CN100450493C - Black fungus composite soft capsule and its preparing process - Google Patents
Black fungus composite soft capsule and its preparing process Download PDFInfo
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- CN100450493C CN100450493C CNB200510009721XA CN200510009721A CN100450493C CN 100450493 C CN100450493 C CN 100450493C CN B200510009721X A CNB200510009721X A CN B200510009721XA CN 200510009721 A CN200510009721 A CN 200510009721A CN 100450493 C CN100450493 C CN 100450493C
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Abstract
The present invention relates to a composite soft capsule of blackfungus and a preparation process thereof. The composite soft capsule of blackfungus comprises the components: blackfungus polysaccharide powder, evening primrose oil, chitin, vitamin, zinc gluconate and VA salad oil. The present invention has the advantages of novel formula combination, scientific reference and original creation and has the function of increasing functional components for the health of a human body. The novel formula combination is mainly prepared by that blackfungus polysaccharide is extracted from blackfungus by a scientific method and is mixed with chitin, evening primrose oil, vitamin E, trace element zinc, etc. which have peculiar functions, so that the addition of the functional ingredients of the product is enhanced, the suction rate of a human body for effective factors is enhanced, and the health care function is greatly improved. Thereby, the formula combination is a pioneer in health care foods.
Description
Affiliated field: the present invention relates to a kind of black fungus composite soft capsule and preparation technology thereof.
Background technology:
Present Auricularia product is more, the overall absorption weak effect, and existing processing technique is coarse, can not effectively discharge the nutritional capacity of Auricularia product.
Summary of the invention:
The purpose of this invention is to provide a kind of absorption that helps the person, have the black fungus composite soft capsule and the preparation technology thereof of health care and better nutritive validity.The objective of the invention is to be achieved through the following technical solutions: the present invention is a kind of black fungus composite soft capsule and preparation technology thereof, black fungus composite soft capsule, and its constituent is:
Auricularia polycose powder 250----350g
Radix Oenotherae erythrosepalae oil 50----70g
Chitin 3.5----5.5g
Vitamin E 3.5----7g
Zinc gluconate 0.3----1.2g
V
ASalad oil 530----630g
Preparation technology of the present invention is: the Auricularia that (1) will clean after drying advances mechanical activation comminution, granularity is controlled at about 20 orders, promptly earlier 20 purpose Auricularia raw materials are put into container, the ethanol 90----95 degree V/V that adds 5 times of raw materials, stir, capping was soaked 1 hour, with the ethanol recover ethanol was reclaimed then; (2) the Auricularia powder after will handling is put into basin, carries out enzymolysis processing, adds the water of 40 times of raw material weights earlier, adjusts pH value scope 4.5----5.0, heat to 50----55 degree centigrade, add pectase 1%, proteinase-10 .8%, start agitator and be mixed, enzymolysis kept 4 hours, the middle stirring 1 time; (3) water is carried: raw material slag and enzymolysis solution directly are warmed up to 85----90 degree centigrade, kept 2.5----3.5 hour, coarse filtration: after raw material slag and extracting solution be cooled to room temperature, carry out screen cloth coarse filtration and filter cloth earlier and filter, the filtering residue list is put and is prepared enzymolysis and water extraction for the second time, for the first time filtrate to put into basin stand-by, same operation is carried out three times, both do the second time, extracted for the third time, again three lixiviating solution had been lumped together, carried out next procedure; (4) fine straining: with kieselguhr cardboard filter machine, above-mentioned three kinds of mixed extracts are carried out fine straining, getting filtrate, to put into basin stand-by, and (5) concentrate: use vacuum concentration pot, above-mentioned filtrate is concentrated, contain polysaccharide about 2.0 in the liquid after concentrated; (6) alcohol precipitation: with the metering of polysaccharide concentrated solution, add the 95%V/V ethanol of 2 times of volumes of concentrated solution, in precipitate with ethanol under 4----10 degree centigrade the temperature about 10 hours; (7) filter: the solution behind the precipitate with ethanol is carried out isolated by filtration, obtain polysaccharide precipitation, liquid reclaims by ethanol, and deposit mixes and carries out drying, promptly obtains polysaccharide; (8) drying: the polysaccharide precipitation material is carried out vacuum drying, and temperature is controlled at about 60 degree, prevents the polysaccharide degeneration; (9) pulverize: the polysaccharide dry matter is put into high speed disintegrator pulverize, reach the 120----200 order and be advisable, package spare; (10) mixing of powder: Auricularia polysaccharide powder, chitin, zinc gluconate are established material by formula proportion mix, require to stir, be through sterilization treatment; (11) mixing of oil preparation: with Radix Oenotherae erythrosepalae oil, vitamin E, V
ASalad oil mixes; (12) slurrying is handled: powder intermixture and oil preparation intermixture are mixed, handle through the mechanical agitation making beating, handle through colloidal grinding, obtain the oil preparation mixed serum, be incubated under 50 degrees centigrade of situations, prepare next procedure and make soft capsule; (13) glue: have blender and heating, cooling, insulation, system vacuum function in the glue jar, after the tank body sterilization, put into the steaming slide earlier and be heated to 80 degrees centigrade, add gelatin again, solid-to-liquid ratio is 1: 2, add an amount of glycerol again and stir, evacuation 4 hours is cooled to 50 degrees centigrade, be incubated 2 hours, be put in the jar that links to each other with pellet processing machine, follow procedure starts pellet processing machine, makes soft capsule.
Formula combination of the present invention is novel unique, and the scientific basis original creation effectively improves the effect of functional component to health.The innovation of formula combination: mainly be from Auricularia, to extract Auricularia polycose with scientific method, be equipped with chitin with unique function, Radix Oenotherae erythrosepalae oil, vitamin E, trace element zinc etc. again, improved the addition of product efficacy composition, improved the absorption rate of human body to efficiency factor, improved health-care effect greatly, so this formula combination is an initiative in the health food, newly show the domestic beyond example of this combination formula through looking into.Extracting method adopts physical pulverization, and the ethanol extraction new technology is decomposed in the plurality of enzymes combination.The physical pulverization granularity is generally about 120 orders, in order to reduce granularity, and make polysaccharide yield higher, adopt multi-enzyme method technology, main with pectase, protease, Ye Huamei etc., make grain refine, the crushed after being dried degree reaches 200 orders, to raw material yield 9.6-10.4%, adopt multiple powder to mix with oil preparation, homogenizing is handled and is made soft capsule, and this technology is the innovation that single oil preparation is made soft capsule, has the value of originality and extensive use.Make the product efficacy enhancing with five kinds of combination of active principles, strengthen absorbing of the person, strengthen health food, health care and nutrition balance, this technology is the compatibility innovation.The combination material is Auricularia polycose, chitin, grass oil, vitamin E, zinc gluconate.Do not appear in the newspapers at home through looking into newly, fill the domestic gaps real the genus.
The specific embodiment:
The present invention is a kind of black fungus composite soft capsule and preparation technology thereof, black fungus composite soft capsule, and its constituent is:
Auricularia polycose powder 250----350g
Radix Oenotherae erythrosepalae oil 50----70g
Chitin 3.5----5.5g
Vitamin E 3.5----7g
Zinc gluconate 0.3----1.2g
V
ASalad oil 530----630g
Concrete constituent in the present embodiment is: Auricularia polycose powder 300g, Radix Oenotherae erythrosepalae oil 60g chitin 4g, vitamin E 5g, zinc gluconate 0.9g, V
ASalad oil 590g.
Preparation technology of the present invention is: the Auricularia that (1) will clean after drying advances mechanical activation comminution, granularity is controlled at about 20 orders, promptly earlier 20 purpose Auricularia raw materials are put into container, the ethanol 90----95 degree V/V that adds 5 times of raw materials, stir, capping was soaked 1 hour, with the ethanol recover ethanol was reclaimed then; (2) the Auricularia powder after will handling is put into basin, carries out enzymolysis processing, adds the water of 40 times of raw material weights earlier, adjusts pH value scope 4.5----5.0, heat to 50----55 degree centigrade, add pectase 1%, proteinase-10 .8%, start agitator and be mixed, enzymolysis kept 4 hours, the middle stirring 1 time; (3) water is carried: raw material slag and enzymolysis solution directly are warmed up to 85----90 degree centigrade, kept 2.5----3.5 hour, coarse filtration: after raw material slag and extracting solution be cooled to room temperature, carry out screen cloth coarse filtration and filter cloth earlier and filter, the filtering residue list is put and is prepared enzymolysis and water extraction for the second time, for the first time filtrate to put into basin stand-by, same operation is carried out three times, both do the second time, extracted for the third time, again three lixiviating solution had been lumped together, carried out next procedure; (4) fine straining: with kieselguhr cardboard filter machine, above-mentioned three kinds of mixed extracts are carried out fine straining, getting filtrate, to put into basin stand-by, and (5) concentrate: use vacuum concentration pot, above-mentioned filtrate is concentrated, contain polysaccharide about 2.0 in the liquid after concentrated; (6) alcohol precipitation: with the metering of polysaccharide concentrated solution, add the 95%V/V ethanol of 2 times of volumes of concentrated solution, in precipitate with ethanol under 4----10 degree centigrade the temperature about 10 hours; (7) filter: the solution behind the precipitate with ethanol is carried out isolated by filtration, obtain polysaccharide precipitation, liquid reclaims by ethanol, and deposit mixes and carries out drying, promptly obtains polysaccharide; (8) drying: the polysaccharide precipitation material is carried out vacuum drying, and temperature is controlled at about 60 degree, prevents the polysaccharide degeneration; (9) pulverize: the polysaccharide dry matter is put into high speed disintegrator pulverize, reach the 120----200 order and be advisable, package spare; (10) mixing of powder: Auricularia polysaccharide powder, chitin, zinc gluconate are established material by formula proportion mix, require to stir, be through sterilization treatment; (11) mixing of oil preparation: with Radix Oenotherae erythrosepalae oil, vitamin E, V
ASalad oil mixes; (12) slurrying is handled: powder intermixture and oil preparation intermixture are mixed, handle through the mechanical agitation making beating, handle through colloidal grinding, obtain the oil preparation mixed serum, be incubated under 50 degrees centigrade of situations, prepare next procedure and make soft capsule; (13) glue: have blender and heating, cooling, insulation, system vacuum function in the glue jar, after the tank body sterilization, put into the steaming slide earlier and be heated to 80 degrees centigrade, add gelatin again, solid-to-liquid ratio is 1: 2, add an amount of glycerol again and stir, evacuation 4 hours is cooled to 50 degrees centigrade, be incubated 2 hours, be put in the jar that links to each other with pellet processing machine, follow procedure starts pellet processing machine, makes soft capsule.
Prescription of the present invention is main according to being " centre halfback No. 2002.51 " file of issuing of the Pharmacopoeia of the People's Republic of China, health ministry in the pertinent regulations, " Chinese health food progress " etc. that are the nutraceutical of polyphagia with emaciation medicine and health food, ad hoc meter formula for a product.
One, Auricularia polycose
Auricularia polycose is to be raw material with the Auricularia that northeast abounds with, the Auricularia polycose material that extracts by scientific method.
1, the biological character of black ear
Auricularia is called for short Auricularia, Basidiomycetes, and Auriculariaceae, the sporophore of Auricularia has another name called black dish, Mulberry, and another names such as timber fungus, tree chicken, wooden moth, wooden young pilose antler are arranged again, belongs to wild edible fungus.Be born on the rotten wood such as fried, Mulberry, ashamed, willow, elm, ancient times is called five Auricularias.Auricularia is a kind of saprophytic fungus of warm nature, relies on the dried growth and breeding of straw of broad leaf tree.Heilungkiang is the township that abounds with natural Auricularia, the mountain area around the Daxing'an Mountainrange, the Xiaoxinanlin Mountains particularly, abound with the natural and pollution-free green Auricularia, big nutritious, the delicious flavour of thick of fine quality, ear, contain protein, Auricularia polysaccharide, multivitamin and trace element, be subjected to the welcome and the favor in broad masses and restaurant especially deeply.
2, the active ingredient of Auricularia
Auricularia meat exquisiteness, tender deliciousness, main is that Auricularia contains rich in protein, protein content 10.6g/100g in dry product, carbohydrate 65g/100g, wherein more than the Auricularia polysaccharide 2000mg/100g, fatty 0.2g/100g, calcium 357m g/100g, phosphorus 201m g/100g, ferrum 185mg/100g (higher 13 times than egg) also have quite high Hu square-bottomed bamboo basket Bu Su, thiamine, riboflavin, nicotinic acid, phospholipid, sterol, VB
1, VB
2, PP etc., and contain more colloid, the effect of extraordinary vigorate qi and replenish the blood, lung moistening calmness, bowel relieving are arranged, washing intestinal.
3, health care
Modern scientific research shows that Auricularia has the effect of antiplatelet aggregation, and can reduce the cholesterol level in the blood.Auricularia can be improved the phagocytic index and the percentage rate of mouse macrophage, to the animal of 60C ° of irradiation, can improve its survival rate, prove radiation resistance, can resist the caused leukopenia of chemicals because of the treatment tumor, Auricularia can also promote proteic biosynthesis in the mice serum.Owing to contain more Auricularia polysaccharide and materials such as colloid, vitamin in the Auricularia, the mankind there are blood sugar lowering, blood fat, the effect of fat-reducing is arranged.
Two, chitin
Chitin is a kind of bioactive substance of finding recent years; it is the Main Ingredients and Appearance of crustacean shell; be called animal fiber again; its chemistry acetyl group dextran amine by name; take off acetyl group; be called chitin again; it has multiple physiological regulation function, can comprehensive adjusting bodily fuctions, replenish the cellulose of needed by human; strengthen people's immunity; the energy activating cell enhances metabolism, and it has affinity; sterilization and row's cholesterol; chloride ion; performance such as heavy metal and radioactive substance; regulate acid-base value in the human body, thereby to have the effect of prevention and strengthening the body resistance owing to the various diseases that immunologic hypofunction caused.Good blood lipid regulation is arranged, regulate functions such as immunity, cholesterol reducing, fat-reducing.Therefore be described as the mankind's the 6th vital principle after protein, fat, saccharide, vitamin and mineral by international academic community in 1991.Up-to-date zoopery shows to have tangible antiobesity action.
Three, Radix Oenotherae erythrosepalae oil
It is the seed oil of plant Radix Oenotherae erythrosepalae, is rich in unsaturated fatty acid, and particularly it contains 10% gamma-Linolenic acid, does not have fully in Oleum Helianthi and Flos Carthami seed oil.It is the intermediate product of the N-6 polyunsaturated long-chain fatty acids of linoleic acid metabolism generation.Experimental results show that gamma-Linolenic acid has significant curative effect to reducing cholesterol and atherosclerosis and preventing and treating multiple sclerosis, and effect such as anticancer growth is arranged.Human body can not synthesize gamma-Linolenic acid, must rely on food to replenish, so be called essential fatty acid.Many in the world at present countries are all being studied Radix Oenotherae erythrosepalae oil, and the someone thinks that it is one of most important nutrient and healthcare products of finding in this century.
According to domestic report, Radix Oenotherae erythrosepalae oil 5ml/kg/d can make high fat rat blood serum T-CHOL, low-density lipoprotein cholesterol, C-VLDL reduce, and the HDL-C level is significantly raise.The variation of HDL-C be because high density lipoprotein inferior component ∏ cholesterol levels raises, and high density lipoprotein subgroup Ш gallbladder goes on foot the result that cholesterol levels does not have remarkable change admittedly.More there is report to find, rat for zinc deficiency, the Radix Oenotherae erythrosepalae oil that is rich in gamma-Linolenic acid is better than only containing the safflower oil that linoleic acid does not contain gamma-Linolenic acid, the former is lower than the latter by serum cholesterol level, the former can reduce the essential fatty acid dysbolismus that zinc deficiency causes simultaneously, and can improve the utilization of zinc in the animal body preferably.
Four, zinc gluconate
Gluconic acid is the carrier of trace element zinc, and zinc element has special role, and zinc mainly is present in human body in skeleton, skin, hair, the blood, and zinc 75%----85% is in cell in the blood, and whole body zinc amount adult is 1.4---2.2g.The nutrition physiology function of zinc mainly is: zinc is the necessary material that various zinc rely on enzyme, as alkali phosphatase, carbonic anhydrase, alcoholdehydrogenase, lactic acid dehydrogenase, glutamte dehydrogenase, carboxypeptidase, the phonetic heavy stone used as an anchor nucleoside kinase of thymus etc.Zinc also is that RNA polymerase, archaeal dna polymerase activate necessary element.Zinc also is contained in the insulin molecule, and zinc also combines with sialoprotein, ferritin, metal sulfur.This shows that zinc has important, complicated, many-sided function in human body.
The zinc deficiency influence is grown, and zinc is the element of needed by human, and zinc deficiency can cause parageusia, appetite descends, and influence is grown, and zinc deficiency influences sexual function, juvenile delay of puberty, sexual disorder also may be because zinc deficiency causes depression, insomnia, hypoimmunity, alopecia etc.So suitably zincification helps adjusting the mental status and function of human body in prescription.Add zinc and make prescription more comprehensively, favourable body metabolism makes the product quality effect better.
Five, vitamin E
The active form of vitamin E tool has 8 kinds, and promptly residual acid is in enol, but to remain alcohol, it represents vitamin E.Vitamin E is a kind of Polyphenols, and very strong antioxidation is arranged, and resists body peroxidating product free radical damage, becomes topmost active substance in the gerocomia food.
Can stop fat oxidation in food and the digestive tract as antioxidant, the protection human body cell is avoided the toxicant injury that the unsaturated fatty acids acid oxidase produces.Vitamin E self is prior to other material generation oxidations in vivo, thereby makes unsaturated fatty acid and vitamin A oxidation Decomposition in intestinal and tissue reduce to minimum degree.The biological action of vitamin E is to suppress polyunsaturated fatty acid oxidation in the tissue film, the lipid part of stabilized cell, and the protection cell is not subjected to poisonous free radical injury, prevents to wear out, and prevents organic trace to move back the aspect and works.Vitamin E can be treated hemolytic anemia as the necessary factor of protection erythrocyte integrity in addition; As the necessary factor of Cellular respiration, be that cardiac muscle and skeletal muscle tissue are breathed desired material, as the synthetic regulator of chemical compound in the body, participate in the synthetic of DNA, also may be the synthetic cofactor of vitamin C and coenzyme; Exempt from air-polluting and ruin agent as the protection lung tissue, vitamin E can also with the iodine synergism, vitamin E and iodine all are antioxidants, but both action pathway differences.
Vitamin E has protective effect on cancer risk, can prevent that chromosome from very becoming, and strengthens the activity of micropartical mixed-function oxidase, influences the carcinogen metabolism, and blocking nitrosamine formation is synthetic etc., thereby can give protection against cancer.Can strengthen the effect of DHA and EPA.Behind the scientific combination prescription, has excellent cleaning blood vessel, the effect of blood lipid regulation.
Claims (2)
1, a kind of black fungus composite soft capsule is characterized in that: its constituent is:
Auricularia polycose powder 250----350g
Radix Oenotherae erythrosepalae oil 50----70g
Chitin 3.5----5.5g
Vitamin E 3.5----7g
Zinc gluconate 0.3----1.2g
V
ASalad oil 530----630g
2, the preparation method of black fungus composite soft capsule according to claim 1, it is characterized in that: the Auricularia that (1) will clean after drying advances mechanical activation comminution, granularity is controlled at about 20 orders, promptly earlier 20 purpose Auricularia raw materials are put into container, the ethanol 90----95 degree V/V that adds 5 times of raw materials, stir, capping was soaked 1 hour, with the ethanol recover ethanol was reclaimed then; (2) the Auricularia powder after will handling is put into basin, carries out enzymolysis processing, adds the water of 40 times of raw material weights earlier, adjusts pH value scope 4.5----5.0, heat to 50----55 degree centigrade, add pectase 1%, proteinase-10 .8%, start agitator and be mixed, enzymolysis kept 4 hours, the middle stirring 1 time; (3) water is carried: raw material slag and enzymolysis solution directly are warmed up to 85----90 degree centigrade, kept 2.5----3.5 hour, coarse filtration: after raw material slag and extracting solution be cooled to room temperature, carry out screen cloth coarse filtration and filter cloth earlier and filter, the filtering residue list is put and is prepared enzymolysis and water extraction for the second time, for the first time filtrate to put into basin stand-by, same operation is carried out three times, both do the second time, extracted for the third time, again three lixiviating solution had been lumped together, carried out next procedure; (4) fine straining: with kieselguhr cardboard filter machine, above-mentioned three kinds of mixed extracts are carried out fine straining, getting filtrate, to put into basin stand-by, and (5) concentrate: use vacuum concentration pot, above-mentioned filtrate is concentrated, contain polysaccharide about 2.0 in the liquid after concentrated; (6) alcohol precipitation: with the metering of polysaccharide concentrated solution, add the 95%V/V ethanol of 2 times of volumes of concentrated solution, in precipitate with ethanol under 4----10 degree centigrade the temperature about 10 hours; (7) filter: the solution behind the precipitate with ethanol is carried out isolated by filtration, obtain polysaccharide precipitation, liquid reclaims by ethanol, and deposit mixes and carries out drying, promptly obtains polysaccharide; (8) drying: the polysaccharide precipitation material is carried out vacuum drying, and temperature is controlled at about 60 degree, prevents the polysaccharide degeneration; (9) pulverize: the polysaccharide dry matter is put into high speed disintegrator pulverize, reach the 120----200 order and be advisable, package spare; (10) mixing of powder: Auricularia polysaccharide powder, chitin, zinc gluconate are established material by formula proportion mix, require to stir, be through sterilization treatment; (11) mixing of oil preparation: with Radix Oenotherae erythrosepalae oil, vitamin E, V
ASalad oil mixes; (12) slurrying is handled: powder intermixture and oil preparation intermixture are mixed, handle through the mechanical agitation making beating, handle through colloidal grinding, obtain the oil preparation mixed serum, be incubated under 50 degrees centigrade of situations, prepare next procedure and make soft capsule; (13) glue: have blender and heating, cooling, insulation, system vacuum function in the glue jar, after the tank body sterilization, put into the steaming slide earlier and be heated to 80 degrees centigrade, add gelatin again, solid-to-liquid ratio is 1: 2, add an amount of glycerol again and stir, evacuation 4 hours is cooled to 50 degrees centigrade, be incubated 2 hours, be put in the jar that links to each other with pellet processing machine, follow procedure starts pellet processing machine, makes soft capsule.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB200510009721XA CN100450493C (en) | 2005-02-07 | 2005-02-07 | Black fungus composite soft capsule and its preparing process |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB200510009721XA CN100450493C (en) | 2005-02-07 | 2005-02-07 | Black fungus composite soft capsule and its preparing process |
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| CN1682985A CN1682985A (en) | 2005-10-19 |
| CN100450493C true CN100450493C (en) | 2009-01-14 |
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| CN104523770A (en) * | 2014-12-05 | 2015-04-22 | 黑龙江众生生物工程有限公司 | Auriculacin soft capsule and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1413605A (en) * | 2001-10-26 | 2003-04-30 | 连汝安 | Soft capsule capable of removing human peculliar smell |
| CN1526315A (en) * | 2003-03-06 | 2004-09-08 | 海南中旭信实业有限公司 | Prepn of health article of edible fungus polysaccharide |
| CN1528339A (en) * | 2003-10-20 | 2004-09-15 | 南京金陵尹氏保健品有限公司 | Chitin soft capsule and preparing method thereof |
-
2005
- 2005-02-07 CN CNB200510009721XA patent/CN100450493C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1413605A (en) * | 2001-10-26 | 2003-04-30 | 连汝安 | Soft capsule capable of removing human peculliar smell |
| CN1526315A (en) * | 2003-03-06 | 2004-09-08 | 海南中旭信实业有限公司 | Prepn of health article of edible fungus polysaccharide |
| CN1528339A (en) * | 2003-10-20 | 2004-09-15 | 南京金陵尹氏保健品有限公司 | Chitin soft capsule and preparing method thereof |
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| CN1682985A (en) | 2005-10-19 |
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