl ester or carbon mixes with maternal diesel oil of preparing above and modification 200# solvent oil and is deployed into combined diesel oil.
In described step 2) in add 20～30 parts of fossil standard diesel oil, add 1～1.6 part of additive; In step 3), add 15～22 parts of 200# solvent oils, add 10～15 parts of lightweight aviation kerosenes; 9 30～50 parts in fatty acid methyl ester that in step 4), adds or carbon.
Described fossil standard diesel oil be 0# diesel oil ,-10# diesel oil or-15# diesel oil.
Density 0.80～the 0.82kg/l of described lightweight aviation kerosene
3
Fatty acid methyl ester is commonly called as and is biofuel, when biofuel is difficult to buy or market value when higher, can replace with the carbon nine of equivalent, and carbon nine adopts commercially available industrial carbon nine to get final product.The two selects for use different, bring variation can for the density of combined diesel oil, under the room temperature, the density of carbon nine than high 0.03 measure unit of fatty acid methyl ester about.So, the combined diesel oil density of producing with carbon nine is higher slightly than the combined diesel oil density of producing with fatty acid methyl ester, but do not influence the quality of combined diesel oil, the two can guarantee that all the quality product of producing meets fossil diesel fuel GB GB252-2000 requirement; The lightweight aviation kerosene has the chemical property similar to fossil diesel fuel, it is heightened the quality of combined diesel oil except rising in this prescription, other two kinds of effects are because its proportion is low and flash-point is higher, it plays the effect of adjusting combined diesel oil proportion and flash-point simultaneously in this prescription, therefore, as long as satisfy density 0.80～0.82 * 10
3Kg/m
3, flash-point all can at the arbitrary aviation kerosene more than 60 ℃; Come the fossil diesel fuel of corresponding selection according to the combined diesel oil label of producing with label.As, just should select the 0# fossil diesel fuel if will select to produce the 0# combined diesel oil.
Combined diesel oil of the present invention is owing to added a large amount of fatty acid methyl esters or carbon nine, and fatty acid methyl ester can utilize reproducible oil product of animals and plants wet goods and waste reclaimation such as sewer oil, swill oil and waste oil pin to make, and carbon nine, 200# solvent oil are the byproducts of oil, the cost of these raw materials is significantly less than the cost of standard diesel oil, thereby combined diesel oil cost of the present invention also will be significantly less than the cost of standard diesel oil, while has saved resource again and has realized the recyclable regenerative utilization of the energy, is the ideal product that substitutes common standard diesel oil.The additive that adds in combined diesel oil has smoke-eliminating combustion-aid, anti-old inhibition, improves cetane value combined diesel oil, increases stability and guarantees that its trouble-free burning in engine has prograding, ferrocene (C wherein
5H
5)
2Fe and zinc peroxide have been realized the catalyticcombustion of combined diesel oil having reduced the discharging of tail gas and particulate matter, have saved the energy, have improved the environment protection ability; Combined diesel oil production technique of the present invention is simple, is convenient to form modularization production.Show after testing, the every physical and chemical index of combined diesel oil of the present invention meets the GB252-2000 national standard fully, and following data are on November 7th, 2006 in the detection data of the 0# combined diesel oil of Research Institute of Petro-Chemical Engineering's analytical test gained (component: 0.3 part of 50 parts of fatty acid methyl esters, 10 parts in coal of boat, 14.7 parts of 200# solvent oils, 25 parts of 0# standard diesel oil and additive):
| Project name | The component title | Analytical data | Method standard |
| Density (20 ℃) | 0.8438g/cm 3 | SH/T 0604 | |
| Viscosity (20 ℃) | 3.960mm 2/s | GB/T 265 | |
| Boiling range | Initial boiling point | 153.5℃ | GB/T 6536 |
| 05％ | 165.0℃ | GB/T 6536 | |
| 10％ | 172.5℃ | GB/T 6536 | |
| 30％ | 221.8℃ | GB/T 6536 | |
| 50％ | 299.8℃ | GB/T 6536 | |
| 70％ | 326.9℃ | GB/T 6536 | |
| 90％ | 343.5℃ | GB/T 6536 | |
| 95％ | 343.5℃ | GB/T 6536 | |
| Final boiling point | 343.5℃ | GB/T 6536 | |
| Acid number | 12.71mgKOH/g | GB/T 264 | |
| Mechanical impurity | Do not have | GB/T 511 | |
| Color | 1.0 look number | GB/T 6540 | |
| Flash-point (remaining silent) | 55℃ | GB/T 261 | |
| Zero pour | -16℃ | GB/T 510 | |
| Condensation point | -9℃ | SH/T 0248 | |
| Copper corrosion (50 ℃, | The 1a level | GB/T 5096 | |
| Ash content | 0.003％ | GB/T 508 | |
| 10% carbon residue | 0.3％ | GB/T 17144 | |
| S content | 68mg/L | SH/T 0253-92 |
| Water-content | 210ppm | SH/T 0246-92 | |
| Cetane value | 51.1 | GB/T 386-91 |
Embodiment
The invention will be further described below in conjunction with specific embodiment.
Embodiment 1:
1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get 40 kilograms of 0# fossil standard diesel oil and above-mentioned additive by weight and be deployed into maternal diesel oil for 0.3 kilogram; 3) get 10 kilograms of 200# solvent oils and become modification 200# solvent oil with 20 kilograms of mixing preparations of lightweight aviation kerosene; 4) getting 10 kilograms of fatty acid methyl esters mixes with a maternal diesel oil of preparing above of kilogram and a kilogram modification 200# solvent oil and is deployed into the 0# combined diesel oil.
Embodiment 2:
1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get by weight-10 kilograms of 10# fossil standard diesel oil are deployed into maternal diesel oil for 2 kilograms with above-mentioned additive; 3) get 30 kilograms of 200# solvent oils and become modification 200# solvent oil with 5 kilograms of mixing preparations of lightweight aviation kerosene; 4) getting 60 kilograms of fatty acid methyl esters mixes with 12 kilograms of maternal diesel oil preparing above and 35 kilograms of modification 200# solvent oils and is deployed into 107 kilograms-10# combined diesel oil.
Embodiment 3:
1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get by weight-30 kilograms of 15# fossil standard diesel oil are deployed into maternal diesel oil for 1 kilogram with above-mentioned additive; 3) get 15 kilograms of 200# solvent oils and become modification 200# solvent oil with 15 kilograms of mixing preparations of lightweight aviation kerosene; 4) getting 9 30 kilograms in industrial carbon mixes with 31 kilograms of maternal diesel oil preparing above and 30 kilograms of modification 200# solvent oils and is deployed into 91 kilograms-15# combined diesel oil.
Embodiment 4:
1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get 20 kilograms of 0# fossil standard diesel oil and above-mentioned additive by weight and be deployed into maternal diesel oil for 1.6 kilograms; 3) get 22 kilograms of 200# solvent oils and become modification 200# solvent oil with 10 kilograms of mixing preparations of lightweight aviation kerosene; 4) getting 9 50 kilograms in industrial carbon mixes with 21.6 kilograms of maternal diesel oil preparing above and 32 kilograms of modification 200# solvent oils and is deployed into 103.6 kilograms of 0# combined diesel oils.
Embodiment 5:
1) by weight with isooctyl ester nitrate 30%, hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get 25 kilograms of 0# fossil standard diesel oil and above-mentioned additive by weight and be deployed into maternal diesel oil for 0.3 kilogram; 3) get 14.7 kilograms of 200# solvent oils and become modification 200# solvent oil with 10 kilograms of mixing preparations of lightweight aviation kerosene; 4) getting 50 kilograms of fatty acid methyl esters mixes with 25.3 kilograms of maternal diesel oil preparing above and 24.7 kilograms of modification 200# solvent oils and is deployed into double centner 0# combined diesel oil.
Describe the present invention with way of example above, but the invention is not restricted to above-mentioned specific embodiment, all protection domains that all belongs to claim of the present invention based on any improvement that the present invention did or modification.
Claims (4)
1. combined diesel oil is characterized in that following these steps to formulated: 1) by weight with isooctyl ester nitrate 30%, and hexahydroaniline 30%, ferrocene 30% and zinc peroxide 10% is hybridly prepared into additive; 2) get 10～40 parts of fossil standard diesel oil and above-mentioned additive by weight and be deployed into maternal diesel oil for 0.3～2 part; 3) get 10～30 parts of 200# solvent oils and become modification 200# solvent oil with 5～20 parts of mixing preparations of lightweight aviation kerosene; 4) getting 9 10～60 parts in fatty acid methyl ester or carbon mixes with maternal diesel oil of preparing above and modification 200# solvent oil and is deployed into combined diesel oil.
2. combined diesel oil according to claim 1 is characterized in that: in described step 2) in add 20～30 parts of fossil standard diesel oil, add 1～1.6 part of additive; In step 3), add 15～22 parts of 200# solvent oils, add 10～15 parts of lightweight aviation kerosenes; 9 30～50 parts in fatty acid methyl ester that in step 4), adds or carbon.
3. combined diesel oil according to claim 1 and 2 is characterized in that: described fossil standard diesel oil be 0# diesel oil ,-10# diesel oil or-15# diesel oil.
4. combined diesel oil according to claim 1 and 2 is characterized in that: the density 0.80～0.82kg/l of described lightweight aviation kerosene
3
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100002806A CN100569928C (en) | 2007-01-18 | 2007-01-18 | Combined diesel oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100002806A CN100569928C (en) | 2007-01-18 | 2007-01-18 | Combined diesel oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101003756A true CN101003756A (en) | 2007-07-25 |
| CN100569928C CN100569928C (en) | 2009-12-16 |
Family
ID=38703140
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007100002806A Expired - Fee Related CN100569928C (en) | 2007-01-18 | 2007-01-18 | Combined diesel oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100569928C (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102051238A (en) * | 2009-10-27 | 2011-05-11 | 北京清研利华石油化学技术有限公司 | Methanol denaturation additive and preparation method thereof |
| CN101565644B (en) * | 2009-06-02 | 2011-12-14 | 李金城 | Synthetic diesel oil |
| CN102382691A (en) * | 2010-08-30 | 2012-03-21 | 东莞市智造生物科技有限公司 | Highly clean biodiesel |
| CN101649241B (en) * | 2009-09-07 | 2013-03-13 | 贵州黄帝车辆净化器有限公司 | Diesel vehicle tail gas collecting regenerated additive and preparation thereof |
| CN103013590A (en) * | 2012-12-20 | 2013-04-03 | 北京清研利华石油化学技术有限公司 | Methanol diesel oil and preparation method thereof |
| CN103113941A (en) * | 2013-02-26 | 2013-05-22 | 宁夏易欣能源科技有限公司 | Additive for production of diesel from condensate oil and preparation method thereof |
| CN103146422A (en) * | 2013-02-26 | 2013-06-12 | 宁夏易欣能源科技有限公司 | Method for producing common diesel mainly from condensate oil |
| CN103160343A (en) * | 2013-04-10 | 2013-06-19 | 刘伟 | Synthetic diesel and preparation method thereof |
| CN103421553A (en) * | 2013-04-11 | 2013-12-04 | 襄阳客瑞客化工科技有限公司 | Diesel additive of energy conservation and emission reduction |
| CN103865593A (en) * | 2014-03-19 | 2014-06-18 | 常胜 | Methyl diesel |
| CN103881771A (en) * | 2014-01-28 | 2014-06-25 | 四川华信能源集团有限公司 | Methyl ester diesel and production method thereof |
| CN104877715A (en) * | 2015-04-20 | 2015-09-02 | 刘敏 | Synthetic diesel oil and synthesis process thereof |
| CN107868684A (en) * | 2017-11-24 | 2018-04-03 | 桂林市雁山区青少年活动中心 | A kind of biodiesel additive and preparation method thereof |
| CN110157500A (en) * | 2019-03-22 | 2019-08-23 | 山东京博石油化工有限公司 | A kind of yacht special oil |
| CN110551538A (en) * | 2019-09-06 | 2019-12-10 | 赵广敏 | oil-saving emission-reducing diesel detergent and preparation method thereof |
-
2007
- 2007-01-18 CN CNB2007100002806A patent/CN100569928C/en not_active Expired - Fee Related
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101565644B (en) * | 2009-06-02 | 2011-12-14 | 李金城 | Synthetic diesel oil |
| CN101649241B (en) * | 2009-09-07 | 2013-03-13 | 贵州黄帝车辆净化器有限公司 | Diesel vehicle tail gas collecting regenerated additive and preparation thereof |
| CN102051238A (en) * | 2009-10-27 | 2011-05-11 | 北京清研利华石油化学技术有限公司 | Methanol denaturation additive and preparation method thereof |
| CN102382691B (en) * | 2010-08-30 | 2013-12-18 | 东莞市智造生物科技有限公司 | Highly clean biodiesel |
| CN102382691A (en) * | 2010-08-30 | 2012-03-21 | 东莞市智造生物科技有限公司 | Highly clean biodiesel |
| CN103013590A (en) * | 2012-12-20 | 2013-04-03 | 北京清研利华石油化学技术有限公司 | Methanol diesel oil and preparation method thereof |
| CN103113941A (en) * | 2013-02-26 | 2013-05-22 | 宁夏易欣能源科技有限公司 | Additive for production of diesel from condensate oil and preparation method thereof |
| CN103146422A (en) * | 2013-02-26 | 2013-06-12 | 宁夏易欣能源科技有限公司 | Method for producing common diesel mainly from condensate oil |
| CN103113941B (en) * | 2013-02-26 | 2015-04-01 | 宁夏易星能源科技开发有限公司 | Additive for production of diesel from condensate oil and preparation method thereof |
| CN103160343B (en) * | 2013-04-10 | 2014-08-06 | 刘伟 | Synthetic diesel and preparation method thereof |
| CN103160343A (en) * | 2013-04-10 | 2013-06-19 | 刘伟 | Synthetic diesel and preparation method thereof |
| CN103421553A (en) * | 2013-04-11 | 2013-12-04 | 襄阳客瑞客化工科技有限公司 | Diesel additive of energy conservation and emission reduction |
| CN103881771A (en) * | 2014-01-28 | 2014-06-25 | 四川华信能源集团有限公司 | Methyl ester diesel and production method thereof |
| CN103865593A (en) * | 2014-03-19 | 2014-06-18 | 常胜 | Methyl diesel |
| CN104877715A (en) * | 2015-04-20 | 2015-09-02 | 刘敏 | Synthetic diesel oil and synthesis process thereof |
| CN107868684A (en) * | 2017-11-24 | 2018-04-03 | 桂林市雁山区青少年活动中心 | A kind of biodiesel additive and preparation method thereof |
| CN110157500A (en) * | 2019-03-22 | 2019-08-23 | 山东京博石油化工有限公司 | A kind of yacht special oil |
| CN110551538A (en) * | 2019-09-06 | 2019-12-10 | 赵广敏 | oil-saving emission-reducing diesel detergent and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100569928C (en) | 2009-12-16 |
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