CN100554392C - 由固体床吸附分离植物油甘油三酯混合物的方法 - Google Patents

由固体床吸附分离植物油甘油三酯混合物的方法 Download PDF

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Publication number
CN100554392C
CN100554392C CNB028085159A CN02808515A CN100554392C CN 100554392 C CN100554392 C CN 100554392C CN B028085159 A CNB028085159 A CN B028085159A CN 02808515 A CN02808515 A CN 02808515A CN 100554392 C CN100554392 C CN 100554392C
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China
Prior art keywords
triglyceride
acid
weight
adsorbent
desorbent
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Expired - Fee Related
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CNB028085159A
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English (en)
Chinese (zh)
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CN1503836A (zh
Inventor
Z·李森科
S·S·卡蒂
R·斯特林菲尔德
T·格雷戈里
G·J·小夸尔德尔
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Dow Global Technologies LLC
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Dow Global Technologies LLC
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/0058Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents or mixtures of solvents of different natures or compositions used in succession

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
CNB028085159A 2001-04-20 2002-03-21 由固体床吸附分离植物油甘油三酯混合物的方法 Expired - Fee Related CN100554392C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US28546401P 2001-04-20 2001-04-20
US60/285,464 2001-04-20

Publications (2)

Publication Number Publication Date
CN1503836A CN1503836A (zh) 2004-06-09
CN100554392C true CN100554392C (zh) 2009-10-28

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CNB028085159A Expired - Fee Related CN100554392C (zh) 2001-04-20 2002-03-21 由固体床吸附分离植物油甘油三酯混合物的方法

Country Status (13)

Country Link
US (1) US7097770B2 (enExample)
EP (1) EP1383854B1 (enExample)
JP (1) JP2004536167A (enExample)
KR (1) KR20030090749A (enExample)
CN (1) CN100554392C (enExample)
AR (1) AR035862A1 (enExample)
BR (1) BR0208770A (enExample)
CA (1) CA2442063C (enExample)
DE (1) DE60218834T2 (enExample)
MX (1) MXPA03009584A (enExample)
PE (1) PE20021111A1 (enExample)
RU (1) RU2003133734A (enExample)
WO (1) WO2002086039A1 (enExample)

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US6743509B2 (en) 2002-10-01 2004-06-01 Dow Corning Corporation Method of treating precipitated calcium carbonate fillers
US7862546B2 (en) 2003-06-16 2011-01-04 Ethicon Endo-Surgery, Inc. Subcutaneous self attaching injection port with integral moveable retention members
US8715243B2 (en) 2003-06-16 2014-05-06 Ethicon Endo-Surgery, Inc. Injection port applier with downward force actuation
US7850660B2 (en) * 2003-12-19 2010-12-14 Ethicon Endo-Surgery, Inc. Implantable medical device with simultaneous attachment mechanism and method
US7897798B2 (en) 2006-08-04 2011-03-01 Mcneff Research Consultants, Inc. Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same
US8445709B2 (en) * 2006-08-04 2013-05-21 Mcneff Research Consultants, Inc. Systems and methods for refining alkyl ester compositions
CA2678519A1 (en) * 2007-02-13 2008-08-21 Mcneff Research Consultants, Inc. Devices and methods for selective removal of contaminants from a composition
US8017796B2 (en) * 2007-02-13 2011-09-13 Mcneff Research Consultants, Inc. Systems for selective removal of contaminants from a composition and methods of regenerating the same
US7943791B2 (en) * 2007-09-28 2011-05-17 Mcneff Research Consultants, Inc. Methods and compositions for refining lipid feed stocks
US8097049B2 (en) * 2008-02-07 2012-01-17 The Dallas Group Of America, Inc. Biodiesel purification by a continuous regenerable adsorbent process
US20100331559A1 (en) * 2008-02-21 2010-12-30 Dow Global Technologies Inc. Separation of natural oil-derived aldehydes or hydroxy methyl esters using process chromatography
US8232419B2 (en) * 2008-10-02 2012-07-31 The Dallas Group Of America Triacylglycerol purification by a continuous regenerable adsorbent process
US8361174B2 (en) * 2008-10-07 2013-01-29 Sartec Corporation Catalysts, systems, and methods for producing fuels and fuel additives from polyols
US9102877B2 (en) * 2008-11-12 2015-08-11 Sartec Corporation Systems and methods for producing fuels from biomass
EP2489276B1 (en) * 2011-02-17 2013-10-16 Neste Oil Oyj Oil recovery method
KR101409121B1 (ko) * 2011-04-13 2014-06-18 경상대학교산학협력단 폐식물성 오일 기반 바이오매스 탄성체의 제조방법
EP2801604B1 (en) 2013-05-07 2017-04-12 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
CN105505574A (zh) * 2015-12-04 2016-04-20 南京威尔化工有限公司 一种层析分离制备高纯蓖麻油的方法
EP3429743B1 (en) 2016-03-14 2021-01-06 3M Innovative Properties Company Composite granules including polymeric sorbent for aldehydes
US10239812B2 (en) 2017-04-27 2019-03-26 Sartec Corporation Systems and methods for synthesis of phenolics and ketones
EP3638414B1 (en) * 2017-06-16 2024-03-27 3M Innovative Properties Company Polymeric sorbents for aldehydes
CN107955706A (zh) * 2017-12-14 2018-04-24 广州白云山汉方现代药业有限公司 一种脱除中长链结构酯中甘油二酯的方法
US10544381B2 (en) 2018-02-07 2020-01-28 Sartec Corporation Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid
US10696923B2 (en) 2018-02-07 2020-06-30 Sartec Corporation Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4297292A (en) * 1979-05-25 1981-10-27 The Procter & Gamble Company Fractionation of triglyceride mixtures
EP0062114A1 (en) * 1981-04-08 1982-10-13 THE PROCTER & GAMBLE COMPANY Fractionation of triglyceride mixtures
US4770819A (en) * 1987-07-06 1988-09-13 Uop Inc. Process for separating di- and triglycerides
EP0367877A1 (en) * 1987-07-06 1990-05-16 Uop Inc. Adsorption process for separating triglycerides according to degree of unsaturation
US4961881A (en) * 1988-02-17 1990-10-09 Uop Process for separating triglycerides and regenerating absorbent used in said separation process

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US1767041A (en) * 1926-04-14 1930-06-24 Wm S Merrell Co Caster-oil soap and process of making castor-oil soap
US2553288A (en) * 1944-12-07 1951-05-15 Swift & Co Solvent treatment
US2581369A (en) * 1948-05-29 1952-01-08 Petrolite Corp Oxyethylated hydrophile derivatives of certain fractional esters of triricinolein
US2985589A (en) * 1957-05-22 1961-05-23 Universal Oil Prod Co Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets
US3173935A (en) * 1961-04-14 1965-03-16 Chemetron Corp Separation of fatty mixtures
US3165540A (en) 1961-09-05 1965-01-12 Charles F Krewson Process for isolation of divernolin and trivernolin
US3647684A (en) * 1968-04-17 1972-03-07 Dexter Corp Adding cationic material to silicic acid sorbent chromatographic sheet for improved performance
US4210594A (en) 1977-12-08 1980-07-01 The Procter & Gamble Company Process for separating esters of fatty acids
US4213913A (en) 1979-03-12 1980-07-22 Uop Inc. Two-stage process for separating mixed fatty-acid esters
US4402832A (en) 1982-08-12 1983-09-06 Uop Inc. High efficiency continuous separation process
US5068418A (en) 1989-05-08 1991-11-26 Uop Separation of lactic acid from fermentation broth with an anionic polymeric absorbent
JPH0384099A (ja) * 1989-08-28 1991-04-09 Ito Seiyu Kk 水添ヒマシ油改質物の製造法
US5225580A (en) 1990-08-16 1993-07-06 Uop Process for separating fatty acids and triglycerides
US5300242A (en) * 1992-03-05 1994-04-05 The Lubrizol Corporation Metal overbased and gelled natural oils
DE69401506T2 (de) * 1993-04-29 1997-09-11 Norsk Hydro As Verfahren zur chromatografischer fraktionierung von fettsäuren und ihre derivaten
US5414100A (en) * 1993-08-27 1995-05-09 Howard University Deacidification of vegetable oils

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4297292A (en) * 1979-05-25 1981-10-27 The Procter & Gamble Company Fractionation of triglyceride mixtures
EP0062114A1 (en) * 1981-04-08 1982-10-13 THE PROCTER & GAMBLE COMPANY Fractionation of triglyceride mixtures
US4770819A (en) * 1987-07-06 1988-09-13 Uop Inc. Process for separating di- and triglycerides
EP0367877A1 (en) * 1987-07-06 1990-05-16 Uop Inc. Adsorption process for separating triglycerides according to degree of unsaturation
US4961881A (en) * 1988-02-17 1990-10-09 Uop Process for separating triglycerides and regenerating absorbent used in said separation process

Also Published As

Publication number Publication date
EP1383854A1 (en) 2004-01-28
CN1503836A (zh) 2004-06-09
DE60218834D1 (de) 2007-04-26
KR20030090749A (ko) 2003-11-28
WO2002086039A1 (en) 2002-10-31
AR035862A1 (es) 2004-07-21
JP2004536167A (ja) 2004-12-02
PE20021111A1 (es) 2002-12-16
CA2442063C (en) 2011-02-22
CA2442063A1 (en) 2002-10-31
US20040094477A1 (en) 2004-05-20
RU2003133734A (ru) 2005-02-27
EP1383854B1 (en) 2007-03-14
BR0208770A (pt) 2004-06-22
US7097770B2 (en) 2006-08-29
DE60218834T2 (de) 2007-10-31
MXPA03009584A (es) 2004-05-24

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Granted publication date: 20091028

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