CN100386389C - Dyeing liquid, dye and their prepn process - Google Patents
Dyeing liquid, dye and their prepn process Download PDFInfo
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- CN100386389C CN100386389C CNB2005100433795A CN200510043379A CN100386389C CN 100386389 C CN100386389 C CN 100386389C CN B2005100433795 A CNB2005100433795 A CN B2005100433795A CN 200510043379 A CN200510043379 A CN 200510043379A CN 100386389 C CN100386389 C CN 100386389C
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Abstract
The present invention discloses dyeing liquid, a dyeing agent and a preparation method thereof. The dyeing agent comprises white medicine liquid, yellow medicine liquid, black medicine liquid and color powder, wherein the mass ratio of the yellow medicine liquid to the black medicine liquid to the white medicine liquid to the color powder is (7 to 18): (14 to 24): (1 to 12): 1. The dyeing liquid comprises water and four dyeing agents of which the main colors are respectively red, blue, black and yellow, wherein the volume proportion of the water to the dyeing agents is 1: (6 to 10), the four dyeing agents are the described dyeing agents, and the dyeing liquid is formed by that the four dyeing agents of which the main colors are the red, the blue, the black and the yellow are mixed to be prepared by adding water, or the liquid is dyed in different steps to be synthesized in a color matching mode according to the requirements of a customer. The dyeing agent of the present invention is a special NA hydrophily dyeing material, and has universality; therefore, a large quantity of funds for purchasing dyeing devices are unnecessarily invested, and various kinds of dyeing medicine liquid are not needed in each industry which with dyeing requirements; dyeing liquid prepared by the dyeing agent of the present invention can be used for dyeing so that the dyeing cost can be greatly reduced.
Description
Technical field
The present invention relates to staining fluid, stain and method of manufacturing technology thereof.
Background technology
Along with the development of society, the raising of standard of living and science and culture artistic level, people not only have very high requirement but also the height of shape, color and the artistic composition thereof of product appearance are also had very high requirement the quality of product.The step process that in the whole prod manufacturing processed color and the artistic composition thereof of product is played an important role is a dyeing process.Therefore all trades and professions of dyeing in the society now scope that all has a wide range of applications.The technician that existing dyeing industry generally needs special dyeing installation and need have the dyeing liquid medicine outfit technology of specialty.In the prior art, general to different materials, the outfit ratio of dyeing liquid medicine has very big difference.This just makes needs painted every profession and trade, and eyeglass dyeing, mirror holder dyeing such as spectacles industry all need special dyeing installation and needs the technical professional, and then make the dyeing cost of this every profession and trade increase, manufacturing cost increases, and this dyeing trouble, and dyeing kinetics is not high yet.
Summary of the invention
The purpose of this invention is to provide a kind of staining fluid, stain and method of manufacturing technology thereof, it has solved the existing technical disadvantages of background technology, and the required cost that dyes is low, and dyeing quality is good, and dyeing is fast convenient.
The present invention adopts following technical scheme: a kind of stain, described stain comprise baiyao water, xanthate water, black powder water and toner; Mass ratio between xanthate water, black powder water, baiyao water, the toner is (7～18): (14～24): (1～12): 1; Wherein, baiyao water is used for fixation; Xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance; Toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant.
Also comprise solubility promoter, it is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body; Mass ratio between xanthate water, black powder water, baiyao water, solubility promoter, the toner is (7～18): (14～24): (1～12): (14～24): 1.
Mass ratio between described xanthate water, black powder water, baiyao water, solubility promoter, the toner is (12～13): (18～19): (6～7): (18～19): 1.
The color of described stain is red, blue, black or yellow.
The present invention adopts another following technical scheme: a kind of staining fluid, and it comprises that water and four kinds of mass-tones are respectively red, blue, black, yellow stain, the volume ratio of water and stain is 1: (6～10); Described four kinds of stains include baiyao water, xanthate water, black powder water and toner; Mass ratio between xanthate water in each stain, black powder water, baiyao water, the toner is (7～18): (14～24): (1～12): 1; Wherein, baiyao water is used for fixation; Xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance; Toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant;
Staining fluid is that red, blue, black, yellow four kinds of stains mix and add the water allotment and form or adopt the synthetic toning of gradation dyeing according to client's needs by mass-tone.
Each stain also comprises solubility promoter, and it is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body; Mass ratio between xanthate water, black powder water, baiyao water, solubility promoter, the toner is (7～18): (14～24): (1～12): (14～24): 1.
The present invention adopts following technical scheme: a kind of method of manufacturing technology of stain:
A, first step: be used to mix xanthate water and black powder water, and stir institute's blended mixture to mixing; Mass fraction between xanthate water, the black powder water is respectively (7～18) part, (14～24) part; Wherein, xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance;
B, second step: the mixture that is used for behind first step adds toner, and stirs institute's blended mixture to mixing; The toner mass fraction is 1 part; Wherein, toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant;
C, third step: the mixture that is used for after second step adds baiyao water, and stirs institute's blended mixture to dissolving fully; Baiyao quality umber is (1～12) part; Wherein, baiyao water is used for fixation.
Also comprise:
D, the 4th step: the mixture that is used for behind third step adds solubility promoter, and stirs institute's blended mixture to mixing; The solubility promoter mass fraction is (14～24) part; Wherein, solubility promoter is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body.
Churning time in the described first step is about 30 minutes at normal temperatures; Churning time in second step is about 60 minutes at normal temperatures; Churning time in the third step is about 30 minutes at normal temperatures; Churning time in the 4th step is about 30 minutes at normal temperatures; And the churning time in the described first step, the churning time in second step, the churning time in the third step, the churning time in the 4th step are along with the high more then required churning time of the temperature of heating is short more.
By the above-mentioned description of this invention as can be known, compare with background technology, the present invention has following advantage:
One, stain of the present invention is the special water soluble dyestuffs of NA, has versatility, it is specially adapted to the dyeing of materials such as AC, CP, CA, PC, PET, CR-39 and part titanium metal, the NA dyestuff integrates various functions, using method is very simple, and using method is as follows: the first, and shake up the back and take out NA dyestuff portion; The second, the water that directly adds more than 6 times can constitute staining fluid; The 3rd, get final product substantive dyeing by staining fluid; So need painted every profession and trade, need not drop into substantial contribution and buy dyeing installation and oneself add the various painted liquid medicine of outfit, the staining fluid that only needs to be equipped with out by stain of the present invention can dye, and the dyeing cost reduces greatly;
Its two, staining fluid of the present invention is that red, blue, black, yellow four kinds of stain mixing and water addings allotment forms according to client's needs by mass-tone, can arbitrarily mix colours; Or adopt the synthetic toning of gradation dyeing, be by catching staining fluid of all kinds successively, and to make the color of the material table matter that is colored body reach the needed color of client;
Its three, staining fluid of the present invention after once using, reuses as need next time, then only needs impurity screening to reuse, and does not cause waste, reduces cost the protection environment;
Its four, baiyao water is by entering color penetration on material table matter top layer, and makes the baiyao glassware for drinking water that good fixing property be arranged;
Its five, staining fluid of the present invention can dye at normal temperatures to materials such as AC, CP, CA, PC, PET, CR-39 and part titanium metal dyeing; To AC, PC, the dyeing of part titanium metal, then colouring is very fast in dyeing under the condition of heating, and 30-40 can paint second usually, and can not ftracture; PC, part titanium metal, dyeing, then better effects if under temperature is spent greater than 80;
Its six, staining fluid of the present invention, can dye, and dyeing kinetics is also fast more along with temperature is high more then between 20 degree-95 degree to materials such as AC, CP, CA, PC, PET, CR-39 and part titanium metal dyeing;
Its seven, by staining fluid of the present invention, fixation is good, colouring property is good.
Embodiment
Embodiment one
A kind of stain comprises baiyao water, xanthate water, black powder water, toner and solubility promoter.
Wherein baiyao water, xanthate water, black powder water and solubility promoter are commercially available product on the existing market.As: there is Wuhan Youji Industrial Company Limited in the aquatic product of baiyao producer, and this manufacturer address is positioned at No. 10, bridge oral region workers and peasants road, Wuhan City; There is fine chemistry industry head factory in border in the Shenyang in the manufacturer of xanthate water and black powder water, and this manufacturer address is positioned at Dadong District Guan Quan road, Shenyang 8-7 number.The sale producer of toner and solubility promoter has Quanzhou City's spring to contain the pigment shop, and its address is positioned at No. 5 54 Room, Quangang District Kingsoft, Quanzhou City street.
The main component of baiyao water is a phenylcarbinol, and it can enter color penetration material table matter top layer, strengthens fixing property, accelerates dyeing kinetics, strengthens the colouring performance; , but make sure to keep in mind can not be excessive, because can destroy material table matter when excessive, can produce white band (as the ladder lineae ablicantes) on material table matter.
Xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; More can make to be colored body such as eyeglass, smooth and be easy to clean, but as the excessive staining fluid that then can make be difficult for dissolving, and can make dyeing be uneven shape.
Xanthate water and baiyao water cooperate with the protection eyeglass; And making that colouring property is good, fixation is good.
Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance; But when excessive, then can make dyeing be difficult for dissolving fully, and can make dyeing be uneven shape, can on material table matter, produce black band.The technical indicator of black powder water is: outward appearance: the brown transparent liquid; Ionic: negatively charged ion; Chemical constitution: teepol, water, STPP (sodium tripolyphosphate), sodium hydroxid; Content: the ratio of teepol, water, STPP (sodium tripolyphosphate), sodium hydroxid is 20: 75: 3: 2; 1; Boiling point: about 100 degree; PH (100%): about 8.5; Water-soluble: dissolving easily in the cold water; Flashing point: do not have; Chemical safety: with safety under the normal condition; Purposes: dyeing and finishing auxiliaries.
Toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant.Existing toner includes two kinds of water-based and oiliness, and what adopt in the present embodiment is the water-based toner.Toner with color and luster own enough whether add an amount of it, various colors can mix mutually can generate various color.As red, yellow, the blue ratio of toner is 1: 1: 1, and it is dark brown then to be approximately generation.
Solubility promoter is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body.As allocating high density and colouring speed dyestuff faster, just need to add dyeing auxiliaries to help dissolving.Thereby, various liquid medicine under the high density state and toner cause the dissolving difficulty because all can separating out, also can play the help solvency action though improve xanthate water ratio, but this also can cause dyeing kinetics slack-off, therefore the effect that adds special-purpose dyeing auxiliaries can be better, also can make redeployed dyestuff have transparency preferably.Solubility promoter is general solubility promoter in the existing dye field.
Quality between above-mentioned xanthate water, black powder water, baiyao water, solubility promoter, the toner can be respectively 5kg, 7.5kg, 2.5kg, 7.5kg, 400g.
In the present embodiment, the stain of generation is respectively four kinds of mass-tones, and is red, blue, black, yellow.
Embodiment two
A kind of staining fluid comprises that water and four kinds of mass-tones are respectively red, blue, black, yellow stain, and the volume ratio of water and stain is 1: (6～10).
Water as adding is few, and then concentration is dense, and this staining fluid dyeing is fast; The water that adds is many, and then concentration is rare, and this staining fluid dyeing is slow.Generally will be colored body such as eyeglass puts into staining fluid and only needs 60-150s can finish dyeing; Being colored body and can using ultrasonic cleaning after the dyeing.
The stain of present embodiment such as embodiment one description.Stain manufacturer produces the stain with four kinds of mass-tones; Need painted every profession and trade to buy the stain of these four kinds of mass-tones, oneself be deployed into the staining fluid of required color then as required by fine arts method; Or adopt gradation dyeing to synthesize required color.
Can be combined into shades of colour by yellow, red, primary colors.Can be such as golden color by yellow and red combination furnishing, most dyestuff also all is a synthetic on such basis, and still, shades of colour all has different separately dye uptakes, and the height of painted time length and temperature all a little aberration can occur.Therefore high-precision staining fluid is generally formed by the stain allotment of four kinds of mass-tones, and it generally adopts the synthetic toning of gradation dyeing, and red colouration is synthetic again can to dye blueness earlier as green colouring; Dye grey and can dye black earlier and dye bluely synthetic or the like again, large batch of dyeing can be write down each synthetic painted time so that the dyeing of each batch is synthetic.It should be noted that: color has dyed shallow can to deepen, shoal with regard to bad but dyed deeply then.
Dyeing temperature during staining fluid dyeing: between the 20-95 degree, spend (it is decided according to staining section) usually but preferably be fixed on 90.Its rule is: temperature is high more, and color and luster is dark more blue more; Temperature is low more, the shallow more tea more of color and luster.
The pass of staining fluid dyeing time and speed is: dyeing time and dyeing kinetics are directly proportional, and the dyeing kinetics of one is slow more, and the time is long more, otherwise then short more.Usually dyeing time might not, by dyeing the depth, evenly deciding.Time is long, and speed is then best slowly, and speed is slow more, and color and luster is dark more, otherwise then shallow more.
Color and luster depth control method is:
1, can directly be colored the color and luster depth of body with dyeing kinetics control; Or directly control the color and luster depth that is colored body with the height of temperature;
2, when making stain, the ratio of available three kinds of liquid medicine, control is colored the color and luster depth of body:
A, need chromosomal color and luster deeply then can: mix with three kinds of liquid medicine and to add, also can be, but had better not use baiyao water separately separately with the adding of baiyao water because the bad phenomenon of white band easily takes place in excessive baiyao water in the material table matter that is colored body;
B, need chromosomal lighter color then can: add with xanthate water or black powder water and get final product, also can add water and shoal, be in the time through reinforcement but add the bad of water, fade, so if add water excess, the eyeglass that is dyed must be gone into the furnace oven dry earlier and just can be strengthened, ten million just can not dry and strengthens.
To the chromosomal test piece method after the dyeing be as required:
1, takes out model (the needed color model of client that this needs painted industry is mainly used in and checks colors), stand under the fluorescent lamp (desk lamp), under this model blank sheet of paper need be arranged;
2, open the action power of dyeing machinery, gas lift revolves liter;
3, a slice being colored body such as eyeglass is loaded on and carries out test piece on the framework;
When a, test piece, if model is reinforcement (reinforcement refers to: can not be worn or abrade through the eyeglass of strengthening) person, directly checking colors gets final product;
B, if model for strengthening the person, not directly check colors, must be with the eyeglass that is tried out, be put in the hot water half a minute approximately, put into cold water again and cool off, checking colors could be correctly.
Cooperate above-mentioned test piece method, the ratio of painted each stain is adjusted.
Be colored the existing shortcoming in body dyeing back, have the reason of shortcoming and the solution of this shortcoming.
Shortcoming 1, dyeing is uneven: promptly lens surface has the current mark phenomenon;
As its occurrence cause be: staining agent is dissolving fully not; Then solution is: stir more;
As its occurrence cause be: toner is for inferior, and dyeing time is long to be caused, dyeing kinetics is slow; Then solution is: dyeing time is short, and it is fast that dyeing kinetics is wanted.
Shortcoming 2, breakpoint: promptly lens surface is just like by cutting phenomenon therefrom (disconnected joint);
Its occurrence cause is: staining agent is dissolving fully not; Then solution is: stir more.
Shortcoming 3, the grains of sand: promptly lens surface has one deck grains of sand, wipes and can remove with hand, but can't clean.
Its occurrence cause is: it is too much that toner is put, fusing fully; Then solution is: stir more.
Shortcoming 4, white band: i.e. lens surface adularescent ladder line;
Its occurrence cause is: black powder water is excessive; Then solution is: add water or add xanthate water restir.
Shortcoming 5, black band: promptly specular surface has black band (ladder line);
As its occurrence cause be: black powder water is excessive; Then solution is: add water or add xanthate water restir;
As its occurrence cause be: dyeing time is long; Then solution is: shorten dyeing time.
Embodiment three
A kind of method of manufacturing technology of stain:
A, first step: be used to mix xanthate water and black powder water, and stirred at normal temperatures 30 minutes, make institute's blended mixture to mixing; Mass fraction between xanthate water, the black powder water is respectively (7～18) part, (14～24) part; Wherein, xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance;
B, second step: the mixture that is used for behind first step adds toner, and stirs at normal temperatures 60 minutes, makes institute's blended mixture to mixing; The toner mass fraction is 1 part; Wherein, toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant;
C, third step: the mixture that is used for after second step adds baiyao water, and stirs at normal temperatures 30 minutes, makes institute's blended mixture to dissolving fully; Baiyao quality umber is (1～12) part; Wherein, baiyao water is used for fixation.
Also comprise:
D, the 4th step: the mixture that is used for behind third step adds solubility promoter, and stirs at normal temperatures 30 minutes, makes institute's blended mixture to mixing; The solubility promoter mass fraction is (14～24) part; Wherein, solubility promoter is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body.
Quality between above-mentioned xanthate water, black powder water, baiyao water, solubility promoter, the toner can be respectively 5kg, 7.5kg, 2.5kg, 7.5kg, 400g.
Churning time in the described first step, the churning time in second step, the churning time in the third step, the churning time in the 4th step are along with the high more then required churning time of the temperature of heating is short more.Open simultaneously and temperature heater when opening stirrer, temperature is when the 80 degree left and right sides, and churning time can reduce half.
The above, only for preferred embodiment of the present invention, so can not limit scope of the invention process with this, i.e. the equivalence of doing according to the present patent application claim and description changes and modification, all should still belong in the scope that patent of the present invention contains.
Claims (9)
1. stain, it is characterized in that: described stain comprises baiyao water, xanthate water, black powder water and toner; Mass ratio between xanthate water, black powder water, baiyao water, the toner is (7～18): (14～24): (1～12): 1; Wherein, baiyao water is used for fixation; Xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance; Toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant.
2. a kind of stain according to claim 1 is characterized in that: also comprise solubility promoter, it is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body; Mass ratio between xanthate water, black powder water, baiyao water, solubility promoter, the toner is (7～18): (14～24): (1～12): (14～24): 1.
3. a kind of stain according to claim 2 is characterized in that: the mass ratio between described xanthate water, black powder water, baiyao water, solubility promoter, the toner is (12～13): (18～19): (6～7): (18～19): 1.
4. a kind of stain according to claim 3 is characterized in that: the color of described stain is red, blue, black or yellow.
5. staining fluid, it is characterized in that: it comprises that water and four kinds of mass-tones are respectively red, blue, black, yellow stain, and the volume ratio of water and stain is 1: (6～10);
Described four kinds of stains include baiyao water, xanthate water, black powder water and toner; Mass ratio between xanthate water in each stain, black powder water, baiyao water, the toner is (7～18): (14～24): (1～12): 1; Wherein, baiyao water is used for fixation; Xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance; Toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant;
Staining fluid is that red, blue, black, yellow four kinds of stains mix and add the water allotment and form or adopt the synthetic toning of gradation dyeing according to client's needs by mass-tone.
6. a kind of staining fluid according to claim 5 is characterized in that: also comprise solubility promoter in each stain, it is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body; Mass ratio between xanthate water, black powder water, baiyao water, solubility promoter, the toner is (7～18): (14～24): (1～12): (14～24): 1.
7. the method for manufacturing technology of a stain: it is characterized in that:
A, first step: be used to mix xanthate water and black powder water, and stir institute's blended mixture to mixing; Mass fraction between xanthate water, the black powder water is respectively (7～18) part, (14～24) part; Wherein, xanthate water is used to protect the material table matter that is colored body, and makes material table matter shinny; Black powder water is used for the dyeing of assisted staining liquid, and makes stain reach balance;
B, second step: the mixture that is used for behind first step adds toner, and stirs institute's blended mixture to mixing; The toner mass fraction is 1 part; Wherein, toner is formed by the allotment of fine arts method by primitive colour reddish yellow indigo plant;
C, third step: the mixture that is used for after second step adds baiyao water, and stirs institute's blended mixture to dissolving fully; Baiyao quality umber is (1～12) part; Wherein, baiyao water is used for fixation.
8. the method for manufacturing technology of a kind of stain according to claim 7: it is characterized in that: also comprise:
D, the 4th step: the mixture that is used for behind third step adds solubility promoter, and stirs institute's blended mixture to mixing; The solubility promoter mass fraction is (14～24) part; Wherein, solubility promoter is used to accelerate the staining fluid dyeing kinetics, and increases transparency and the brightness that is colored body.
9. the method for manufacturing technology of a kind of stain according to claim 8: it is characterized in that: the churning time of described first step is about 30 minutes at normal temperatures; The churning time of second step is about 60 minutes at normal temperatures; The churning time of third step is about 30 minutes at normal temperatures; The churning time of the 4th step is about 30 minutes at normal temperatures; And the churning time of the churning time of the churning time of described first step, second step, the churning time of third step, the 4th step is along with the high more then required churning time of the temperature of heating is short more.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100433795A CN100386389C (en) | 2005-04-21 | 2005-04-21 | Dyeing liquid, dye and their prepn process |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100433795A CN100386389C (en) | 2005-04-21 | 2005-04-21 | Dyeing liquid, dye and their prepn process |
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| CN1810890A CN1810890A (en) | 2006-08-02 |
| CN100386389C true CN100386389C (en) | 2008-05-07 |
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| CNB2005100433795A Expired - Fee Related CN100386389C (en) | 2005-04-21 | 2005-04-21 | Dyeing liquid, dye and their prepn process |
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| CN114369964A (en) * | 2021-11-30 | 2022-04-19 | 惠州市艺康新材料科技有限公司 | Coloring agent and coloring method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199176A (en) * | 1997-05-09 | 1998-11-18 | 杨波 | Thermal dyeing process of eye-protecting optical resin lens |
| US20030182737A1 (en) * | 2002-03-29 | 2003-10-02 | Hoya Corporation | Method of dyeing thermoplastic resin and colored plastic lens obtainable by that method |
-
2005
- 2005-04-21 CN CNB2005100433795A patent/CN100386389C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199176A (en) * | 1997-05-09 | 1998-11-18 | 杨波 | Thermal dyeing process of eye-protecting optical resin lens |
| US20030182737A1 (en) * | 2002-03-29 | 2003-10-02 | Hoya Corporation | Method of dyeing thermoplastic resin and colored plastic lens obtainable by that method |
Non-Patent Citations (4)
| Title |
|---|
| CR-39树脂镜片染色工艺的研究. 于丽霞.塑料，第32卷第63期. 2003 |
| CR-39树脂镜片染色工艺的研究. 于丽霞.塑料，第32卷第63期. 2003 * |
| 浅谈染色镜片. 杨波.中国眼镜科技杂志，第5期. 2005 |
| 浅谈染色镜片. 杨波.中国眼镜科技杂志，第5期. 2005 * |
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