CN100502689C - Sweetener added with momordica grosvenori extract and its preparing method - Google Patents
Sweetener added with momordica grosvenori extract and its preparing method Download PDFInfo
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- CN100502689C CN100502689C CNB2005100552281A CN200510055228A CN100502689C CN 100502689 C CN100502689 C CN 100502689C CN B2005100552281 A CNB2005100552281 A CN B2005100552281A CN 200510055228 A CN200510055228 A CN 200510055228A CN 100502689 C CN100502689 C CN 100502689C
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Abstract
The sweetener of the present invention consists of sugar alcohol sweetener 40-99.9 wt%, Grosvenor momordica extract 0.1-60 wt% and Arabia gum 0.1-5 wt%, and the sugar alcohol sweetener is one or several of Palapinose, erythritol, xylitol, lactitol, isomaltitol, sorbitol and maltose oligomer. It is prepared through dissolving, sucking filtering, heating and spraying, and vacuum drying. The sweetener of the present invention is green, nutritive, stable, delicious, unique in taste and safe, has unique health function, and is also suitable for the patients of obesity, diabetes, dental caries, etc.
Description
Technical field
The present invention relates to a kind of sweetener and preparation method thereof, specifically, relate to a kind of sweetener that has added Fructus Monordicae extract and preparation method thereof.
Background technology
Sweet taste is one of favorite taste of people.Use sweetener very general now in the Food ﹠ Drink.The non-sugar sweetener that has been found that now and use mainly contains following several:
(1) synthetic sweetener: mainly be asccharin, belong to non-caloric sweetener, sugariness is 500 times of sucrose, but human carcinogen's possibility is not got rid of as yet fully.
(2) sugar alcohol sweetener: mainly contain xylitol, sorbierite, maltitol etc.Must be an amount of but the glycitols sweetener is taken in, otherwise easily cause diarrhoea, even cause gastrointestinal dysfunction.
(3) natural sweetener: as liquiritin, rebaudioside etc.They extract from natural plants, safety relatively, and sugariness height, heat are low, and have certain functional effect.
(4) amino acid derivativges sweetener: mainly be Aspartame, albumen sugar.Its heat is identical with sucrose.But because sugariness is very high, can ignore by the heat that normal use amount produces, be a kind of natural sweetener of in fact empty calory therefore, and it all is safe to general population and diabetic.
Along with growth in the living standard, people not only pay attention to the taste of food, pay attention to the health care of food more, so the development and application of functional food additives is expanded rapidly.Aspect sweetener, the green confectionery of complying with consumer health's consciousness and modish idea is subjected to green grass or young crops day by day and narrows.Natural, nutrition, functional green additive, because of security is much better than synthetic sweetener, especially special populations such as carious tooth, obesity, diabetic can relieved enjoyments and are had wide development prospect.
Utilizable sweet taste substitute is diversified.It is the strong sweet substance of glucoside S-5 that Momordica grosvenori contains 1% triterpene, its sugariness is equivalent to 300 times of sucrose, much sweeter than Stevioside and glycyrrhizin, and there is not a bitter peculiar smell of Stevioside, this strong sweet substance flavor is sweet and pure, free from extraneous odour, aftertaste sense are strong, thermally-stabilised good, and be stable in 100 ℃ of aqueous solution, 120 ℃ continuously heating still be not destroyed more than 12 hours.Belong to non-fermented material, be beneficial to processing and store.Japan bamboo professor Ben Changsong studies supposition, and this material has the effect of treatment cancer.The main active ingredient of Momordica grosvenori is Momordica-Glycosides, can extract to separate from the Momordica grosvenori fruit to obtain natural sweet taste protein Momordica-Glycosides, and it is the strong sweet substance of triterpene system.It is compared with sweetener on the market, except going even farther aspect the sweet low-heat of height, also has quality better, Heat stability is good, taste novelty, pure taste uniqueness, uses advantage and unique health care such as simple, edible safety.Illness patients such as obesity, diabetes, carious tooth are not needed to limit intake, be used as diabetes patient's supplemental treatment product as the sugar-free sweetener again in a large number.
Now, there is list of references to disclose to utilize the arhat fructose low in calories of Momordica grosvenori preparation, caused people's extensive attention.Application number is that 200410022754.3 Chinese patent application discloses a kind of arhat fructose low in calories and manufacture method thereof, the comprising the steps: choosing fruit, fragmentation---water is carried---filter that------wash-out---concentrates that---drying---is mixed---inclusion recrystallization---drying, got finished product in absorption of its manufacture method.Because arhat fructose low in calories, be that Momordica grosvenori is carried through water, after insoluble impurity such as grade is removed in separation, pass through wash-out again, concentrate, operations such as drying, obtain the higher relatively Fructus Monordicae extract of a kind of Momordica-Glycosides content, and then form with plant multi-sugar alcohol inclusion recrystallization, its finished product is difficult for the moisture absorption, good water solubility, without any side effects, be a kind of lower calories prod that can eat for a long time, but high heat materials such as complete place of sucrose are used for various food, the processing of beverage and home cooking are more suitable for diabetes, obesity, cardio-cerebral vascular disease patient and people's the ideal that is not suitable for high heat materials such as edible sucrose are for confectionery.
But there are two major defects in prior art, one, Momordica grosvenori and other material combination are perfect not to the utmost, its two, the physiologically active ingredient of Momordica grosvenori is not fully played, so its effect is not fully up to expectations.
As a kind of sweetener natural, nontoxic and low in calories,, provide a kind of composite sweetener with Momordica-Glycosides with other sweetener synergies.To reduce the consumption of high-intensity sweeteners, the application of widening natural low intensity sweeteners is given full play to the advantage of Momordica-Glycosides and the health care of uniqueness and also is not seen in report.
Summary of the invention
The technical issues that need to address of the present invention just are to overcome the defective of existing sweetener, a kind of sweetener that has added Fructus Monordicae extract and preparation method thereof is provided, it with the glycitols sweetener as carrier, with Fructus Monordicae extract as coating agent, cover on the carrier equably, it is natural to make this sweetener both have a green sweetener, the characteristics of nutrition have the quality better of Fructus Monordicae extract again, Heat stability is good, the taste novelty, the pure taste uniqueness, use simple, advantage such as edible safety and unique health care and to obesity, diabetes, illness patients such as carious tooth do not need to limit the characteristics of intake.
For addressing the above problem, the present invention adopts following technical scheme:
The present invention has added the sweetener of Fructus Monordicae extract, and it is to have added Fructus Monordicae extract in the glycitols sweetener.
Preferably, sweetener of the present invention contains following parts by weight of component:
Glycitols sweetener 40-99.9 part
Fructus Monordicae extract 0.1-60 part
Gum arabic 0.1-5 part.
Further preferably, sweetener of the present invention contains following parts by weight of component:
Glycitols sweetener 65-99.5 part
Fructus Monordicae extract 0.5-10 part
Gum arabic 0.1-3 part.
More preferably, sweetener of the present invention contains following parts by weight of component:
99 parts of glycitols sweeteners
1 part of Fructus Monordicae extract
1 part of gum arabic.
Glycitols sweetener of the present invention be in palatinose, antierythrite, xylitol, lactitol, hydroxyl isomaltulose, D-sorbite or the oligoisomaltose any one or multiple.
Fructus Monordicae extract of the present invention is for by ultraviolet--and it is 80% or more or by high-efficient liquid phase chromatogram HPLC (High Performance LiquidChromatography) method mensuration Momordica grosvenori mogroside V weight content to be Fructus Monordicae extract more than 20% that visible spectrophotometric UV (ultraviolet-visible spectrophotometry) method is measured the Momordica-Glycosides weight content, and it is prepared by following steps and gets:
1) Momordica grosvenori is placed 6 times to the water of its weight soak, decoct water extract A;
2) Momordica grosvenori is placed 8 times to the water of its weight soak, decoct water extract B;
3) A and B are merged, filter;
4) filtrate is concentrated, and add ethanol in the filtrate after concentrating, again filtrate is refrigerated, suction filtration;
5) ethanol in the recovery filtrate, at last that its process is concentrated, dry, pulverization process obtains the Fructus Monordicae extract fine powder.
Preferably, among the preparation method of Fructus Monordicae extract of the present invention, the soak time of Momordica grosvenori is 1～3 hour; Extraction time is 1～2 hour, and the concentration of alcohol that adds when concentrating is 45～95%, and the ethanol content in the filtrate is 20～80%.
Further preferably, among the preparation method of Fructus Monordicae extract of the present invention, in the step 1), the soak time of Momordica grosvenori is 3 hours; Extraction time is 1.5 hours; Step 2) in, soak time is 2 hours; Extraction time is 1 hour; In the step 4), the concentration of alcohol that adds when concentrating is 70%, and the ethanol content in the filtrate is 50%.
Sweetener of the present invention can be granule, pulvis and other acceptable formulation.
The present invention provides a kind of method for preparing above-mentioned sweetener simultaneously, and it comprises the steps:
A, get the raw materials ready: take by weighing glycitols sweetener 40-99.9 part by weight ratio; Fructus Monordicae extract 0.1-60 part; Gum arabic 0.1-5 part;
B, dissolving suction filtration: the ethanol dissolving Fructus Monordicae extract with 95% gets solution A, and the ethanol consumption is as the criterion with the molten intact Fructus Monordicae extract of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is as the criterion with the molten intact gum arabic of minimum volume; Solution A and solution B are evenly mixed, and suction filtration gets solution C;
C, add thermal spray: pour the glycitols sweetener into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously; After treating that solution C has been sprayed, continue rotation heating 5 minutes;
D, vacuum drying: is 0.08-0.1Mpa with material in vacuum, and temperature is vacuum drying 45 minutes under 50-51 ℃ the condition, stirs once in per 15 minutes.
The present invention rest on a scientific basis theory, through repetition test, chosen safe, the without any side effects and palatinose that can directly take, antierythrite, xylitol, lactitol, hydroxyl isomaltulose, D-sorbite, oligoisomaltose respectively with Momordica-Glycosides content more than 80% or the Momordica grosvenori mogroside V weight content be Fructus Monordicae extract, gum arabic collocation more than 20%, to prepare sweetener of the present invention.When choosing each raw material of the present invention and carry out combination collocation, must consider effect that they can be brought into play separately and the trade-off effect that they are arranged in pairs or groups and can produce.
Palatinose (Palatinose): also be isomaltoketose.Be that maltulose synzyme (ECS.4.99.11) acts on the sucrose generation.Palatinose is a kind of disaccharide molecule of similar sucrose, forms in α-1,6 bond mode by a part glucose and a part fructose, and be the isomeric compound of sucrose (α-1,2), its sweetness ratio sucrose is low, is 0.4 times of sucrose approximately; Can not cause carious tooth, can be digested and assimilated by small intestine, therefore, be not the Bifidobacterium MF, yet the condensation of palatinose intramolecular dehydration forms para gold compound sugar, do not absorbed by people's gastro-intestinal digestion and reach large intestine, promotes the propagation of Bifidobacterium.
Antierythrite: be a kind of naturally occurring tetrose alcohol, sweet taste is pure, and sweet taste characteristic is good, and is very approaching with the sweet taste characteristic of sucrose, no bad back bitter taste.Its good crystallinity, hygroscopicity is low, is easy to pulverize make powder product, and is also non-hygroscopic in the relative humidity 90% above environment, than the more difficult moisture absorption of sucrose.Antierythrite is very stable to heat and acid, brown stain or decomposing phenomenon can occur hardly under the normal food processing conditions, the high temperature infusion in ability hard candy when production and not brown stain.Antierythrite belongs to the filled-type sweetener, can absorb more energy when water-soluble, and heat of solution-43cal/g has a kind of nice and cool mouthfeel characteristic during use, and anti-carious tooth and suitable diabetic and obesity patient use.
Xylitol (Xylitol): be present in multiple fruit, the vegetables with crudeness.Industrial production is a pentose that the corncob hydrolysis is obtained through separating, and the hydrogenation again of purifying is refining, crystallization, the crystal of making.Be white crystalline powder, aqueous solution clear has the sweet taste of similar sucrose, and its sugariness equates with sucrose, and free from extraneous odour has refrigerant sense, can be absorbed by the body, but heat is slightly less than sucrose.The preventing decayed tooth characteristic is better than fructose and sucrose.Because xylitol is not produced the bacterium of carious tooth and is utilized.It does not produce acid in the oral cavity, keep oral cavity neutrality, can prevent the acid etching of tooth.
Lactitol: lactitol is to be made through catalytic hydrogenation by the reduction group alcohol of lactose, and sugariness is 0.4 times of sucrose, can be absorbed by the body after the absorption, and heat is generally 2 kilocalories/gram.
Isomalt: claiming Palatinitol (Palatinitol) again, claim isomalt abroad, is to be that raw material generates isomaltoketose through the effect of α-glycosyltransferase with sucrose, and isomaltoketose obtains through hydrogenation.As a kind of novel functional sweetener, have not deliquescence, non-hygroscopic, sweet taste is pure, and sapid characteristics, its sugariness are 0.6--0.9 times of sucrose, and use amount is also close.Can not all be absorbed after being characterized in taking the photograph the people by body metabolism, the heat that is provided lacks (hydroxyl isomaltulose heat 2kcal/g, sucrose heat 4kcal/g) than sucrose, and can not cause that the tooth dental caries become, can not cause the fluctuation of serum glucose and insulin level after the picked-up, so can supply diabetes patient, energy value is low, can be edible for adiposis patient and fat-reducing personage, can not cause abdominal distension, diarrhoea after eating.
D-sorbite: from the sugar alcohol that aspen tree fruit extracts, sugariness only is half of multitudinous sugar, and heat and sucrose are close.After D-sorbite entered human body: at first be slow diffusion, be oxidized to fructose and be utilized, participate in the fructose metabolic pathway, to blood glucose value and not influence of glucose in urine, the sweetener that can be used as the diabetes patient used, and solves the misery that the diabetes patient can not eat sweet food.
Oligoisomaltose: with the cornstarch is raw material, use the microbial fermentation hydrolysis, 3-8 glucose molecules making through purifying are the sugar of main component, have low sugariness, low heat value, moisture retention, anti-carious tooth, Bifidobacterium in the human body intestinal canal are had the characteristics of splendid cultivation effect; Be a kind of energetic nourishing goods, have easy digestion, low sugariness, Hyposmolality, can promote advantage such as calcium absorption; Because wherein non-fermentable carbohydrate content does not contain dextrose components substantially greater than 90%, therefore be particularly suitable for diabetes patient.
Momordica grosvenori has treatment pertussis, phlegm-fire cough, the dry constipation of blood, and acute and chronic bronchitis and tonsillitis promote multiple efficacies such as functions of intestines and stomach.Modern medicine proves, also contain multiple scavenger (cleanser) material in the Momordica grosvenori, can remove the active oxygen in the human body effectively, so can prevent and treat and cancer that supplemental treatment is caused by free radical, hypertension, physiological pain, climacteric obstacle, cataract, gastritis, ulcer, constipation, eczema, pellagra or the like.In addition, Momordica grosvenori contains treatment coronary heart disease and angiosclerotic oleic acid of prevention and linoleic acid etc.Momordica grosvenori has also contained the composition of scavenger effect, by taking or put on the skin elimination lipofuscin (freckle, foxiness etc.) orally outward.Also can be used for bathing with the lipid peroxide in purifying the blood, improve whole skin metabolism.There is report to say that Momordica grosvenori also can be used for the treatment of acne, obesity and fash alopecia.
The main active ingredient of Momordica grosvenori is Momordica-Glycosides, can extract to separate from the Momordica grosvenori fruit to obtain natural sweet taste protein Momordica-Glycosides, and it is the strong sweet substance of triterpene system.Compare with artificial synthesis edulcorant and other sweetener, the most outstanding advantage of Momordica-Glycosides is an edible safety, sugariness height (pure product sugariness is 300 times of sucrose) is best sweetener of patients such as obesity, hypertension, diabetes, heart disease and best health products.Soluble in water and the alcoholic solution of this product, Heat stability is good, stable in 100 ℃ of aqueous solution, under 120 ℃ of high temperature, still be not destroyed for a long time, and belong to non-fermented material, be beneficial to food storage and processing.Can be widely used in industry such as medicine, food, daily use chemicals, beverage, health care for the aged product.
Advantage and unique health cares such as Momordica-Glycosides has high sweet low-heat, quality better, Heat stability is good, taste novelty, pure taste uniqueness, it is simple to use, edible safety.Illness patients such as obesity, diabetes, carious tooth are not needed to limit intake.Be adapted at using in sugar-free low hot beverage, sugar-free candy and the sugar-free chewing gum.Momordica-Glycosides is the strong sweetener of sugar-free low-heat, and mouthfeel is good, is usually used in the flavor enhancement of food, beverage, should be used as the sweetener in sugar-free low hot beverage, sugar-free candy and the sugar-free chewing gum; Be used as diabetes patient's supplemental treatment product again in a large number as the sugar-free sweetener.Simultaneously Momordica-Glycosides is original and to have thousands of years use historical and accept for the people easily to the health-care treatment of human body, and Momordica-Glycosides also has the health care of advantage such as high sweet low-heat, edible safety and uniqueness.
Adding gum arabic in the present invention, is because the aqueous solution of gum arabic can form firm film after the drying, and Momordica-Glycosides evenly and is closely combined with the glycitols sweetener.
The present invention formulates through scientific experimentation repeatedly, it has, and green sweetener is natural, the characteristics of nutrition, have again Fructus Monordicae extract quality better, Heat stability is good, taste novelty, pure taste uniqueness, use advantage such as simple, edible safety and unique health care and illness patients such as obesity, diabetes, carious tooth do not needed to limit the characteristics of intake.
The present invention has wide practical use on food as non-caloric sweetener and flavor enhancement.Can use for normal food and health food, be specially adapted to patients such as diabetes and hypertension.It can be used in beverage, dessert, baked goods etc. with carbohydrates such as sucrose.In soda, the synergy of it and sucrose and sweetener can significantly reduce the consumption of sucrose or sweetener.
The specific embodiment
The preparation of embodiment 1 Fructus Monordicae extract
1) Momordica grosvenori is placed 6 times to the water of its weight soak 3 hours, decoct to water and seethed with excitement back 1.5 hours again, water extract A;
2) Momordica grosvenori is placed 8 times to the water of its weight soak 2 hours, decoct to water and seethed with excitement back 1 hour, water extract B;
3) A and B are merged, filter;
4) filtrate is concentrated, and to add weight concentration in the filtrate after concentrating be 70% ethanol, make the ethanol content in the filtrate reach 50%, again filtrate is refrigerated, suction filtration;
5) ethanol in the recovery filtrate, at last that its process is concentrated, dry, pulverization process, it is standby to obtain the Fructus Monordicae extract fine powder.The content of its Momordica-Glycosides more than 80% or the Momordica grosvenori mogroside V weight content be more than 20%.
The preparation of embodiment 2 Fructus Monordicae extracts
1) Momordica grosvenori is placed 6 times to the water of its weight soak 1 hour, decoct to water and seethed with excitement back 2 hours again, water extract A;
2) Momordica grosvenori is placed 8 times to the water of its weight soak 3 hours, decoct to water and seethed with excitement back 1 hour, water extract B;
3) A and B are merged, filter;
4) filtrate is concentrated, and to add weight concentration in the filtrate after concentrating be 45% ethanol, make the ethanol content in the filtrate reach 20%, again filtrate is refrigerated, suction filtration;
5) ethanol in the recovery filtrate, at last that its process is concentrated, dry, pulverization process, it is standby to obtain the Fructus Monordicae extract fine powder.The content of its Momordica-Glycosides more than 20% or the Momordica grosvenori mogroside V weight content be more than 20%.
The preparation of embodiment 3 Fructus Monordicae extracts
1) Momordica grosvenori is placed 6 times to the water of its weight soak 1 hour, decoct to water and seethed with excitement back 2 hours again, water extract A;
2) Momordica grosvenori is placed 8 times to the water of its weight soak 3 hours, decoct to water and seethed with excitement back 1 hour, water extract B;
3) A and B are merged, filter;
4) filtrate is concentrated, and to add weight concentration in the filtrate after concentrating be 95% ethanol, make the ethanol content in the filtrate reach 80%, again filtrate is refrigerated, suction filtration;
5) ethanol in the recovery filtrate, at last that its process is concentrated, dry, pulverization process, it is standby to obtain the Fructus Monordicae extract fine powder.The content of its Momordica-Glycosides more than 80% or the Momordica grosvenori mogroside V weight content be more than 20%.
Embodiment 4
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in palatinose that commercial 200kg Japan Shin Mitsui Sugaring Co., Ltd produces, Fructus Monordicae extract that 2kg Guilin Laiyin Biological Product Co., Ltd produces, the Hunan, 2kg Hunan;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C;
4) palatinose is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08Mpa, 50 ℃ of temperature, were stirred once 45 minutes time in per 15 minutes;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 5
1) get the raw materials ready: taking by weighing in the Fructus Monordicae extract, Hunan, 1kg Hunan of antierythrite that commercial 99kg Shandong Baolingbao Biotechnology Co., Ltd. produces, 1kg embodiment 1 preparation the chemical reagent development centre, to produce gum arabic standby;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) antierythrite is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.1Mpa, 51 ℃ of temperature, were stirred once 45 minutes time in per 15 minutes;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 6
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in the Fructus Monordicae extract, Hunan, 0.1kg Hunan of xylitol that commercial 40kg Shandong Futian Pharmacy Co., Ltd., Shandong Yucheng produces, 0.1kg embodiment 2 preparations;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) xylitol is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08-0.1Mpa, 45 minutes time, stirred once in per 15 minutes by temperature 50-51 ℃;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 7
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in the Fructus Monordicae extract, Hunan, 5kg Hunan of lactitol that commercial 99.9kg Purao AS produces, 60kg embodiment 3 preparations;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) lactitol is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08-0.1Mpa, 45 minutes time, stirred once in per 15 minutes by temperature 50-51 ℃;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 8
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in isomaltoketose that commercial 65kg Nanning chemical pharmacy Co., Ltd produces, Fructus Monordicae extract that 0.5kg Guilin Laiyin Biological Product Co., Ltd produces, the Hunan, 0.1kg Hunan;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) isomaltoketose is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08-0.1Mpa, 45 minutes time, stirred once in per 15 minutes by temperature 50-51 ℃;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 9
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in D-sorbite that 99.5kg Shanghai Dasheng Food Co., Ltd produces, Fructus Monordicae extract that 10kg Guilin Laiyin Biological Product Co., Ltd produces, the Hunan, 3kg Hunan;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) D-sorbite is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08-0.1Mpa, 45 minutes time, stirred once in per 15 minutes by temperature 50-51 ℃;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Embodiment 10
1) get the raw materials ready: it is standby to take by weighing the gum arabic that the chemical reagent development centre produces in oligoisomaltose that commercial 99kg Shanghai Dasheng Food Co., Ltd produces, Fructus Monordicae extract that 1kg Guilin Laiyin Biological Product Co., Ltd produces, the Hunan, 1kg Hunan;
2) get solution A with 95% ethanol dissolving Fructus Monordicae extract, the ethanol use amount is with molten intact being as the criterion of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is with molten intact being as the criterion of minimum volume;
3) solution A and solution B are evenly mixed, suction filtration gets solution C, and is stand-by;
4) oligoisomaltose is poured into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously;
5) treat that solution C has been sprayed after, continue rotation heating 5 minutes;
6) material is poured into from coating pan on the pallet, pallet is put into vacuum drying chamber, vacuum 0.08-0.1Mpa, 45 minutes time, stirred once in per 15 minutes by temperature 50-51 ℃;
7) dried material is sieved with No. 2 pharmacopeia sieves, disinfection, packing gets product.
Claims (6)
1, a kind of method for preparing the sweetener that has added Fructus Monordicae extract is characterized in that it comprises the steps:
A, get the raw materials ready: take by weighing glycitols sweetener 40-99.9 part by weight ratio; Fructus Monordicae extract 0.1-60 part; Gum arabic 0.1-5 part;
B, dissolving suction filtration: the ethanol dissolving Fructus Monordicae extract with 95% gets solution A, and the ethanol consumption is as the criterion with the molten intact Fructus Monordicae extract of minimum volume; Get solution B with pure water heating for dissolving gum arabic, the use amount of pure water is as the criterion with the molten intact gum arabic of minimum volume; Solution A and solution B are evenly mixed, and suction filtration gets solution C;
C, add thermal spray: pour the glycitols sweetener into rotary coating pan, the rotation heating, kettle temperature is controlled at 65-70 ℃, uniformly is sprayed onto material on atomizer solution C simultaneously; After treating that solution C has been sprayed, continue rotation heating 5 minutes;
D, vacuum drying: is 0.08-0.1Mpa with material in vacuum, and temperature is vacuum drying 45 minutes under 50-51 ℃ the condition, stirs once in per 15 minutes.
2, a kind of sweetener for preparing by the described method of claim 1.
3, sweetener as claimed in claim 2 is characterized in that: described Fructus Monordicae extract is got by the following steps preparation:
1) Momordica grosvenori is placed 6 times to the water of its weight soak, decoct water extract A;
2) Momordica grosvenori is placed 8 times to the water of its weight soak, decoct water extract B;
3) A and B are merged, filter;
4) filtrate is concentrated, and add ethanol in the filtrate after concentrating, again filtrate is refrigerated, suction filtration;
5) ethanol in the recovery filtrate, at last that its process is concentrated, dry, pulverization process obtains the Fructus Monordicae extract fine powder.
4, sweetener as claimed in claim 3 is characterized in that among the preparation method of described Fructus Monordicae extract that the soak time of Momordica grosvenori is 1～3 hour; Extraction time is 1～2 hour, and the concentration of alcohol that adds when concentrating is 45～95%, and the ethanol content in the filtrate is 20～80%.
5, sweetener as claimed in claim 3 is characterized in that among the preparation method of described Fructus Monordicae extract, and in the step 1), the soak time of Momordica grosvenori is 3 hours; Extraction time is 1.5 hours; Step 2) in, soak time is 2 hours; Extraction time is 1 hour; In the step 4), the concentration of alcohol that adds when concentrating is 70%, and the ethanol content in the filtrate is 50%.
6, as claim 2,3,4 or 5 described sweeteners, it is characterized in that: described sweetener is granule or pulvis.
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| CN102379411A (en) * | 2010-09-02 | 2012-03-21 | 日谷国际有限公司 | Optimized sugar substitute composition |
| EP2446753A1 (en) * | 2010-10-26 | 2012-05-02 | Sunshine Valley International Co., Ltd | Optimized sugar substitute composition |
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| CN101214040B (en) * | 2008-01-04 | 2012-07-25 | 纽威公司 | Momordica grosvenori sweetening agent and preparation thereof |
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2005
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102379411A (en) * | 2010-09-02 | 2012-03-21 | 日谷国际有限公司 | Optimized sugar substitute composition |
| EP2446753A1 (en) * | 2010-10-26 | 2012-05-02 | Sunshine Valley International Co., Ltd | Optimized sugar substitute composition |
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