CN100591631C - Pearl small-micelle water as well as making method and uses thereof - Google Patents

Pearl small-micelle water as well as making method and uses thereof Download PDF

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CN100591631C
CN100591631C CN200610165456A CN200610165456A CN100591631C CN 100591631 C CN100591631 C CN 100591631C CN 200610165456 A CN200610165456 A CN 200610165456A CN 200610165456 A CN200610165456 A CN 200610165456A CN 100591631 C CN100591631 C CN 100591631C
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pearl
small
water
micelle water
micelle
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CN101205095A (en
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蔡继业
赵毅
陈险峰
陈俊岭
汪晨熙
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Guangdong Junfeng BFS Co., Ltd.
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Guangdong Junfeng Investment Co Ltd
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Abstract

The invention discloses small molecular mass water of a pearl, a manufacturing method and application thereof, wherein, the method includes the following steps: firstly, grinding material, pure pearlsor pearl conch, into ultrafine powder; then mixing the ultrafine powder with the water and hydrolyzing thermally under alkalescent condition; adjusting pH value; disinfecting by ozone; filtering andpurifying; then activating as the small molecular mass water of the pearl by using an infrared wave field or an AC electromagnetic field conforming with a spectrum field of human body. The invention combines beneficial elements and nutrients in the pearls with the small molecular mass water so that the beneficial elements so as to be easier to be absorbed by the human body. The small molecular mass water of the pearl can be applied to the fields of drinking, medical treatment, cosmetology, bath and breeding industry.

Description

Pearl small-micelle water and preparation method thereof and application
Technical field
The present invention relates to a kind of small-micelle water and preparation method thereof and use, relate in particular to utilize pearl powder and utilize bionics principle and infrared waves or ac magnetic field prepare pearl small-micelle water method and drink, the application of medical treatment, beauty treatment or aquaculture.
Background technology
Water is Source of life, and more than 70% of percentage of liveweight in human body, water is intravital all the vital movement processes of participant almost, comprises that the element that various vital movements are essential is transported to each organ of human body.The polar molecule that water is made up of the hydrogen-oxygen atom, common form with more than ten the molecular molecular groupings of moisture exists under the room temperature.
Several nanometers being arranged to the aperture of tens nanometer on the cell of human body, is cell and extraneous alternative passage, and the size distribution figure that can measure the ultrastructure of cell surface and obtain the hole with high-resolution atomic force microscope (sees Fig. 2 and shown in Figure 3; Fig. 2 is the ultrastructure with the erythrocyte membrane surface of atomic force microscope measurement, the existence of the microtexture of erythrocyte surface and film surface aperture as can be seen, and the size of aperture is about several nanometers to tens nanometer range, and the diameter of most of micropores is in 12 nanometers; Fig. 3 is that the most of diameters of orifice size on the dried cell membrane of embryo (ES) surface are 45 nanometers as can be seen with the ultrastructure on embryo (ES) the stem cell membrane surface of atomic force microscope measurement.) because the Ultrastructural restriction of cell surface, big water clusters is not easy to pass in and out cell, is unfavorable for cell and extraneous exchanging, and the easier turnover cell of small-micelle water, and with nutritive ingredient input and metabolite output cell.
Human body is lived in the electromagnetic field of the earth, and human body itself also has electromagnetic field, and as electrocardiogram(ECG, electroencephalogram, clectrogastrogram etc., having recorded human body at present has the biological spectrum field in 0.1-100 hertz frequency scope and at infrared band.
Pearl is used as the valuable ingredients of traditional Chinese medicine since ancient times, is applied to health care nutriment and makeup.In the Compendium of Material Medica of Ming Dynasty's LI Shi-Zhen, put down in writing pearl powder and had " controlling order profit flesh skin ", " peace soul; arresting convulsion is throbbed with fear ", " towards the variola poison ", " controlling dysphoria with smothery sensation " ... etc. effect, in " legendary god of farming's hundred grass warps ", treatise on Febrile Diseases, " Jinkui Yaolue ", all on the books to the effect of pearl.Aspect modern medicine, in, the clinical trial certificate of state such as U.S., day, the European Community, pearl powder is effective in cure to diseases such as cardiovascular diseases, hepatitis, asthma, nervous disorders.
Simultaneously, contain the element and the nutritive substance of various needed by human such as calcium, manganese, zinc, iron and amino acid in the pearl powder, how more effectively to allow these nutritive ingredients of absorption of human body be research key issue.
Summary of the invention
An object of the present invention is to provide a kind of making method that contains the pearl small-micelle water of mineral substance,, form pearl water, use again with the electromagnetic field of human body close frequencies and handle pearl water the mineral substance water dissolution in the mother pearl shellfish powder.Will form by positively charged ions such as mineral element such as calcium, manganese, zinc, iron is core, mixes the small-micelle water that polar water molecules is formed---pearl small-micelle water on every side, makes that the mineral substance that contains in pearl or the mother pearl shellfish is easier to be absorbed by the body.
Another object of the present invention provides a kind of making method that contains the pearl small-micelle water of amino acid and mineral substance, makes each seed amino acid in the pearl and mineral substance etc. nutritive ingredient is easier to be absorbed by the body.
For achieving the above object, the invention provides the making method of pearl small-micelle water, may further comprise the steps:
Step 1, pulverizing: pure pearl of raw material or mother pearl shellfish pulverizing are made ultrafine powder, and granularity is less than 10 μ m;
Step 2, hydrolysis: the ultrafine powder after will pulverizing is revolved in the stirring at turbine with pure water and is mixed, and the total cation concentration range adds alkaline solution in the control solution liquid between 0.10-10mmol/L, regulates pH value between 10-14, heating hydrolysis;
Step 3, adjusting pH value: adding lactic acid or citric acid are neutralized to the pH value between 5-6 in the solution after hydrolysis;
Step 4, filtration, purification: the aqueous solution that will mix up the pH value filters, and obtains pearl water stoste;
Step 5, activation: pearl water stoste is passed in infrared light wave field or ac magnetic field, form constitutionally stable pearl small-micelle water.
The making method of above-mentioned pearl small-micelle water, wherein step 4 can also comprise: feed ozone and carry out disinfection and the charcoal absorption purification; Can also comprise a step after the step 5: dilute 100 to 1000 times.
The making method of above-mentioned pearl small-micelle water, alkaline solution is KOH solution or NaHCO in the wherein said step 2 3Solution.
When raw material in the step 1 was pure pearl, the mode of heating hydrolysis was in the step 2: temperature is lower than 80 ℃, hydrolysis 2 hours.
When raw material in the step 1 was mother pearl shellfish, the mode of heating hydrolysis was in the step 2: temperature is 100 ℃-150 ℃, hydrolysis 1 hour.
When choosing infrared waves in the step 5, wavelength region is the 1-25 micron; When selecting ac magnetic field for use, range of frequency is the 50-100 hertz.
When raw material described in the step 1 was pure pearl, the nutritive substance that the pearl small-micelle water of made contains comprised calcium, magnesium, manganese, potassium and amino acid; When described raw material was mother pearl shellfish, the nutritive substance that the pearl small-micelle water of made contains comprised calcium, magnesium, manganese and potassium.
Pearl small-micelle water described in the step 5 17The halfwidth of O nuclear magnetic resonance spectrum is in 30-70 hertz scope.
Pearl small-micelle water described in the present invention can be applied to drink, medical treatment, beauty treatment and aquaculture.
When described pearl small-micelle water is applied to bottled drinking water, becoming bottled drinking water through the pearl small-micelle water can after will diluting on ozone sterilization and the disinfectant streamline.
The present invention also provides a kind of pearl small-micelle water that utilizes above-mentioned making method to make.
The pearl small-micelle water that the present invention makes is absorbed by the body easily, and the nutritive elements such as mineral substance of the needed by human that contains in the pearl effectively can be transported in the cell.
Description of drawings
Fig. 1 is the making method process flow diagram of pearl small-micelle water of the present invention;
Fig. 2 is the ultrastructure with the erythrocyte membrane surface of atomic force microscope measurement;
Fig. 3 is the ultrastructure with embryo (ES) the stem cell membrane surface of atomic force microscope measurement.
Embodiment
Do elaborating by the following examples, but not as a limitation of the invention.
Embodiment 1:
With reference to the making method process flow diagram of figure 1 pearl small-micelle water, adopt the making raw material of pure pearl as pearl small-micelle water, may further comprise the steps:
Step 1, pulverizing: remove variegated pearl, dry in drying machine after the pearl of picking out is cleaned with water purification, make Margarita ultrafine powder with the comminution by gas stream technology less than 10 μ m;
Step 2, basic hydrolysis: the Margarita ultrafine powder after will pulverizing mixes in turbine stirrer with pure water, and the total cation concentration range adds alkaline solution (KOH or NaHCO at 0.10-10mmol/L in the control Margarita liquid 3), regulate pH value between 10-14, heating hydrolysis, temperature is lower than 80 ℃, hydrolysis 2 hours;
Step 3, adjusting pH value: adding lactic acid or citric acid are neutralized to pH value between 5-6 in the solution after hydrolysis;
Step 4, sterilization and filtration, purification: feed streams of ozone sterilization, filtration and active carbon purifying, obtain to contain the pearl water stoste of mineral substance such as nutritive substances such as calcium, manganese and zinc and each seed amino acid;
Step 5, activation: pearl water stoste is passed in infrared light wave field or ac magnetic field (wavelength is that 1-25 micron or frequency are the 50-100 hertz), form constitutionally stable pearl small-micelle water, its 17The halfwidth of O nuclear magnetic resonance spectrum is in 30-70 hertz scope;
Step 6, with 100 to 1000 times of the pearl crude liquid after above-mentioned activation dilutions.
The pearl small-micelle water that this method is made removes and contains calcium, and zinc outside the element of various needed by human such as manganese, also contains the nutritive substances such as each seed amino acid that comprise in the pearl; Can be applied to drink, medical treatment, beauty treatment or aquaculture; When being applied to bottled drinking water, it further comprises following steps:
Step 7, the pearl small-micelle water can is being become bottled drinking water through on ozone sterilization and the disinfectant streamline.
Embodiment 2:
When the finished product being used for beauty treatment or aquaculture, its step is compared with embodiment 1, and the streams of ozone sterilization and the active carbon purifying that can remove in the step 4 are handled.
Embodiment 3:
With reference to the making method process flow diagram of figure 1 pearl small-micelle water, adopt the making raw material of mother pearl shellfish as pearl small-micelle water, may further comprise the steps:
Step 1, the mother pearl shellfish picked out cleaned with water purification after, dry in drying machine, make ultra-fine pearl mother Bei Fen with the comminution by gas stream technology less than 10 μ m;
Step 2, the female Bei Fen of the ultra-fine pearl after will pulverizing mix in the turbine whirler with pure water, in the control Margarita liquid total cation concentration range at 0.10-10mmol/L, adding alkaline solution (KOH or NaHCO 3), regulate pH value between 10-14, heating hydrolysis, temperature is 100 ℃~150 ℃, hydrolysis 1 hour;
Adding lactic acid or citric acid are neutralized to pH value between 5-6 in step 3, the solution after hydrolysis;
Step 4, the sterilization of feeding streams of ozone, filtration and active carbon purifying are removed impurity such as organism, obtain to contain the pearl water stoste of mineral substance such as calcium, manganese and zinc etc.
Step 5, pearl water stoste is passed in infrared light wave field or ac magnetic field (wavelength is that 1-25 micron or frequency are the 50-100 hertz), forming the more stable pearl small-micelle water of structure, its 17The halfwidth of O nuclear magnetic resonance spectrum is in 30-70 hertz scope.
Step 6, with 100 to 1000 times of the pearl crude liquid after above-mentioned activation dilutions.
The pearl small-micelle water that this method is made contains calcium, zinc, and the element of various needed by human such as manganese can be applied to drink, medical treatment, beauty treatment or aquaculture; When being applied to bottled drinking water, it further comprises following steps:
Step 7, the pearl small-micelle water can is being become bottled drinking water through on ozone sterilization and the disinfectant streamline.
Embodiment 4:
When the finished product being used for beauty treatment or aquaculture, its step is compared with embodiment 3, and the streams of ozone sterilization and the active carbon purifying that can remove in the step 4 are handled.
It should be noted last that, above embodiment is the unrestricted technical scheme of the present invention in order to explanation only, although the present invention is had been described in detail with reference to the foregoing description, will be understood by those skilled in the art that: still can make amendment or be equal to replacement the present invention, and do not break away from any modification or partial replacement of the spirit and scope of the present invention, all should contain within the scope of the invention.

Claims (9)

1, a kind of making method of pearl small-micelle water is characterized in that may further comprise the steps:
Step 1, pulverizing: pure pearl of raw material or mother pearl shellfish pulverizing are made ultrafine powder, and granularity is less than 10 μ m;
Step 2, hydrolysis: the ultrafine powder after will pulverizing is mixed with pure water, and the total cation concentration range adds alkaline solution in the control solution between 0.10-10mmol/L, regulates the pH value between 10-14, heating hydrolysis; Described alkaline solution is KOH solution or NaHCO 3Solution;
Step 3, adjusting pH value: adding lactic acid or citric acid are neutralized to the pH value between 5-6 in the solution after hydrolysis;
Step 4, filtration, purification: the aqueous solution that will mix up the pH value filters, and obtains pearl water stoste;
Step 5, activation: pearl water stoste is passed in infrared light wave field or ac magnetic field, form constitutionally stable pearl small-micelle water; Described pearl small-micelle water 17The halfwidth of O nuclear magnetic resonance spectrum is in 30-70 hertz scope.
2, the making method of pearl small-micelle water according to claim 1, wherein step 4 also comprises: feed ozone and carry out disinfection and the charcoal absorption purification; Also comprise a step after the step 5: dilute 100 to 1000 times.
3, the making method of pearl small-micelle water according to claim 1 and 2, when raw material was pure pearl in the wherein said step 1, the mode of heating hydrolysis is in the step 2: temperature was lower than 80 ℃, hydrolysis 2 hours.
4, the making method of pearl small-micelle water according to claim 1 and 2, when raw material was mother pearl shellfish in the wherein said step 1, the mode of heating hydrolysis was in the step 2: temperature is 100 ℃-150 ℃, hydrolysis 1 hour.
5, the making method of pearl small-micelle water according to claim 1 and 2, when wherein choosing infrared waves in the step 5, wavelength region is the 1-25 micron; When selecting ac magnetic field for use, range of frequency is the 50-100 hertz.
6, the making method of pearl small-micelle water according to claim 1 and 2, when wherein raw material described in the step 1 was pure pearl, the nutritive substance that the pearl small-micelle water of made contains comprised calcium, magnesium, manganese, potassium and amino acid; When described raw material was mother pearl shellfish, the nutritive substance that the pearl small-micelle water of made contains comprised calcium, magnesium, manganese and potassium.
7, a kind of application of the pearl small-micelle water that is made by the making method of claim 1 or 2 described pearl small-micelle waters, wherein said pearl small-micelle water are used to drink, medical treatment, beauty treatment or aquaculture.
8, the application of pearl small-micelle water according to claim 7 when wherein said pearl small-micelle water is applied to bottled drinking water, is becoming bottled drinking water through the pearl small-micelle water can after will diluting on ozone sterilization and the disinfectant streamline.
9, a kind of pearl small-micelle water that adopts the described method of claim 1 to make.
CN200610165456A 2006-12-20 2006-12-20 Pearl small-micelle water as well as making method and uses thereof Active CN100591631C (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102335199B (en) * 2011-09-30 2013-03-27 温州大学 Microwave-hydrolyzation method of pearl powder
CN103405154A (en) * 2013-08-15 2013-11-27 李镇南 Water dispenser and water treatment device and method for preparing micro cluster water thereof
CN105640786A (en) * 2014-11-13 2016-06-08 宋裕平 External-use liquid water, nano nutrient solution and preparation method thereof
CN108338992A (en) * 2018-04-08 2018-07-31 西安建筑科技大学 A kind of preparation method of pearl essence Selenium-rich nutrient solution
CN113896352B (en) * 2021-10-21 2023-11-21 张倩婷 Active water for improving drug effect of traditional Chinese medicine and production process thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
水分子团簇结构的改变及其生物效应. 张建平等.化学通报,第4期. 2004
水分子团簇结构的改变及其生物效应. 张建平等.化学通报,第4期. 2004 *

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