CN100491095C - Novel production process of gypsum shaving board - Google Patents
Novel production process of gypsum shaving board Download PDFInfo
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- CN100491095C CN100491095C CNB2006100383165A CN200610038316A CN100491095C CN 100491095 C CN100491095 C CN 100491095C CN B2006100383165 A CNB2006100383165 A CN B2006100383165A CN 200610038316 A CN200610038316 A CN 200610038316A CN 100491095 C CN100491095 C CN 100491095C
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Abstract
The invention relates the gypsum chipboard manufacturing new technique. The first new technology comprises stirring material, forming, single pressing and solidifying plate blank at 30-60Deg.C and drying. The second new technology comprises stirring material, squeezing and forming and solidifying at 30-60Deg.C, sawing and drying. Providing the proper temperature at the course of pressurization, the pressing and solidifying time is shortened, and physical mechanics property is improved. The technology has the advantages of simple technique and device, high production efficiency and homogeneous thickness of gypsum chipboard, solving the problem that the current technology can not produce the hollow gypsum chipboard.
Description
Affiliated technical field
The present invention relates to a kind of novel production process of gypsum shaving board, belong to the man-made board technology field.
Background technology
Gypsum particle board belongs to the inorganic adhesive wood-based plate.At the beginning of the eighties in last century, a kind of gypsum particle board semidry method production technology (forestry science and technology communication 1995.5.p36) has been invented by Germany not professor Kossatz of labor Hough research institute (Fraunhofer Gesellschaft).The material component of producing gypsum particle board comprises gypsum, wood shavings, water and set retarder (citric acid).The effect of set retarder is to prevent that gypsum from producing curing before pressurization.Its main technique step comprises: the stirring of material, the moulding of mating formation, accumulation formula cure under pressure, branch plate, drying.Exert pressure is decided according to density, the thickness requirement of gypsum particle board, is generally about 3.0MPa.Gypsum is longer hardening time, and cure under pressure generally needs more than 2 hour (stressed size of institute and cure under pressure time are irrelevant substantially) at normal temperatures, just can make gypsum particle board have certain intensity.Being added in of set retarder delays gypsum also can make the performance number of gypsum particle board descend to some extent in the time of the presetting period.And can cause gypsum dehydration as other wood-based plate cure under pressure under high temperature (more than 100 ℃), the intensity of plate is very poor.Therefore, this method is produced gypsum particle board and is adopted accumulation formula cure under pressure under the normal temperature, be called " cold-press method " in the industry, the alternate accumulation with backing plate of tens of slabs of moulding of being about to mat formation reaches certain height, in driving grade single drylight presses greatly, force down the height of regulation, and release press with the fixing back of special fixture, cure under pressure is sent into after 2 hours again and is opened a grade single drylight presses pressurization greatly and unload anchor clamps at normal temperatures.The major defect of accumulation formula cure under pressure technology is: 1, the cure under pressure time oversize, need more than 2 hour usually, production efficiency is low; 2, pile up the levels unbalance stress that the formula cure under pressure makes straight sheet pile, cause the thickness deviation of levels gypsum particle board big, use for gypsum particle board as materials for wall and brought certain difficulty; 3, complex technical process needs with many cover special fixtures, and is bulky, takies too much production site; 4, can't produce the hollow gypsum particieboard.
Summary of the invention
The technical problem to be solved in the present invention is: overcome the shortcoming of existing gypsum particle board production technology, two kinds of novel production process of gypsum shaving board are provided.
It is as follows that the present invention solves the problems of the technologies described above the technical scheme that is adopted: first kind of novel production process of gypsum shaving board, its material component comprises gypsum, wood shavings, water and set retarder, its processing step comprises: the stirring of material, the moulding of mating formation, individual slab cure under pressure, drying, described cure under pressure temperature range are 30 ℃-60 ℃.
It is as follows that the present invention solves the problems of the technologies described above the technical scheme that is adopted: second kind of novel production process of gypsum shaving board, its material component comprises gypsum, wood shavings, water and set retarder, its processing step comprises: the stirring of material, extrusion modling curing, sawing, drying, described extrusion modling solidification temperature scope are 30 ℃-60 ℃.
The present invention proposes on the basis to the further investigation of the slow setting mechanism of gypsum particle board and experiment.Through experiment with discover: gypsum can discharge certain heat when solidifying, and its exothermic temperature decreases with the increase of set retarder addition, because of the adding of wood shavings decreases, when the gypsum particle board pressurized and decrease; Simultaneously, also phase delay of its time that arrives the exothermic temperature peak value.Referring to Fig. 1, Fig. 2 and table 1.This explanation set retarder is in the ability drop that delays to make when gypsum solidifies its heat release, wood shavings can absorb the heat that is discharged when gypsum solidifies, in gypsum particle board pressurized solidification process, the heat release ability drop of gypsum, and the heat release ability drop also means the prolongation of solidification process.Therefore, the present invention considers to give suitable temperature-compensating to the gypsum particle board cure under pressure time, promotes the curing of gypsum, shortens its cure under pressure time, the theoretical foundation of the heat pressing process that gypsum particle board employing that Here it is is new.
Facts have proved, when gypsum particle board pressurizes, give suitable temperature (30 ℃-60 ℃) condition, both can shorten its cure under pressure time, can make it have higher physical and mechanical property again.
First kind of novel production process of gypsum shaving board of the present invention has the following advantages and effect: can adopt individual hot pressing of multidaylight press, work simplification, production equipment is simple, does not need special fixture, production site reduces, the production efficiency height, the cure under pressure time shortens dramatically, and shortens to 20-30 minute by more than 2 hours, individual slab cure under pressure is stressed evenly, the thickness deviation of gained gypsum particle board is little, and performance meets or exceeds the index of correlation of prior art, referring to Fig. 3 and table 2.
Second kind of novel production process of gypsum shaving board of the present invention has the following advantages and effect: continuously extruded, technology is simplified more, production equipment is simpler, the production efficiency height, extrusion modling shortens dramatically hardening time, shortened to 20-30 minute by more than 2 hours, use different hollow mould can produce the gypsum particle board of multiple hollow-core construction, solve existing production technology and can not produce the difficult problem of various hollow gypsum particieboards, the thickness of gained gypsum particle board is even, and performance indications are referring to table 3.
Description of drawings
Fig. 1 is not for after adding set retarder at ambient temperature and adding 0.025%, 0.05%, 0.1 citric acid set retarder respectively, exothermic temperature when gypsum solidifies and the schematic diagram of time.Exothermic temperature when as can be seen from the figure gypsum solidifies decreases with the increase of set retarder addition, the highest exothermic temperature of gypsum that does not add set retarder can reach 50 ℃ and 60 minutes short heat release time, increase exothermic temperature reduction along with the citric acid addition, the heat release time is extended, and exothermic temperature has dropped to about 43-40 ℃.
Fig. 2 is not for after adding set retarder at ambient temperature and having added 0.025%, 0.05%, 0.1 citric acid set retarder, exothermic temperature the when gypsum that contains wooden shavings solidifies and the schematic diagram of time.As can be seen from the figure, wood shavings can absorb the thermal discharge of gypsum, and the exothermic temperature of gypsum is reduced.In gypsum, add wooden shavings, not adding the gypsum of set retarder and the exothermic temperature of wood shavings is 43.7 ℃, the exothermic temperature that adds set retarder drops to 39-36.55 ℃, can draw from test data, the exothermic temperature when Fig. 2 and Fig. 1 have identical trend promptly to solidify along with the increase gypsum of the addition of citric acid is lowered.
Fig. 3 is the schematic diagram that concerns of pressing time and temperature and gypsum particle board MOR.As can be seen from the figure: gypsum particle board cure under pressure half an hour under 30 ℃ of-40 ℃ of temperature conditions, its MOR value meets and exceeds the MOR value of 2 hours plates of cure under pressure under the normal temperature.
The specific embodiment
Describe the present invention with relevant figure, table below in conjunction with embodiment.But the invention is not restricted to given example.
First kind of novel production process of gypsum shaving board concrete steps of the present invention are as follows:
(1), presses wooden cream than 0.4, water paste ratio 0.35, plate nominal density 1.2g/cm
3, set retarder citric acid (chemical pure) addition is 0.05% (is benchmark with the gypsum consumption) raw materials weighing land plaster, masson pine wood shavings, citric acid and water;
The water and the wood shavings that will be added with citric acid (2), earlier stir, and mixed gypsum stirs again, then the mixture that stirs are mated formation into by hand the slab of 30 X, 30 X 10mm;
(3), individual slab is put into press, put a backing plate in its lower section, press is 3.0MPa to the gypsum particle board applied pressure, 30 ℃-60 ℃ of hot pressing temperature scopes, the time of cure under pressure is more than or equal to 20 minutes, carries out the group experiment of 2h (hour, down with)-0.5h; Can with slab individual put into multidaylight press each the layer simultaneously the pressurization, enhance productivity; Also the same one deck that two slabs that separated by backing plate can be put into press pressurizes, and further enhances productivity;
(4), the gypsum particle board that cure under pressure is good puts into baking oven and dries by the fire 24h, regulating oven temperature is 45 ℃;
(5), will dry by the fire good gypsum particle board and take out, be placed on one week of health under the room temperature condition, measure every performance of gypsum particle board.
The present invention provides 5 embodiment of first kind of novel production process of gypsum shaving board, referring to table 4.
Second kind of novel production process of gypsum shaving board concrete steps of the present invention are as follows:
(1), presses wooden cream than 0.4, water paste ratio 0.35, plate nominal density 1.2g/cm
3, set retarder citric acid (chemical pure) addition is 0.05% (is benchmark with the gypsum consumption) raw materials weighing land plaster, masson pine wood shavings, citric acid and water;
(2), the water and the wood shavings that will be added with citric acid earlier stir, mixed gypsum stirs again, then the mixture that stirs is cured as banded gypsum particle board with the extruder extrusion modling, the band-like plate width is less than 1.5m, thickness range is 15-30mm, and sawing becomes the plate of certain specification, and extrusion modling solidification temperature scope is 30 ℃-60 ℃, time was carried out the group experiment of 1h-0.5h more than or equal to 20 minutes among the embodiment; Utilize hollow moulded board can squeeze out hollow gypsum particle board, change the shape of hollow moulded board, can squeeze out the gypsum particle board of various hollow shape;
(3), the gypsum particle board that sawing is good puts into baking oven and dries by the fire 24h, regulating oven temperature is 45 ℃;
(4), will dry by the fire good gypsum particle board and take out, be placed on one week of health under the room temperature condition, measure the performance of gypsum particle board.
The present invention provides 7 embodiment of second kind of novel production process of gypsum shaving board, and is as shown in table 5.
The gypsum particle board that two kinds of new technologies of the present invention are produced has the better physical mechanical property, and with reference to the countries concerned and industry standard, test result sees Table 6 and table 3 respectively.
Explanation about table 1: table 1 is the exothermic temperature of gypsum particle board gypsum when pressurization.Table 1 shows that the heat release maximum temperature that does not add the gypsum of set retarder in the pressure process is 24.8 ℃ only, adds about 27 ℃ of the heat release maximum temperature of set retarder.Explanation thermal discharge of gypsum in pressure process is dispersed in the air, and the evidence gypsum adds the solidification intensity that an amount of heat helps to improve gypsum in curing, so the gypsum particle board behind the hot-press solidifying has intensity preferably.
Explanation about table 2: table 2 is the performance of gypsum particle board under different temperatures and pressurized conditions, under 30 ℃ of-50 ℃ of temperature conditions, pressurizes half an hour, and gypsum particle board can reach 2 hours performance of normal temperature pressurization.
Explanation about table 3: the physical and mechanical property of the gypsum particle board that table 3 is made at different temperatures and extrusion time for 7 embodiment of second kind of technology of the present invention, as can be seen from Table 3, the performance parameter value of gypsum particle board was the highest when the temperature when extrusion modling is solidified was 30 ℃-40 ℃, and extrusion time is that the performance parameter of the performance parameter of halfhour gypsum particle board and 1 hour is similar.
Explanation about table 6: the physical and mechanical property of the gypsum particle board that table 6 is made for 5 embodiment of first kind of technology of the present invention, as can be seen from Table 6, the performance parameter value of gypsum particle board was the highest when the temperature during cure under pressure was 30 ℃-40 ℃, and be that the performance parameter of halfhour gypsum particle board can reach 2 hours performance parameter of pressurization under the normal temperature pressing time.
The exothermic temperature of table 1 gypsum particle board gypsum when pressurization
The performance of table 2 gypsum particle board under different temperatures and pressurized conditions
The physical and mechanical property of the gypsum particle board that 7 embodiment of second kind of technology of table 3 the present invention make at different temperatures and extrusion time
| Temperature-time | Internal bond strength MPa | MOR MPa | Elastic modelling quantity MPa | Thickness swelling rate % |
| 30 |
0.28 | 4.79 | 1910 | 2.87 |
| 30℃(0.5h) | 0.27 | 4.65 | 1771 | 2.43 |
| 40 |
0.30 | 5.53 | 2102 | 2.44 |
| 40℃(0.5h) | 0.30 | 5.75 | 1917 | 2.19 |
| 50 |
0.29 | 4.88 | 2045 | 2.18 |
| 50℃(0.5h) | 0.28 | 4.24 | 1842 | 2.03 |
| 60℃(0.5h) | 0.26 | 4.01 | 1752 | 2.83 |
5 embodiment of first kind of technology of table 4 the present invention
7 embodiment of second kind of technology of table 5 the present invention
| Index | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 |
| Wood cream ratio | 0.4 | 0.4 | 0.4 | 0.3 | 0.3 | 0.4 | 0.4 |
| Water paste ratio | 0.35 | 0.40 | 0.40 | 0.35 | 0.35 | 0.35 | 0.35 |
| Set retarder (%) | 0.05 | 0.75 | 0.75 | 0.05 | 0,05 | 0.05 | 0.05 |
| Pressed temperature (℃) | 30 | 30 | 40 | 40 | 50 | 50 | 60 |
| Pressing time (h) | 1 | 0.5 | 1 | 0.5 | 1 | 0.5 | 0.5 |
The physical and mechanical property of the gypsum particle board that first kind of technology of table 6 the present invention is made
Claims (5)
1, novel production process of gypsum shaving board, its material component comprises gypsum, wood shavings, water and set retarder, its processing step comprises: the stirring of material, the moulding of mating formation, individual slab cure under pressure, drying, described cure under pressure temperature range are 30 ℃-60 ℃.
2, novel production process of gypsum shaving board according to claim 1, it is characterized in that in the cure under pressure step with slab individual put into each layer pressurization simultaneously of multidaylight press.
3, novel production process of gypsum shaving board according to claim 1 and 2 is characterized in that in the cure under pressure step and will be pressurizeed by same one deck that two slabs that backing plate separates are put into press.
4, novel production process of gypsum shaving board, its material component comprises gypsum, wood shavings, water and set retarder, its processing step comprises: the stirring of material, extrusion modling curing, sawing, drying, described extrusion modling solidification temperature scope are 30 ℃-60 ℃.
5, novel production process of gypsum shaving board according to claim 4 is characterized in that utilizing in the extrusion modling curing schedule hollow moulded board to squeeze out the gypsum particle board strip of hollow-core construction.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100383165A CN100491095C (en) | 2006-02-16 | 2006-02-16 | Novel production process of gypsum shaving board |
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| CNB2006100383165A CN100491095C (en) | 2006-02-16 | 2006-02-16 | Novel production process of gypsum shaving board |
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| CN1807047A CN1807047A (en) | 2006-07-26 |
| CN100491095C true CN100491095C (en) | 2009-05-27 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108724382A (en) * | 2018-08-29 | 2018-11-02 | 南京工业大学 | A kind of wooden foundation stone cream composite material and preparation method of structure |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112092186B (en) * | 2020-09-17 | 2021-11-16 | 东阳市玖鑫新材料有限公司 | Composite wall board manufacturing process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108724382A (en) * | 2018-08-29 | 2018-11-02 | 南京工业大学 | A kind of wooden foundation stone cream composite material and preparation method of structure |
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Granted publication date: 20090527 Termination date: 20110216 |