CN100496750C - Special measuring flask for preparing and storing volatile standard liquid and using method thereof - Google Patents
Special measuring flask for preparing and storing volatile standard liquid and using method thereof Download PDFInfo
- Publication number
- CN100496750C CN100496750C CNB2007100212819A CN200710021281A CN100496750C CN 100496750 C CN100496750 C CN 100496750C CN B2007100212819 A CNB2007100212819 A CN B2007100212819A CN 200710021281 A CN200710021281 A CN 200710021281A CN 100496750 C CN100496750 C CN 100496750C
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- Prior art keywords
- silica gel
- gel sealing
- volumetric flask
- bottleneck
- sealing plug
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- 239000007788 liquid Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000007789 sealing Methods 0.000 claims abstract description 49
- 239000000741 silica gel Substances 0.000 claims abstract description 42
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 42
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 41
- 238000002360 preparation method Methods 0.000 claims abstract description 26
- 150000001875 compounds Chemical class 0.000 claims description 4
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 238000005070 sampling Methods 0.000 claims description 4
- 238000012546 transfer Methods 0.000 claims description 4
- 238000004804 winding Methods 0.000 claims description 3
- 230000002093 peripheral effect Effects 0.000 claims 1
- 238000002474 experimental method Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000003556 assay Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 230000006378 damage Effects 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 239000000383 hazardous chemical Substances 0.000 description 2
- 231100000206 health hazard Toxicity 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 125000001997 phenyl group Chemical class [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
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Abstract
The invention discloses a special measuring flask for preparing and storing volatile standard liquid and a using method thereof. The multifunctional vacuum flask is sealed by combining the threaded bottle cap, the silica gel sealing gasket and the T-shaped silica gel sealing plug, so that the vacuum flask can be fully ensured to have no volatility loss in the preparation, storage and use processes of a standard liquid, and the stability of the content of each component in a volatile standard sample is ensured.
Description
Technical field:
The present invention relates to the glass measurement instrument used a kind of assay laboratory, relate in particular to and a kind ofly be used for the preparation of volatility titer, store the glass measurement instrument of usefulness.
Background technology:
At present the assay laboratory is in preparation with to store benzene series, halogenated hydrocarbons, farming residual etc. a series of when relating to poisonous, harmful volatile solvent and mark thing, usually volumetric flask is adopted in preparation, store and then adopt the good sealing performance vial, but in the practical operation application process, still have following defective:
1. when the above-mentioned volatility titer of preparation, volumetric flask must add the mark thing under the state of open ports, because solvent and mark thing are volatile liquid, solvent and the constantly volatilization of mark thing in the process of operation, this just brings two consequences, and the one, volatile poisonous and harmful solvent and mark thing can damage experiment operator health; The 2nd, when preparation mixes the mark thing, must repeatedly open bottle cap, cause the volatilization loss of mark thing, make the mark substrate concentration of preparation inaccurate.
2. because the sealing property of volumetric flask is not good, mark thing liquid must be transferred in other good sealing performance container and store after preparing, and also has devolatilization in transfer process; Can prevent volatilization though use the good sealing performance container to store, but when each the use, still need open the bottle cap sampling, so in use, exist volatile toxic gas that the health hazards of experiment operator and the volatilization loss of mark thing are caused the inaccurate defective of mark substrate concentration equally.
Through applicant's retrieval and investigation, present domestic a kind of desirable glass measurement instrument that do not have as yet, it can effectively solve the problems referred to above that the laboratory runs into when preparing and store the volatility titer.
Summary of the invention:
In order effectively to address the above problem, the object of the present invention is to provide a kind of special-purpose measuring bottle that is used for the preparation of volatility titer, stocks, another purpose provides the using method of this special-purpose measuring bottle.This volatility titer preparation and the special-purpose measuring bottle of stocking of being used for can guarantee that institute prepares the stability of marking thing content, and the toxic and harmful of avoiding again volatilizing is to the Health cost of experiment operator, and easy to use.
Be used for preparation of volatility titer and the special-purpose measuring bottle of stocking, form by screw cap 1, silica gel sealing pad 2, T type silica gel sealing plug 3, volumetric flask 6, the bottleneck that T type silica gel sealing plug 3 is hermetic filled at volumetric flask 6, bottleneck at volumetric flask 6 is provided with external screw thread 4, containing mark line 5 is accurately arranged on the bottle of volumetric flask 6, be convenient to accurate constant volume, silica gel sealing pad 2 is arranged on the inner chamber end face of screw cap 1, and screw cap 1 is tightened on the whorl of bottleneck place of volumetric flask 6.
Preparation and the method for storing the volatility titer: according to the preparation requirement, choose threaded mouthful normal capacity bottle 6 of respective volume, the bottleneck of hermetic filling at volumetric flask 6 with T type silica gel sealing plug 3, ratio requirement according to predetermined compound concentration, with syringe 7 as transfer tool, the pin of syringe 7 is passed T type silica gel sealing plug 3, inject the preparation liquid of various components, prepare and screw and to store with screw cap 1 immediately after qualified to volumetric flask 6.When needing to use the volatility titer in the volumetric flask 6, the screw cap 1 of outwarding winding, silica gel sealing pad 2 leaves bottleneck with screw cap 1, and the bottleneck that T type silica gel sealing plug 3 is still filled at volumetric flask 6 passes the mark liquid that T type silica gel sealing plug 3 is drawn wherein with the pin of syringe 7.
T type silica gel sealing plug 3 in the present invention, silica gel sealing pad 2, screw cap 1 is the key component of whole device, seal bottleneck by it, get mark during thing adding, make volumetric flask 6 internal standard compound liquid be in sealing state, avoid the effusion of volatile toxic and harmful, sealing when sealed silicon rubber cushion 2 main matching thread bottle caps 1 are used for storing at ordinary times, get mark during thing adding, need micro-sampling pin puncture T type silica gel sealing plug 3 with syringe 7, can there be small puncturing hole the puncture back on T type silica gel sealing plug 3, though these micropores meeting auto-closings, but for thorough leakproof, set up silica gel sealing pad 2 between T type silica gel sealing plug 3 and screw cap 1, storage at ordinary times realizes final sealing by silica gel sealing pad 2 and screw cap 1 combination, does not have the slow effusion of gas in the guaranteed capacity bottle.
Owing to set up external screw thread 4 at the bottleneck of volumetric flask 6, add at bottleneck and to have filled in T type silica gel sealing plug 3, in the inner chamber of screw cap 1, be provided with silica gel sealing pad 2, like this in preparation, store, when taking the mark thing, volatility mark thing in the volumetric flask 6 can't be overflowed, it can reduce to greatest extent and has joined the volatilization loss of marking thing in the volumetric flask 6, guarantee preparation result's accuracy, stop the health hazards of volatile substance simultaneously to experiment operator, with screw cap 1, silica gel sealing pad 2 and 3 combinations of T type silica gel sealing plug seal, fully guaranteed capacity bottle 6 is in the preparation of mark liquid, non-volatility loss in storage and the use, the stability of each constituent content in the assurance volatility standard specimen.This special-purpose measuring bottle has preparation and stores two kinds of functions, having realized using one bottle more, the quantity of reduce preparation, storing utensil, in process for preparation, can guarantee join the mark thing accurately, simplified operation sequence, can not produce any injury again, solved the problems that the assay laboratory runs into when preparation and storage volatility titer operating personnel.
Description of drawings:
Fig. 1 is the structural representation of special-purpose measuring bottle of the present invention;
Fig. 2 is the schematic diagram that adds or extract volatile liquid in special-purpose measuring bottle.
Among the figure: the 1-screw cap; 2-silica gel sealing pad; 3-T type silica gel sealing plug; The 4-external screw thread; The 5-graduation mark; The 6-volumetric flask; The 7-syringe.
The specific embodiment:
Below in conjunction with description of drawings the specific embodiment of the present invention:
As shown in Figure 1 and Figure 2, be used for preparation of volatility titer and the special-purpose measuring bottle of stocking, form by screw cap 1, silica gel sealing pad 2, T type silica gel sealing plug 3, volumetric flask 6, the bottleneck that T type silica gel sealing plug 3 is hermetic filled at volumetric flask 6, external screw thread 4 is arranged on the bottleneck of volumetric flask 6, containing mark line 5 is accurately arranged on the bottle of volumetric flask 6, be convenient to accurate constant volume, silica gel sealing pad 2 is arranged on the inner chamber end face of screw cap 1, and screw cap 1 is tightened on the whorl of bottleneck place of volumetric flask 6 by external screw thread 4.
The using method of above-mentioned special-purpose measuring bottle is as follows: according to the preparation requirement of waiting to join titer, choose the volumetric flask 6 of respective volume, the bottleneck of hermetic filling at volumetric flask 6 with T type silica gel sealing plug 3, ratio requirement according to predetermined compound concentration, each component is prepared in the liquid injection capacity bottle 6 as transfer tool with syringe 7, concrete method for implanting is: the micro-sampling pin of syringe 7 is passed T type silica gel sealing plug 3, draw respectively with syringe 7 in the preparation liquid and injection capacity bottle 6 of various components, prepare and screw with screw cap 1 immediately after qualified, can store; When needing to use the volatility titer in the volumetric flask 6, the screw cap 1 of outwarding winding, silica gel sealing pad 2 leaves bottleneck with screw cap 1, and the bottleneck that T type silica gel sealing plug 3 is still filled at volumetric flask 6 passes the mark liquid that T type silica gel sealing plug 3 is drawn in the volumetric flasks 6 with the pin of syringe 7.
Claims (2)
1, a kind of volatility titer that is used for is prepared, the special-purpose measuring bottle of stocking, it is characterized in that: it is by screw cap (1), silica gel sealing pad (2), T type silica gel sealing plug (3), volumetric flask (6) is formed, bottleneck peripheral hardware screw thread (4) at volumetric flask (6), on the bottle of volumetric flask (6), be provided with containing mark line (5) accurately, be convenient to the volume of accurate constant volume measuring bottle (6), T type silica gel sealing plug (3) is hermetic filled in the bottleneck in volumetric flask (6), silica gel sealing pad (2) is arranged on the inner chamber end face of screw cap (1), and screw cap (1) is rotated with whorl of bottleneck section at volumetric flask (6) by screw thread.
2, the described volatility titer that is used for of claim 1 is prepared, the using method of the special-purpose measuring bottle of stocking is: according to the preparation requirement of volatility titer to be prepared, choose the amount of respective volume and hold bottle (6), hermetic fill in bottleneck with T type silica gel sealing plug (3) in volumetric flask (6), ratio requirement according to predetermined compound concentration, as transfer tool each component being prepared the liquid injection rate with syringe (7) holds in the bottle (6), concrete method for implanting is: the micro-sampling pin of syringe (7) is passed T type silica gel sealing plug (3), draw the preparation liquid and the injection rate of various components respectively holds in the bottle (6) with syringe (7), prepare and use screw cap (1) to screw immediately after qualified, can store; When needing to use the volatility titer in the volumetric flask (6), the screw cap (1) of outwarding winding, silica gel sealing pad (2) leaves bottleneck with screw cap (1), T type silica gel sealing plug (3) is still filled in the bottleneck in volumetric flask (6), the pin of syringe (7) is passed T type silica gel sealing plug (3) draw mark liquid in the volumetric flask (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100212819A CN100496750C (en) | 2007-04-15 | 2007-04-15 | Special measuring flask for preparing and storing volatile standard liquid and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100212819A CN100496750C (en) | 2007-04-15 | 2007-04-15 | Special measuring flask for preparing and storing volatile standard liquid and using method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101091927A CN101091927A (en) | 2007-12-26 |
| CN100496750C true CN100496750C (en) | 2009-06-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007100212819A Expired - Fee Related CN100496750C (en) | 2007-04-15 | 2007-04-15 | Special measuring flask for preparing and storing volatile standard liquid and using method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN100496750C (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102247901B (en) * | 2011-04-14 | 2013-08-07 | 山东电力研究院 | Measuring flask used for preparation of volatile standard solution and application method thereof |
| CN102658220A (en) * | 2012-05-14 | 2012-09-12 | 陆胜龙 | Reagent bottle provided with blue cap and capable of quickly fixing volume |
| CN103776507A (en) * | 2013-11-30 | 2014-05-07 | 成都新基因格生物科技有限公司 | Falling-prevention measuring cylinder |
| CN106769369B (en) * | 2016-12-07 | 2019-06-04 | 中国计量科学研究院 | Prepare container, the device and method of the organic mixed solution standard substance of volatility |
| CN113484488B (en) * | 2021-07-06 | 2023-11-24 | 陕西中天盛隆智能科技有限公司 | Intelligent reference liquid pool for detecting concentration of ions in liquid |
| CN114279772A (en) * | 2021-12-03 | 2022-04-05 | 奇瑞新能源汽车股份有限公司 | Odor bottle for detecting automobile odor and odor detection method |
| CN114878281A (en) * | 2022-06-13 | 2022-08-09 | 山东大学 | Integrated device for generating and collecting dimethyl mercury and application method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2138379A1 (en) * | 1971-05-25 | 1973-01-05 | Berthelin Andre | |
| US20060185421A1 (en) * | 2005-02-23 | 2006-08-24 | Walker Stephan H | Volumetric densiometer flask |
| CN2852069Y (en) * | 2005-11-17 | 2006-12-27 | 周慧 | Measuring flask |
| CN2880246Y (en) * | 2006-03-03 | 2007-03-21 | 上海药明康德新药开发有限公司 | Quantitative dropping bottle |
| CN201023051Y (en) * | 2007-04-15 | 2008-02-20 | 夏卫文 | Special measuring flask for preparing and storing volatile standard liquid |
-
2007
- 2007-04-15 CN CNB2007100212819A patent/CN100496750C/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2138379A1 (en) * | 1971-05-25 | 1973-01-05 | Berthelin Andre | |
| US20060185421A1 (en) * | 2005-02-23 | 2006-08-24 | Walker Stephan H | Volumetric densiometer flask |
| CN2852069Y (en) * | 2005-11-17 | 2006-12-27 | 周慧 | Measuring flask |
| CN2880246Y (en) * | 2006-03-03 | 2007-03-21 | 上海药明康德新药开发有限公司 | Quantitative dropping bottle |
| CN201023051Y (en) * | 2007-04-15 | 2008-02-20 | 夏卫文 | Special measuring flask for preparing and storing volatile standard liquid |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101091927A (en) | 2007-12-26 |
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Granted publication date: 20090610 Termination date: 20100415 |